• Title/Summary/Keyword: high temperature high pressure

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Analyses of Densification and Consolidation of Copper Powders during High-Pressure Torsion Process Using Finite Element Method (유한요소해석을 이용한 고압비틀림 공정 중의 구리 분말의 치밀화 및 고형화 거동 분석)

  • Lee, Dong Jun;Yoon, Eun Yoo
    • Journal of Powder Materials
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    • v.22 no.1
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    • pp.6-9
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    • 2015
  • In this study, the behavior of densification of copper powders during high-pressure torsion (HPT) at room temperature is investigated using the finite element method. The simulation results show that the center of the workpiece is the first to reach the true density of copper during the compressive stage because the pressure is higher at the center than the periphery. Subsequently, whole workpiece reaches true density after compression due to the high pressure. In addition, the effective strain is increased along the radius during torsional stage. After one rotation, the periphery shows that the effective strain is increased up to 25, which is extensive deformation. These high pressure and severe strain do not only play a key role in consolidation of copper powders but also make the matrix harder by grain refinement.

Effect of Sputtering Working Pressure on the Optical and Electrical Properties of InZnO Thin-Film Transistors (스퍼터링 공정 압력이 InZnO 박막트랜지스터의 광학 및 전기적 특성에 미치는 영향)

  • Park, Ji-Min;Kim, Hyoung-Do;Jang, Seong Cheol;Kim, Hyun-Suk
    • Korean Journal of Materials Research
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    • v.30 no.4
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    • pp.211-216
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    • 2020
  • Amorphous In-Ga-Zn-O (a-IGZO) thin film transistors, because of their relatively low mobility, have limits in attempts to fulfill high-end specifications for display backplanes. In-Zn-O (IZO) is a promising semiconductor material for high mobility device applications with excellent transparency to visible light region and low temperature process capability. In this paper, the effects of working pressure on the physical and electrical properties of IZO films and thin film transistors are investigated. The working pressure is modulated from 2 mTorr to 5 mTorr, whereas the other process conditions are fixed. As the working pressure increases, the extracted optical band gap of IZO films gradually decreases. Absorption coefficient spectra indicate that subgap states increase at high working pressure. Furthermore, IZO film fabricated at low working pressure shows smoother surface morphology. As a result, IZO thin film transistors with optimum conditions exhibit excellent switching characteristics with high mobility (≥ 30㎠/Vs) and large on/off ratio.

Vaporization of Hydrocarbon Fuel Droplet in High Pressure Environments (고압 환경하에서 탄화수소 연료 액적의 기화특성 연구)

  • Kim, Sung-Yup;Yoon, Woong-Sup
    • Proceedings of the KSME Conference
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    • 2003.11a
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    • pp.127-132
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    • 2003
  • A study of high-pressure n-heptane droplet vaporization is conducted with emphasis placed on equilibrium at vapor-liquid interface. General frame of previous rigorous model[1] is retained but tailored for flash equilibrium calculation of vapor-liquid interfacial thermodynamics. The model is based on complete time-dependent conservation equations with a full account of variable properties and vapor-liquid interfacial thermodynamics. The influences of high-pressure phenomena, including ambient gas solubility, thermodynamic non-ideality, and property variation on the droplet evaporation are investigated. The governing equations and associated moving interfacial boundary conditions are solved numerically using a implicit scheme with the preconditioning method and the dual time integration technique. And a parametric study of entire droplet vaporization history as a function of ambient pressure, temperature has been conducted. Some computational results are compared with Sato's experimental data for the validation of calculations. For low ambient temperatures, the droplet lifetime first increases with pressures, then decreases for high pressures. For higher ambient temperatures, the droplet lifetime increase with less amplitude than that of low ambient temperatures, which then decreases with more amplitude than that of low temperatures. The solubility of nitrogen can not be neglected in the high pressure and it becomes higher as the pressure goes up.

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Frictional Characteristics of Silicon Graphite Lubricated with Water at High Pressure and High Temperature (고온 고압에서 물로 윤활되는 실리콘그라파이트 재질의 마찰 특성에 관한 연구)

  • Lee, Jae-Seon;Kim, Eun-Hyun;Park, Jin-Seok;Kim, Jong-In
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.151-156
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    • 2001
  • Experimental frictional and wear characteristics of silicon graphite materials is studied in this paper. Those specimens are lubricated with high temperature and highly pressurized water to simulate the same operating condition for the journal bearing and the thrust bearing on the main coolant pump bearing in the newly developing nuclear reactor named SMART(System-integrated Modular Advanced ReacTor). Operating condition of the bearings is realized by the tribometer and the autoclave. Friction coefficient and wear loss are analyzed to choose the best silicon graphite material. Pin on plate test specimens are used and coned disk springs are used to control the applied force on the specimens. Wear loss ana wear width are measured by a precision balance and a micrometer. The friction force is measured by the strain gauge which can be used under high temperature and high pressure. Three kinds of silicon graphite materials are examined and compared with each other, and each material shows similar but different results on frictional and wear characteristics.

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Realization of silver fixed-point and application for the high temperature platinum resistance thermometry using the gas-pressure controlled sodium heat-pipe furnace (가스압력조절식 나트륨 열관전기로를 이용한 은 고정점 실현과 고온백금저항온도 계측에의 응용)

  • Gam, K.S.;Choi, I.M.;Yang, I.;Kim, Y.G.
    • Journal of Sensor Science and Technology
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    • v.18 no.2
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    • pp.116-121
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    • 2009
  • Pressure-controlled sodium heat pipe furnace was designed and fabricated, and its characteristics was investigated. Pressure control system was controlled within ${\pm}0.5\;Pa$ at 150 kPa and the stability of pressure was decreased to ${\pm}2.5\;Pa$, when the pressure-controlled system connected with the heat pipe. The melting curve of Ag fixed-point realized well by the adiabatic method using the pressure-controlled sodium heat pipe furnace and its accuracy showed ${\pm}2.27\;mK$ from the calculation of 20% to 80% at the plateau. The freezing curve of Ag fixed-point also realized and its plateau value was 2.23 mK lower than that of the melting curve.

An Experimental Study on the Performance of Brazed Plater Heat Exchangers (용접형 판형열교환기 성능측정에 관한 실험적 연구)

  • Park, Hyun-Min;Park, Chang Yong
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.3_1spc
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    • pp.551-557
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    • 2013
  • The heat transfer performance and pressure drop characteristics of brazed-plate heat exchangers with 20 and 30 plates were experimentally measured and analyzed in this study. The mass flow rates of the heat exchangers with 20 and 30 plates were fixed at 0.6 and 0.9 kg/s for the low temperature side, respectively. The mass flow rate for the high temperature side was controlled from 0.2 kg/s to 1.2 kg/s. The inlet temperatures for the high and low temperature sides were $10^{\circ}C$ and $7^{\circ}C$, respectively. The heat transfer characteristics were not influenced by the number of plates. The pressure drop at the heat exchanger with 30 plates was slightly higher than that with 20 plates. The values calculated from the correlations based on gasket plate heat exchangers were compared with the experimental results. It was found that the predicted Nusselt numbers for the gasket plate heat exchangers were about 5% to 20% lower than the measured Nusselt numbers for the brazed plate heat exchangers. However, a pressure drop comparison showed that the calculated pressure drops at the gasket plate heat exchangers were less than half of the measured pressure drops at the brazed plate heat exchangers.

Properties of TiO2 Thin Films Deposited on PET Substrate for High Energy Density Capacitor (고에너지밀도 캐패시터를 위해 PET 기판에 증착한 TiO2 박막의 특성)

  • Park, Sang-Shik
    • Korean Journal of Materials Research
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    • v.22 no.8
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    • pp.409-415
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    • 2012
  • $TiO_2$ thin films for high energy density capacitors were prepared by r.f. magnetron sputtering at room temperature. Flexible PET (Polyethylene terephtalate) substrate was used to maintain the structure of the commercial film capacitors. The effects of deposition pressure on the crystallization and electrical properties of $TiO_2$ films were investigated. The crystal structure of $TiO_2$ films deposited on PET substrate at room temperature was unrelated to deposition pressure and showed an amorphous structure unlike that of films on Si substrate. The grain size and surface roughness of films decreased with increasing deposition pressure due to the difference of mean free path. X-ray photoelectron spectroscopy (XPS) analysis revealed the formation of chemically stable $TiO_2$ films. The dielectric constant of $TiO_2$ films was significantly changed with deposition pressure. $TiO_2$ films deposited at low pressure showed high dissipation factor due to the surface microstructure. The dielectric constant and dissipation factor of films deposited at 70 mTorr were found to be 100~120 and 0.83 at 1 kHz, respectively. The temperature dependence of the capacitance of $TiO_2$ films showed the properties of class I ceramic capacitors. $TiO_2$ films deposited at 10~30 mTorr showed dielectric breakdown at applied voltage of 7 V. However, the films of 500~300 nm thickness deposited at 50 and 70 mTorr showed a leakage current of ${\sim}10^{-8}{\sim}10^{-9}$ A at 100 V.

Ultrafine Grained Bulk Al Matrix Carbon Nanotube Composites Processed by High Pressure Torsion (고압비틀림 성형 공정에 의한 Al 기지 CNT 복합재료의 초미세결정 벌크화)

  • Joo,, S.H.;Kim, H.S.
    • Transactions of Materials Processing
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    • v.19 no.7
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    • pp.423-428
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    • 2010
  • Carbon nanotubes(CNTs) are expected to be ideal reinforcements of metal matrix composite materials used in aircraft and sports industries due to their high strength and low density. In this study, a high pressure torsion(HPT) process at an elevated temperature(473K) was employed to achieve both powder consolidation and grain refinement of aluminummatrix nanocomposites reinforced by 5vol% CNTs. CNT/Al nanocomposite powders were fabricated using a novel molecular-level mixing process to enhance the interface bonding between the CNTs and metal matrix before the HPT process. The HPT processed disks were composed of mostly equilibrium grain boundaries. The CNT-reinforced ultrafine grained microstructural features resulted in high strength and good ductility.