• Title/Summary/Keyword: hydrochloric acid

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Measurement of Cement Content on Concrete Using the Method of Hydrochloric Acid Melting Heat (염산용해열법을 이용한 콘크리트의 단위시멘트량 추정)

  • Kim, Sang-Min;Sin, Se-Jun;Hyun, Seung Yong;Kim, Jong;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.11a
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    • pp.102-103
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    • 2020
  • In this study, the effect of the change in the cement contents on the basic properties of the concrete and the estimation of the cement contents of hardened concretes using the hydrochloric acid melting heat. As a result of the study, as the cement contents increased, the fluidity and compressive strength increased, and there was no significant difference in the air contents and the unit volume mass. In addition, it showed a high correlation when compared with the estimated cement contents derived using the hydrochloric acid melting and the cement contents at the time of mixing. Therefore, it is considered that the hydrochloric acid melting is possible as a method of estimating the cement contents of concrete.

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Sulfuric acid and Hydrochloric acid resistance properties of Light Weight Matrix Based on Blast furnace slag (고로슬래그 기반 경량 경화체의 황산 및 염산 저항 특성)

  • Kim, Weon-Jeong;Lee, Seung-Ho;Park, Sun-Gyu;Lee, Sang-Soo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2015.11a
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    • pp.137-138
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    • 2015
  • The use of the cement and increased with the recent development of the construction industry. If the cement is the environmental problems caused by generating a large quantity of CO2 and the production process. Accordingly, this study is the test to determine the sulfuric acid and hydrochloric acid resistance properties of the Light weight matrix product of blast furnace slag-based light. A result, the compression strength of the sulfuric acid and hydrochloric acid immersion showed alower strength than the Plain.

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Characteristics of Surface Modified Activated Carbons Prepared by Potassium Salt Sequentially After Hydrochloric Acid Treatment

  • Oh, Won-Chun;Park, Chong-Sung;Bae, Jang-Soon;Ko, Young-Shin
    • Carbon letters
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    • v.7 no.1
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    • pp.34-41
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    • 2006
  • The objective of this paper is to compare the variation of surface properties by hydrochloric acid pre-treatment and of metallic potassium and their salts loading effect for activated carbon after surfaces transformation by acid. From the results of nitrogen adsorption, each isotherm shows a distinct knee band, which is closely related to the characteristic of microporous carbons with capillary condensation in micropores. In order to present the causes of the differences in surface properties and $S_{BET}$ after the samples were treated with hydrochloric acid, pore structure and surface morphology are investigated by adsorption analysis. X-ray diffraction (XRD) patterns indicate that activated carbons show better performance for metallic potassium and potassium salts by pre-treatment with hydrochloric acid. Scanning electron microscopy (SEM) pictures of potassium/activated carbon particles provide information about the homogeneous distribution of metal or metal complex on the surface. For the chemical composition microanalysis for potassium treatment of the activated carbon pre-treated with hydrochloric acid, samples were analyzed by energy disperse X-ray (EDX). Finally, the type and quality of oxygen groups are determined from the method proposed by Boehm. A positive influence of the acidic groups on the carbon surface by acid treatment is also demonstrated by an increase in the contents of potassium salts with increasing of acidic groups calculated from Boehm titration.

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A Study on Improvement of Recycling Process of Waste Fluorescent Lamps (폐형광등 재활용 공정의 개선 연구)

  • Lee, Gee Hun;Lee, Dong Hoon;Song, Young Jun;Kim, Chang Kwon
    • Resources Recycling
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    • v.29 no.3
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    • pp.61-74
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    • 2020
  • This study was conducted to improve the recycling process of waste fluorescent lamp, and investigate the possibility of using the waste fluorescent lamp glass as a raw material for glass beads, the leaching method of rare earth from the waste phosphor powder, and the possibility of solvent extraction of rare earth from the rare earth leaching solution. The waste phosphor contained 28.9% yttrium oxide, 3.46% cerium oxide, 1.95% europium oxide, 1.76% terbium oxide, and 1.43% lanthanum oxide. As a result of the trial production of glass beads using waste fluorescent lamp glass, it was judged that the production yield and quality were excellent, so that waste fluorescent lamp glass could be used as a raw material for glass beads. The soda roasted waste phosphor was leached in water and thereby the aqueous solution was blown with CO2 to drop the pH to about 7, Then, Al, Si and residual N2CO3 were dissolved, and NaAlCO3(OH)2 and SiO2 were precipitated in the aqueous solution. In the solvent extraction of cyanex272-hydrochloric acid, cyanex272-sulfuric acid, D2EHPA-hydrochloric acid, D2EHPA-sulfuric acid, Ionquest290-hydrochloric acid, Ionquest290-sulfuric acid, p507-hydrochloric acid using xylene as a diluent, the extraction yield of Y, Eu, Ce, La, and Tb are close to 100%. However, in this conditions, the difference in extraction yield for each element, that is, selectivity is 16% or less.

A Study on the Effect of Damages on the Conditions of Dike in the Leakage of Hydrochloric Acid Storage Tank (염산 저장탱크 누출 시 방류벽 조건에 따른 피해영향 연구)

  • Kang, Jungchun;Kim, Seungha;Kim, KyuHwan;Kim, YeonSoo;Kwon, Donguk
    • Korean Journal of Hazardous Materials
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    • v.6 no.2
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    • pp.7-12
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    • 2018
  • Hydrochloric acid is a highly corrosive toxic substance and requires proper safety to minimize damage in case of leakage. Among the various risk-reduction facilities, the dike is a typical safety facility installed to protect the surrounding buildings and facilities by preventing the external spread of hazardous materials from the storage tank. In this study, the KORA program was used to assume leakage accident of hydrochloric acid storage tank. At this time, the extent of the damage effects of ERPG-2 were assessed for each of the three separation distance between the storage tank and the dike. The study found that the smaller the separation distance between the dike and the storage tank, the smaller the extent of damage caused by hydrochloric acid leakage, and the greater the impact of indoor conditions under the same conditions. Through this process, we are going to assist in selecting locations and installing facilities for new and existing businesses.

Hydrolysis of Silk Fibroin with Boiling Water, Hydrochloric Acid, and Sodium Hydroxide -On the Quantitative Change in Terminal Amino Group Content- (견피브로인의 비등수 염산 및 수산화나트륨에 의한 가수분해 -말단아미노기의 정양적변화를 중심으로-)

  • Park Chan Hun;Dho Seong Kook
    • Journal of the Korean Society of Clothing and Textiles
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    • v.11 no.1
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    • pp.63-69
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    • 1987
  • Silk fibroin is likely to be hydrolyzed by acids or alkalies at high temperature, and the degree of the hydrolysis has been inferred from the changes in tensile strength and elongation. But, in this experiment, it was intended to infer that from the quantitative changes in terminal aminp group content as well as in tensile strength and elongation. Silk yarn was treated with boiling water, hydrochloric acid, and sodium hydroxide under various conditions. The boiling water somewhat degraded silk fibroin. Silk yarn treated with sodium hydroxide contained more terminal amino group than that treated with hydrochloric acid. This result agreed fairly well with the loss in weight, tensile strength, and elongation: the terminal amino group content increased with the decrease of tensile strength, elongation, and weight. The damage by sodium hydroxide to the silk fibroin was greater than that by hydrochloric acid.

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The Effect of pH on the Ettringite Formation (Ettringite의 생성에 미치는 pH의 영향)

  • 이의학;정찬일;송명신;이경희
    • Journal of the Korean Ceramic Society
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    • v.39 no.7
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    • pp.699-703
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    • 2002
  • In order to see the effect of pH on the formation of ettringite, pH was controlled with addition of boric acid, hydrochloric acid, nitric acid and potassium hydroxide during the formation of ettringite. The behavior of ettringite formation was discussed with XRD, SEM analysis. The result was that ettringite was unstablely formed with stabilization of aluminate gel and gypsum at below PH 10.

Effects of Adulterants in HCl on Artificial Hatching in the Silkworm Eggs (염산의 협잡물이 잠종의 인공부화에 미치는 영향)

  • 김윤식;김락상
    • Journal of Sericultural and Entomological Science
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    • v.17 no.1
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    • pp.35-39
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    • 1975
  • The acid treatment hatching method has been used practically for about 60 years and a number of investigators have studied about the artificial hatching for silkworm e99s, but the basic theory about the acid treatment hatching is not clarified yet. It is no exaggeration to say that the accidents of non hatching is continued ceaselessly in the silkworm egg by hydrochloric acid treatment. It is believed that the accident is due to the adulterants in HCl lather than inattention of acid treatment. Therefore, the authors mixed hydrochloric acid (analytical grade) with or added it to chemical ingredients which are possible to be included in the process of hydrochloric acid production, and treated it to summer and fall silkworm egg. The metalic adulterants such as iron, mercury, lead and arsenic are appeared not to be worried, but damage of SO$_3$ and free chlorine is seemed to lie considerable. Therefore, before acid treatment for hatching hydrochloric acid was warmed to 50$^{\circ}C$ with shaking to evaporate several injurious gases, by whick the damage due to use of hydrochloric acid for acid treatment hatching is prevented considerably. In conclusion, it is recommended to pretest bioassay with every HCl samples before artificial hatching of silkworm egg.

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Analytical method of trace elements in ceramic capacitor materials (세라믹 축전물질들의 미량성분 분석방법)

  • Choi, J.K.;Kim, T.H.;Lim, H.B.
    • Analytical Science and Technology
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    • v.10 no.1
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    • pp.35-42
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    • 1997
  • The sample pretreatment technique using a high pressure acid digestion bomb for the analysis of ceramic capacitor materials, such as barium titanate and PZT, was studied. When the concentrations of hydrochloric acid were varied with the addition of nitric acid or distilled water, quantitative measurements for those samples were carried out using inductively coupled plasma atomic emission spectrometry. From this experiment the results indicate that most of elements, such as Ba, Mn, Zn, Si, etc., aren't affected by the concentration of hydrochloric acid but Nb and Zr are very susceptable to it. It however turns out that the digestion time relatively gave little effects on the analytical result. In case of Nb the ratio of hydrochloric acid to water should be greater than 3:1(v / v) for the best analytical result. For the Pb determination use of diluted hydrochloric acid compared to the mixture of nitric acid and hydrochloric acid showed a better analytical result.

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Vital Wheat Gluten by Hot Air Drying (Vital Wheat Gluten 의 제조)

  • Suh, Hong-Kyl
    • Korean Journal of Food Science and Technology
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    • v.5 no.1
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    • pp.1-5
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    • 1973
  • Dry vital wheat gluten was prepared by atmospheric hot air drying of wet gluten blended with salt and acid. Products of good quality were obtained over a wide range of conditions, as shown by dough expansion, nitrogen solubility, rehydration test, and easinass of smashing and drying after blending. Gluten of good quality was produced by atmospheric hot air drying at $60^{\circ}C$, after blending wet gluten with salt in the range of 5 to 10% and acid, preferably, hydrochloric, at 0.12%.

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