• 제목/요약/키워드: in-situ SEM

검색결과 197건 처리시간 0.022초

Preventive Effect of Sugar-free Chewing Gum Containing Maltitol on Dental Caries in situ

  • Lee, Eun-Jung;Jin, Bo-Hyoung;Paik, Dai-Il;Hwang, In-Kyeong
    • Food Science and Biotechnology
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    • 제18권2호
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    • pp.432-435
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    • 2009
  • The preventive effect of chewing gum containing maltitol, xylitol, gum base, and sugar on remineralization were investigated. The clinical study consisted of 8 weeks' randomized, double blind, controlled, cross-over clinical trials including 24 healthy adults had chew gum. After each test week, remineralization effect was evaluated by measuring microhardness and scanning electron microscopy (SEM). Microhardness of experimental chewing gum containing maltitol or xylitol was significantly higher than that of sugar gum (p<0.005). Images of SEM showed the remineralization effect of gum containing gum base, maltitol, or xylitol compared with sugar gum. Maltitol and xylitol gums were more effective in remineralization than sugar gum. It was concluded that maltitol and xylitol can be used as sugar substitute to prevent dental caries.

Development of methodology for evaluating tribological properities of Ion-implanted steel (이온 주입한 강의 미시적 마모 튼성의 평가)

  • MOON, Bong-Ho;CHOI, Byung-Young
    • Journal of the Korean Society for Precision Engineering
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    • 제14권9호
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    • pp.146-154
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    • 1997
  • Ion implantation has been used successfully as a surface treatment technology to improve the wear. fatigue and corrosion resistances of materials. A modified surface layer by ion implantation is very thin(under 1 m), but it has different mechanical properties from the substrate. It has also different wear characteristics. Since wear is a dynamic phenomenon on interacting surfaces with relative motion, an effective method for investigtating the wear of a thin layer is the observation of wear process in microscopic detail using in-situ system. The change of wear properties produces the transition of wear mode. To know the microscopic wear mechanism of this thin layer, it is very important to clarify its microscopic wear mode. In this paper, using the SEM and AFM Rribosystems as in-situ system, the microscopic wear of Ti ion-implanted 1C-3Cr steel, a material for roller in the cold working process, was investigated in repeated sliding. The depth of wear groove and the speciffc wear amount were changed with transition of microscopic wear mode. The depth of wear groove with friction cycles in AFM tribosystem and specific wear amount of Ti ion-implanted 1C-3Cr steel were less about 2-3 times than those of non-implanted 1C-3Cr steel. The microscopic wear mechansim of Ti ion-implanted 1C-3Cr steel was also clarified. The microscopic wear property was quantitatively evaluated in terms of microscopic wear mode and specific wear amount.

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Estimation of Machinability of Lead Brass Based on In-Situ Observation in Scanning Electron Microscope (전자현미경 In-Situ 관찰방법을 이용한 황동의 절삭성평가)

  • Jung, Seung-Boo;Lim, Ok-Dong;An, Seong-Uk
    • Applied Microscopy
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    • 제24권3호
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    • pp.87-93
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    • 1994
  • In order to elucidate the machinability of lead brass, orthogonal machining experiment was conducted in SEM(Scanning Electron Microscope) equipped with a micro-machining device at a cutting speed of $7{\mu}m/s$ for brass containing 0.2 to 3wt% Pb. The microfactors (i.e., shear angle, contact length between chip and tool) were determined by in-situ observations. Machinability of brass containing lead is discussed in terms of the microfactors and the cutting resistant force tested by lathe cutting. The dynamic behavior of the chip formation of lead brass during the machining process was examined: The chips of lead brass form as a shear angle type. The shear angle increases with the content of lead in (6:4) brass. The pronounced effect of lead on the contact length between chip and tool was observed above 1% Pb. The cutting resistant force tested by lathe decreases remarkably with the lead content in brass. The observed microfactors are in close relation to the tested resistant force in macromachining.

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How does the knowledge level affect the seismic retrofit cost? The case study of a RC building

  • Miano, Andrea;Chiumiento, Giovanni;Formisano, Antonio;Prota, Andrea
    • Structural Engineering and Mechanics
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    • 제82권5호
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    • pp.557-569
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    • 2022
  • The retrofit of existing structures in high seismic zones is a crucial issue in the earthquake engineering field. The interest of the research community is particularly high for the structures that do not respect current seismic codes and present structural deficiencies such as poor detailing and lack of capacity design provisions. A reinforced concrete (RC) school building is used as case study to show the influence of different knowledge levels on the seismic retrofitting cost assessment. The safety assessment of the case study building highlights deficiencies under both vertical and seismic loads. By considering all the possible knowledge levels defined by the Italian such as by the European codes in order to derive the mechanical properties of the school building constitutive materials, the retrofit operations are designed to achieve different seismic safety thresholds. The retrofit structural costs are calculated and summed up to the costs for in-situ in tests. The paper shows how for the case study building the major costs spent for a large number of in-situ tests allows to save a consistent amount of money for retrofit operations. The hypothesis of demolition and reconstruction of the building is also compared in terms of costs with all the analyzed retrofit options.

Intestinal Permeabilities of Polyethylene Glycols (330-1122D) in the In Situ Perfused Rat (장내 관류된 동물에서 Polyethylene Glycols에 의한 장내 투과율 (Intestinal Permeability)측정에 관한 연구)

  • 김미혜
    • Journal of Nutrition and Health
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    • 제29권2호
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    • pp.153-158
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    • 1996
  • Polyethylene glycols(PEGs)are hydrophilic molecules that have been used to characterize intestinal permeability via the paracellular pathway. Using a mixture of PEGs(400, 600 and 1000), containing oligomers in the molecular weight range 330 to 1122 D, the molecular weight permeability dependence in the jejunum of the rat small intestine was examined, employing an in situ recirculation perfusion technique. Individual oligomers were determined by HPLC with refractive detection. In the range studied, a distinct molecular weight cut-off was not apparent. Corrected for the length of jejunum used in the study, over the molecular weight range 330 to 1122D, the apparent permeability(Papp) of PEG ranged from 4.92$\pm$0.02$\times$10-5cm/sec(mean$\pm$SEM, n=5) to 0.28$\times$10-5cm/sec. Also, it was observed that the apparent permeability was inversely proportional to approximately MW2. The results in this study suggest that molecular weight is an important factor in determining the intestinal permeability.

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Shear-induced microstructure and rheology of cetylpyridinium chloride/sodium salicylate micellar solutions

  • Park, Dae-Geun;Kim, Won-Jong;Yang, Seung-Man
    • Korea-Australia Rheology Journal
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    • 제12권3_4호
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    • pp.143-149
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    • 2000
  • In this article, we considered shear-induced microstructure and rheological behavior of micellar solutions of cationic surfactant, cetylpyridinium chloride (CPC) in the presence of a structure-forming additive, sodium salicylate (NaSal). Shear viscosity, shear moduli and flow birefringence were measured as functions of the surfactant and additive concentrations. In the presence of NaSal, the micellar solution exhibited the non-linear rheological behavior due to the formation of supramolecular structures when the molar ratio of NaSal to CPC exceeded a certain threshold value. Flow birefringence probed the change in micelle alignment under shear flow. At low shear rates, the flow birefringence increased as the shear rate increased. On the other hand, fluctuation of flow birefringence appeared from the shear rate near the onset of shear thickening, which was caused by shear-induced coagulation or aggregation. These results were confirmed by the SEM images of in situ gelified micelle structure through sol-gel route.

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Gas Flow Rate Dependency of Etching Result: Use of VI Probe for Process Monitoring (가스 유량 변화에 따른 식각 공정 결과: VI Probe 활용 가능성 제안)

  • Song, Wan Soo;Hong, Sang Jeen
    • Journal of the Semiconductor & Display Technology
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    • 제20권3호
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    • pp.27-31
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    • 2021
  • VI probe, which is one of various in-situ plasma monitoring sensor, is frequently used for in-situ process monitoring in mass production environment. In this paper, we correlated the plasma etch results with VI probe data with the small amount of gas flow rate changes to propose usefulness of the VI probe in real-time process monitoring. Several different sized contact holes were employed for the etch experiment, and the etched profiles were measured by scanning electron microscope (SEM). Although the shape of etched hole did not show satisfactory relationship with VI probe data, the chamber status changed along the incremental/decremental modification of the amount of gas flow was successfully observed in terms of impedance monitoring.

열처리 조건에 따른 Rubrene 박막의 결정 특성 변화 연구

  • Yun, Yeong-Un;Kim, Song-Hui;Lee, Han-Ju;Kim, Tae-Dong;Lee, Gi-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 한국전기전자재료학회 2009년도 추계학술대회 논문집
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    • pp.124-124
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    • 2009
  • We observed the changes of crystal structure of Rubrene (5,6,11,12-tetraphenylnaphthacene) polycrystal thin films at various in situ substrate temperature and process by scanning electron microscope(SEM), x-ray diffraction (XRD) and near-field microwave microprobe (NFMM). Amorphous rubrene thin film was initially obtained on 200 nm thick $SiO_2/Si$ substrate at 35 $^{\circ}C$ in a vacuum evaporation but in situ long time postannealing at the temperature 80 $^{\circ}C$ transformed the amorphous phase into crystalline. Four heating conditions are followed : (a) preheating (b) annealing (c) preheating, annealing (d) preheating, cooling(35 $^{\circ}C$), annealing. We have obtained the largest polycrystal disk in sample (c). But the highest crytallity and conductivity of the rubrene thin films were obtained in sample (d).

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Surface Migration in Al and Cu Films (알루미늄 및 구리 박막에서의 표면전자이주)

  • 박종원;김윤태;이진호
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 한국전기전자재료학회 1994년도 추계학술대회 논문집
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    • pp.106-108
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    • 1994
  • Electromigration(EM) tests were carried out on Al and Cu films in HV systems to study surface migration. The Al films were made on oxidized silicon wafers by thermal evaporation, in-situ annealed at 300$^{\circ}C$, patterned, and EM tested at 260$^{\circ}C$ and 4.5MA/$\textrm{cm}^2$. SEM observation with back scattered electron mode on the EM tested Al films disclosed that thinning took place under the native Al oxide. In the case of Cu films, tested using in-situ TEM, thinning was also observed at the early stage of void formation even though the thinned areas were much less than those of the Al films.

Modelling and integrity assessment of shear connectors in precast cast-in-situ concrete bridges

  • Moyo, Pilate;Sibanda, Bongani;Beushausen, Hans
    • Structural Engineering and Mechanics
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    • 제42권1호
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    • pp.55-72
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    • 2012
  • Precast-cast insitu concrete bridge construction is widely practiced for small to medium span structures. These bridges consist of precast pre-stressed concrete beams of various cross-sections with a cast in-situ reinforced concrete slab. The connection between the beams and the slab is via shear links often included during the manufacturing process of the beams. This form of construction is attractive as it provides for standardisation, reduced formwork and construction time. The assessment of the integrity of shear connectors in existing bridges is a major challenge. A procedure for assessment of shear connectors based on vibration testing and finite element model updating is proposed. The technique is applied successfully to a scaled model bridge model and an existing bridge structure.