• Title/Summary/Keyword: high temperature high pressure

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Effects of High Hydrostatic Pressure and Gamma Irradiation on Quality and Microbiological Changes of Kochujang-Gulbi. (고추장굴비의 품질과 저장성에 미치는 초고압처리와 감마선 조사 효과)

  • Kang, Seong-Gook;Park, Nan-Hee;Ko, Do-Ock;Li, Jing-Lei;Kim, Bo-Sub;Park, Yang-Kyun
    • Food Science and Preservation
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    • v.18 no.1
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    • pp.1-6
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    • 2011
  • Kochujang-gulbi, a Korean traditional food, was prepared with kochujang and freeze-dried gulbi slices. Kochujang-gulbi was treated with high hydrostatic pressure (200, 400 and 600 MPa) and gamma-irradiation (7, 10, 20 and 30 KGy) to improve its quality and shelf-life. The pH of high hydrostatic pressure and gamma-irradiation treated kochujang-gulbi samples did not significantly different compared to that of control. However, Hunter L value slightly increased, and Hunter a and b values decreased by high hydrostatic pressure and gamma-irradiation treatment. During storage, the pH and color of high hydrostatic pressure and gamma-irradiation treated kochujang-gulbi samples did not significantly changed. The VBN and TBA level decreased by the increase treatment of high hydrostatic pressure and then slowely increased during storage. The VBN and TBA level of kochujang-gulbi samples treated by the strong gamma ray emission slowely increased during storage. In particular, gamma-irradiation treatment was very effective to sterilize microorganisms when compared to that of high hydrostatic pressure in kochujang-gulbi products. In addition, the high hydrostatic pressure and gamma-irradiation treated kochujang-gulbi samples shown significantly lower total viable cell number than control for the 20 days of storage at room temperature with retort pouch packaging.

High-Temperature Corrosion Behavior of 316 L Stainless Steel in Carbon Dioxide Environment (고온 이산화탄소 분위기에서 316 L 스테인리스강의 부식 거동)

  • Chae, Hobyung;Seo, Sukho;Jung, Yong Chan;Lee, Soo Yeol
    • Korean Journal of Materials Research
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    • v.27 no.10
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    • pp.552-556
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    • 2017
  • Evaluation of the durability and stability of materials used in power plants is of great importance because parts or components for turbines, heat exchangers and compressors are often exposed to extreme environments such as high temperature and pressure. In this work, high-temperature corrosion behavior of 316 L stainless steel in a carbon dioxide environment was studied to examine the applicability of a material for a supercritical carbon dioxide Brayton cycle as the next generation power plant system. The specimens were exposed in a high-purity carbon dioxide environment at temperatures ranging from 500 to $800^{\circ}C$ during 1000 hours. The features of the corroded products were examined by optical microscope and scanning electron microscope, and the chemical compound was determined by x-ray photoelectron spectroscopy. The results show that while the 316 L stainless steel had good corrosion resistance in the range of $500-700^{\circ}C$ in the carbon dioxide environment, the corrosion resistance at $800^{\circ}C$ was very poor due to chipping the corroded products off, which resulted in a considerable loss in weight.

Hydrogen Effect on the Oxidation of Zr-Alloy Claddings under High Temperature (수소화물에 의한 Zr 합금의 고온산화 가속효과)

  • Jung, Yunmock;Ha, Sungwoo;Park, Kwangheon
    • Journal of Surface Science and Engineering
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    • v.49 no.4
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    • pp.389-394
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    • 2016
  • The operation method of nuclear power plants is currently changing to high burn-up and long period that can enhance economics and efficiency of the plant. Since nuclear plant operation environment has been becoming severe, the amount of absorbed hydrogen also has increased. Absorbed hydrogen can be fatal securing safety of nuclear fuel cladding in case of Loss of Coolant Accidents(LOCA). In order to examine the impact of hydride on high-temperature oxidation, high-temperature oxidation experiment was performed on normal Zry-4 cladding and on Zry-4 cladding where hydrogen is charged in air pressure steam atmosphere under the $950^{\circ}C$ and $1000^{\circ}C$. According to the results, while oxidation acceleration due to charged hydrogen was not observed prior to breakaway oxidation creation, oxidation began to accelerate in cladding where hydrogens charged as soon as the breakaway oxidation started. If so much hydrogen are charged in the cladding, equiaxial monoclinic phase to unstable of stress is formed and it is presumed that oxidation is accelerated because nearby stress caused a crack in equiaxial phase, and that makes corrosion resistance decline sharply.

A Study of Bulk Modulus of Beryl Using Water as a Pressure-Transmitting Medium (물을 압력 매개체로 이용한 녹주석의 체적탄성률 연구)

  • Hwang, Gil Chan;Kim, Hyunho;Lee, Yongjae
    • Journal of the Mineralogical Society of Korea
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    • v.30 no.3
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    • pp.83-91
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    • 2017
  • In-situ high-pressure and ex-situ high temperature-pressure experiments of natural beryl ($Be_3Al_2Si_6O_{18}$, P6/mcc) from two different localities (beryl-A and beryl-B) were studied using pure water as pressure transmitting medium. Compared to the previous study using a mixture of methanol:ethanol medium in 4 : 1 by volume, pressure- and temperature-induced chemical and structural changes under water medium are expected to be different. The derived bulk moduli are 111(7) GPa, $K{_0}^{\prime}=73(7)$; 110(9) GPa, $K{_0}^{\prime}=65(8)$ for beryl-A and beryl-B, respectively. We observe densifications in volume compression, which appear to be attributed to the phase transitions of water to ICE VI and ICE VII around 1.0 GPa and 2.5 GPa, respectively.

Effects of Sputtering Pressure on the Properties of BaTiO3 Films for High Energy Density Capacitors

  • Park, Sangshik
    • Korean Journal of Materials Research
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    • v.24 no.4
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    • pp.207-213
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    • 2014
  • Flexible $BaTiO_3$ films as dielectric materials for high energy density capacitors were deposited on polyethylene terephthalate (PET) substrates by r.f. magnetron sputtering. The growth behavior, microstructure and electrical properties of the flexible $BaTiO_3$ films were dependent on the sputtering pressure during sputtering. The RMS roughness and crystallite size of the $BaTiO_3$ increased with increasing sputtering pressure. All $BaTiO_3$ films had an amorphous structure, regardless of the sputtering pressures, due to the low PET substrate temperature. The composition of films showed an atomic ratio (Ba:Ti:O) of 0.9:1.1:3. The electrical properties of the $BaTiO_3$ films were affected by the microstructure and roughness. The $BaTiO_3$ films prepared at 100 mTorr exhibited a dielectric constant of ~80 at 1 kHz and a leakage current of $10^{-8}A$ at 400 kV/cm. Also, films showed polarization of $8{\mu}C/cm^2$ at 100 kV/cm and remnant polarization ($P_r$) of $2{\mu}C/cm^2$. This suggests that sputter deposited flexible $BaTiO_3$ films are a promising dielectric that can be used in high energy density capacitors owing to their high dielectric constant, low leakage current and stable preparation by sputtering.

Fabrication and Property Evaluation of Cu-Mn Compacts for Sputtering Target Application by a Pulsed Current Activated Sintering Method (펄스전류활성소결법을 이용한 스퍼터링 타겟용 Cu-Mn 소결체 제조 및 특성평가)

  • Jang, Jun-Ho;Oh, Ik-Hyun;Lim, Jae-Won;Park, Hyun-Kuk
    • Journal of Powder Materials
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    • v.23 no.1
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    • pp.1-7
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    • 2016
  • Cu-Mn compacts are fabricated by the pulsed current activated sintering method (PCAS) for sputtering target application. For fabricating the compacts, optimized sintering conditions such as the temperature, pulse ratio, pressure, and heating rate are controlled during the sintering process. The final sintering temperature and heating rate required to fabricate the target materials having high density are $700^{\circ}C$ and $80^{\circ}C/min$, respectively. The heating directly progresses up to $700^{\circ}C$ with a 3 min holding time. The sputtering target materials having high relative density of 100% are fabricated by employing a uniaxial pressure of 60 MPa and a sintering temperature of $700^{\circ}C$ without any significant change in the grain size. Also, the shrinkage displacement of the Cu-Mn target materials considerably increases with an increase in the pressure at sintering temperatures up to $700^{\circ}C$.

Combustion Characteristics of High Pressure Gas Generator for Liquid Rocket Engine (액체로켓엔진용 가스발생기의 고압연소특성)

  • Han Yeoung-Min;Lee Kwang-Jin;Moon Il-Yoon;Seo Seong-Hyeon;Choi Hwan-Seok;Lee Soo-Yong
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2005.11a
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    • pp.341-345
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    • 2005
  • This paper is for the combustion characteristics of gas generator which drive 1.5MW-class turbo pump and runs in fuel-rich combustion regime with LOx/kerosene as propellant. The outline of development procedure of real scale high pressure gas generator is introduced and the relation between O/F ratio and outlet temperature and the molecular weight and specific heat ratio of combustion gas are described. The relation between O/F ratio and temperature is newly obtained at higher pressure and the molecular weight and specific heat ratio is modified and their validity is confirmed by the mass relation equation.

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Effects of Temperature, Pressure, and Gas Residence Time on Methane Combustion Characteristics of Oxygen Carrier Particle in a Pressurized Fluidized Bed Reactor (가압 유동층 반응기에서 산소공여입자의 메탄 연소 특성에 미치는 온도, 압력 및 기체체류시간의 영향)

  • Ryu, Ho-Jung;Park, Sang-Soo;Moon, Jong-Ho;Choi, Won-Kil;Rhee, Young-Woo
    • Journal of Hydrogen and New Energy
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    • v.23 no.2
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    • pp.173-182
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    • 2012
  • Effects of temperature, pressure, and gas residence time on methane combustion characteristics of mass produced oxygen carrier particle (OCN706-1100) were investigated in a pressurized fluidized bed reactor using methane and air as reactants for reduction and oxidation, respectively. The oxygen carrier showed high fuel conversion, high $CO_2$ selectivity, and low CO concentration at reduction condition and very low NO emission at oxidation condition. Moreover OCN706-1100 particle showed good regeneration ability during successive reduction-oxidation cyclic tests up to the 10th cycle. Fuel conversion and $CO_2$ selectivity decreased and CO emission increased as temperature increased. These results can be explained by trend of calculated equilibrium CO concentration. However, $CO_2$ selectivity increased as pressure increased and fuel conversion increased as gas residence time increased.

An Experimental Study on Flow and Heat / Mass Transfer Characteristics of $LiBr-H_2O$ Solution Flowing over a Cooled Horizontal Tube (수평 냉각관 외부를 흘러내리는 $LiBr-H_2O$ 수용액의 유동 및 열/물질 전달 특성에 관한 실험적 연구)

  • Seal, Sin-Su;Lee, Sang-Yang
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.8
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    • pp.1085-1096
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    • 2000
  • An experimental study was performed to examine the heat and mass transfer characteristics of $LiBr-H_2O$ solution flowing over a single horizontal tube with the water vapor absorption. Effects of the flow rate and the temperature of the solution at the top of the tube, the absorber pressure and the drainage pattern were considered. The absorption rate depends highly on the absorber pressure at the low flow rate condition while on the solution inlet temperature at the high flow rate condition. Also, when the flow rate is low, the absorption performance with the sheet flow drainage appeared to be higher than that with the dripping/jet drainage. However, at the high flow rate condition, the case became reversed. The liquid film became wavy with the higher absorption rate. The waves were more probable to form with the lower flow rate and temperature of the solution, and with the higher absorber pressure.

Optimization of Electrical and Optical Properties of a-IZO Thin Film for High-Efficiency Solar Cells (고효율 태양전지용 a-IZO 박막의 전기적 및 광학적 특성 최적화에 관한 연구 )

  • Somin Park;Sungjin Jeong;Jiwon Choi;Youngkuk Kim;Junsin Yi
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.36 no.1
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    • pp.49-55
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    • 2023
  • The deposition of indium zinc oxide (IZO) thin films was carried out on substrate at room temperature by RF magnetron sputtering. The effects of substrate temperature, RF power and deposition pressure were investigated with respect to physical and optical properties of films such as deposition rate, electrical properties, structure, and transmittance. As the RF power increases, the resistivity gradually decreases, and the transmittance slightly decreases. For the variation of deposition pressure, the resistivity greatly increases, and the transmittance is decreased with increasing deposition pressure. As a result, it was demonstrated that an IZO film with the resistivity of 3.89 × 10-4 Ω∙cm, the hole mobility of 51.28 cm2/Vs, and the light transmittance of 86.89% in the visible spectrum at room temperature can be prepared without post-deposition annealing.