• 한국전기전자재료학회논문지
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• 제35권5호
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• pp.431-438
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• 2022

기능성 소재연구에서 in situ 분석 기법은 외부 자극 (전기장, 자기장, 빛, 등) 또는 주변 환경 (온도, 습도, 압력, 등)과 같이 주어진 자극에 의해 소재의 물리적 특성이 어떻게 활성화/진화되는지 분석하는데 있어서 매우 중요하다. 특히, 전기장 인가에 따른 in situ X-선 회절(XRD) 실험은 다양한 강유전체, 압전체, 전왜 재료의 외부 전기장 인가에 따른 전기-기계적 반응의 기본 원리를 이해하기 위해 광범위하게 활용되었다. 본 튜토리얼 논문에서는 일반 실험실 규모의 XRD 장비를 이용하여 전기장 인가에 따른 in situ XRD 분석의 기본 원리/핵심 개념을 간략하게 소개한다. In situ XRD 측정법은 외부 전기장을 인가하여 구동되는 다양한 전기-기계 재료의 구조적 변형을 체계적으로 식별/모니터링하는 데 매우 유용할 것으로 기대한다.

• 터널과지하공간
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• 제14권4호
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• pp.295-303
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• 2004

연약층과 견고한 암반층이 습곡형태로 혼재된 지질조건의 지하 심부 채굴 현장을 대상으로, 심부 급경사 연약층의 단계적 굴착 진행에 따른 갱도 및 주변 암반의 거동 양상을 전산해석과 현장계측을 통하여 비교 분석하였다. 전산해석에서는 Hoek ＆ Brown의 경험적 파괴기준 및 변형률연화모델을 적용한 탄소성 해석 기법을 이용하였다. 현장계측에서는 유압캡슐, 지중변위계, 내공변위계를 갱도 및 주변 암반에 설치하여 응력과 변위를 계측하였다. 경험적 파괴조건 및 변형률연화모델을 이용한 탄소성 해석은, 현장 지질조건 및 채굴과정의 복잡함에도 불구하고 현장계측결과와 유사한 양상을 보여주어 타당성을 검증할 수 있었다. 이러한 전산해석 및 현장계측의 비교를 통해 지하 굴착 갱도의 변형 거동 과정을 예측하고 이후의 굴착 및 지보보강 설계의 지침을 제공할 수 있을 것이다.

• 방사선산업학회지
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• 제17권1호
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• pp.1-9
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• 2023

Since a large amount of radioactive waste is expected to be generated due to permanent shutdown of many nuclear power plants, it is necessary to prepare efficient management methods for radioactive waste. Therefore, there is a need for a based study to apply the In-Situ gamma spectrometry, which can simplify the measurement procedure. The purpose of this study is to analyze research cases of In-Situ gamma spectrometry and to analyze the sensitivity of measurement according to influencing factors on In-Situ gamma spectrometry. Research cases of five institutions, including the CERN and the Imperial College Reactor Centre (ICRC), were selected as the institutions to be investigated. Research on the In-Situ gamma spectrometry was conducted on the satisfaction of the acceptance criteria for radioactive waste and the analysis of residual radioactivity in the site. In-Situ Objective Counting System (ISOCS) was used as a major measuring device. Sampling and computer code were used to verify the analysis results. For evaluation of measuring sensitivity according to influencing factors on In-Situ gamma spectrometry, the thickness of the measurement target, the distance between the detector and the target, the angle of the collimator, and the contamination location were performed using ISOCS's Geometry Composer. In every case, based on 122 keV, the efficiency decreased as the energy increased in the high energy region, and the efficiency decreased as the energy decreased in the low energy region. As the target thickness increased, the efficiency decreased, and as the distance between target and detector increased, the efficiency decreased. As the distance between contamination and detector increased, the efficiency decreased, and as the angle of the collimator increased, the measurement efficiency increased. However, when simulating the measurement situation using Geometry Composer, the background is not considered, and the probability of incident in the background increases as the angle increases, so further research needs to be conducted in consideration of these. This study can be utilized when applying the In-Situ gamma spectrometry of radioactive waste clearance in the future.

• Corrosion Science and Technology
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• 제23권2호
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• pp.113-120
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• 2024

An attempt was made to apply digital image correlation (DIC) strain analysis to in-situ scanning electron microscopy (SEM) observations of bending deformation to quantify local strain distribution inside a ZnMgAl-alloy coating in deformation. Interstitial-free steel sheets were hot-dipped in a Zn-3Mg-6Al (mass%) alloy melt at 400 ℃ for 2 s. The specimens were deformed using a miniature-sized 4-point bending test machine inside the SEM chamber. The observed in situ SEM images were used for DIC strain analysis. The hot-dip ZnMgAl-alloy coating exhibited a solidification microstructure composed of a three-phase eutectic of fine Al (fcc), Zn (hcp), and Zn2Mg phases surrounding the primary solidified Al phases. The relatively coarsened Zn₂Mg phases were locally observed inside the ZnMgAl-alloy coating. The DIC strain analysis revealed that the strain was localized in the primary solidified Al phases and fine eutectic microstructure around the Zn₂Mg phase. The results indicated high deformability of the multi-phase microstructure of the ZnMgAl-alloy coating.

• Bulletin of the Korean Chemical Society
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• 제33권5호
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• pp.1577-1580
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• 2012

The orientational and dynamic behavior of liquid crystal molecules on the alignment layer surfaces of liquid crystal display (LCD) devices is crucial to their performance, but there are only a few methods of experimentally elucidating the interactions between the liquid crystals and the alignment layers. Inspired by the natural and technical similarities between membrane proteins in lipid bilayers and liquid crystals in LCDs, we employed solid-state NMR methodologies originally developed for the study of membrane proteins in lipid bilayers for the in-situ analysis of liquid crystal display panels. In this article, we present a home-built 500 MHz narrowbore (NB) The orientational and dynamic behavior of liquid crystal molecules on the alignment layer surfaces of liquid crystal display (LCD) devices is crucial to their performance, but there are only a few methods of experimentally elucidating the interactions between the liquid crystals and the alignment layers. Inspired by the natural and technical similarities between membrane proteins in lipid bilayers and liquid crystals in LCDs, we employed solid-state NMR methodologies originally developed for the study of membrane proteins in lipid bilayers for the in-situ analysis of liquid crystal display panels. In this article, we present a home-built 500 MHz narrowbore (NB) $^{19}F-^{13}C$ double resonance solid-state NMR probe with a flat-square coil and the first application of this probe for the in-situ analysis of LCD panel samples. double resonance solid-state NMR probe with a flat-square coil and the first application of this probe for the in-situ analysis of LCD panel samples.

• Applied Microscopy
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• 제45권4호
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• pp.208-213
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• 2015

Nanomanipulators installed in focused ion beam (FIB), which is used in the lift-out of lamella when preparing transmission electron microscopy specimens, have recently been employed for electrical resistance measurements, tensile and compression tests, and in situ reactions. During the pick-up process of a single nanowire (NW), there are crucial problems such as Pt, C and Ga contaminations, damage by ion beam, and adhesion force by electrostatic attraction and residual solvent. On the other hand, many empirical techniques should be considered for successful pick-up process, because NWs have the diverse size, shape, and angle on the growth substrate. The most important one in the in-situ precedence, therefore, is to select the optimum pick-up process of a single NW. Here we provide the advanced methodologies when manipulating NWs for in-situ mechanical and electrical measurements in FIB.

• 한국지반공학회:학술대회논문집
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• 한국지반공학회 2000년도 봄 학술발표회 논문집
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• pp.167-172
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• 2000

In this study, the behaviors of a cast-in-situ concrete pile embedded in the weathered rock were analysed by a 3D numerical analysis using PENTAGON 3D and the results were compared with those of the field load test. The load-settlement relation and the load transfer relationship were evaluated from the numerical analysis. As a result, the load-settlement relation at the pile top and the axial load distribution with depth were predicted reasonably. And those results were similar with those of the field load test.

• 한국세라믹학회지
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• 제56권3호
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• pp.308-316
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• 2019

CdS_xSe_1-x ternary alloy nanowires (x = 0, 0.5, 1.0) were fabricated by in-situ synthesis on interdigitated electrode. Morphology analysis of the alloy nanowires according to the synthesis zone and composition analysis of the nanowires were carried out by SEM and EDX. The crystal structures of the alloy nanowires were studied by XRD analysis. The I-V characteristics of the nanowire photosensors were analyzed according to the intensity of incident light. The influence of zonal synthesis position on the photosensor response to the wavelength of incident light was also analyzed, and was found to be related to the bandgap of alloy nanowires. The analysis results indicate that photosensors with a specific photoresponse could be selected based on the composition of the source materials of nanowires as well as by controlling the in-situ synthesis zone.

• 소성∙가공
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• 제16권3호
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• pp.210-214
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• 2007

Manufacturing bulk nanostructured materials with least grain growth from initial powders is challenging because of the bottle neck of bottom-up methods using the conventional powder metallurgy via compaction and sintering. In the study, densification behavior of nano Cu powders during pressureless sintering was investigated using an in-situ optical dilatometer technique. The initial heating and steady temperature stages during the sintering of nano Cu powder compacts were observed. At the initial heating stage, the powder compact has many porosities and full densification needs high temperature and/or high pressure sintering. In the experimental analysis, changes in geometry and density were measured and discussed for optimal consolidation and densification by the in-situ optical dilatometer.

• 대한기계학회논문집B
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• 제29권12호
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• pp.1307-1312
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• 2005

Turbulent in-situ mixing process is a new material process technology to get dispersed phase in nanometer size by controlling reaction of liquid/liquid, liquid/solid and liquid/gas, flow and solidification speed simultaneously. In this study mixing, the key technology to this synthesis method will be studied by computational fluid dynamics. For the simulation of mixing of liquid metal, static mixers will be investigated. Two inlets for different liquid metal meet and merge like 'Y' shape tube. The tube has various shapes such as straight and curved. Also, the radius of curve will be varied. The performance of mixer will be evaluated with quantitative analysis with coefficient of variance of mass fraction. Also, detailed plots of intersection will be presented to understand effect of mixer shape on mixing.