• Journal of Food Hygiene and Safety
• /
• v.26 no.1
• /
• pp.36-42
• /
• 2011

In order to optimize the supercritical fluid extraction (SFE) conditions of ginger oleoresin (GO), we conducted an evaluation of quality properties such as yield (%), color, volatile flavor compounds and gingerol components. The extraction yield gained by SFE increased as extraction pressure and temperature increased. The highest yield was $8.96{\pm}0.68%$ at 500 bar $65^{\circ}C$ extraction condition. The total color difference (${\Delta}E$) values decreased at high pressure. In case of the 100 bar pressure conditions, ${\Delta}E$-values increased as the temperature went up. The analysis of the 6-gingerol, 8-gingerol, 10-gingerol, 6-shogaol and curcumin contents decreased at high temperature conditions of identical pressure and increased at high pressure conditions. The volatile flavor compounds were detected in zingiberene, ${\beta}$-sesquiphellandre, ${\beta}$-phellandre, ${\alpha}{\gamma}$-curcumene, 2,3-butandiol, ${\beta}$-bisabolene and so on. Also volatile component contents showed difference in each of extraction conditions.

• Economic and Environmental Geology
• /
• v.56 no.1
• /
• pp.13-21
• /
• 2023

X-ray powder diffraction study was conducted on the bulk modulus and phase transition behavior of synthetic zeolite X under high temperature and high pressure. Water and HCO₃^- solution were used as a PTM. Sample was heated and pressurized up to 250 ℃ and 5.18 GPa. The change of unit cell volume and phase transition were observed by X-ray diffraction. The lattice constants and unit cell volume of zeolite X, gmelinite, natrolite, and smectite were calculated using the GSAS2 program to which Le Bail's whole powder pattern decomposition (WPPD) method was applied. The bulk modulus of each zeolite X and smectite were calculated using the EosFit program to which the Birch-Murnaghan equation was applied. The bulk modulus of zeolite X is 89(3) GPa in water run, and zeolite X is 92(3) GPa in HCO₃^- solution run. In both run, pressure induced hydration (PIH) occurred due to the inflow of PTM into the zeolite X framework at initial pressure. Zeolite X transited to gmelinite, natrolite, and smectite in water run. Zeolite X, however, transited to smectite in HCO₃^- solution run. Interzeolite transformation occurred in water run, and did not occur in HCO₃^- solution run, which is assumed that conflict between the environment to form zeolite and the pH of the HCO₃^- solution.

• International Journal of Automotive Technology
• /
• v.5 no.3
• /
• pp.155-164
• /
• 2004

The direct injection gasoline spray-wall interaction was characterized inside a heated pressurized chamber using various visualization techniques, including high-speed laser-sheet macroscopic and microscopic movies up to 25,000 frames per second, shadowgraph, and double-spark particle image velocimetry. Two hollow cone high-pressure swirl injectors having different cone angles were used to inject gasoline onto a heated plate at two different impingement angles. Based on the visualization results, the overall transient spray impingement structure, fuel film formation, and preliminary droplet size and velocity were analyzed. The results show that upward spray vortex inside the spray is more obvious at elevated temperature condition, particularly for the wide-cone-angle injector, due to the vaporization of small droplets and decreased air density. Film build-up on the surface is clearly observed at both ambient and elevated temperature, especially for narrow cone spray. Vapor phase appears at both ambient and elevated temperature conditions, particularly in the toroidal vortex and impingement plume. More rapid impingement and faster horizontal spread after impingement are observed for elevated temperature conditions. Droplet rebounding and film break-up are clearly observed. Post-impingement droplets are significantly smaller than pre-impingement droplets with a more horizontal velocity component regardless of the wall temperature and impingement angle condition.

• Proceedings of the KSME Conference
• /
• 2003.11a
• /
• pp.314-319
• /
• 2003

The concept of lean-premixed combustion in gas turbine combustor operation has become a standard in recent years as an effective means to meet stringent enviromental standards on NOx emissions. The combustion characteristics of 75 kW class lean premixed combustor were investigated at the conditions of high temperature and ambient pressure. The exit temperature and emissions of CO and NOx were measured at the center of exit plane. The high temperature air of $550K{\sim}650K$ was supplied through air preheater. As expected, experimental results indicate that NOx emission was increased and CO emission was decreased by increasing inlet air temperature. But CO emission measured at the center of exit plane was increased because of the non-uniform radial direction profiles. The Semi-Empirical Correlation method was applied to obtain the design point emissions of NOx and CO. Also the flame temperature, CO and NOx emissions were measured along the centerline of liner at 650K inlet air temperature to determine the position of dilution holes.

• Journal of the Korean Society for Precision Engineering
• /
• v.16 no.8
• /
• pp.46-52
• /
• 1999

Large valves for steam turbines of fossil power plants are exposed to a severe mechanical and thermal loading resulting from steam with high pressure and high temperature. Valve casings are designed to withstand such a loading. During the operation of a plant, temperatures at inner and outer surface of the casings are measured and steam flow is controlled so that the measured difference is lower than the maximum allowable value determined in the design stage. In this paper, a method is presented to calculate the maximum allowable temperature difference at the inner and outer surface of valve casings for steam turbines of fossil power plants. The finite element method is used to analyze distribution of temperature and stresses of a casing under the operating condition. Low cycle fatigue and creep rupture are taken into consideration to determine the maximum allowable temperature difference. The method can be usefully applied in the design stage of the large valves for the steam turbines, contributing to safe and reliable operation of the fossil power plants.

• Proceedings of the Korean Society of Propulsion Engineers Conference
• /
• 2003.05a
• /
• pp.266-269
• /
• 2003

During liquid rocket engine combustion, the resulting combustion gas has flow characteristics of high temperature and high velocity. An experimental study was performed to obtain basic data for a flame deflector design that is endurable under such flow characteristics. While the injected-water cools down the combustion plume, temperature and pressure of the plume was measured. As the experiment is being performed, gas temperature was measured using infrared cameras, and the gas temperature data was compared with the temperature data from the sensor in the plume. With the results of this experiment, we were able to obtain applicable temperature data for flame deflector design and predict the performance and structural strength required for installation of water injector.

• Textile Coloration and Finishing
• /
• v.34 no.3
• /
• pp.197-206
• /
• 2022

The purpose of this study was to confirm the optimal spinning conditions for PLA (Polylactic acid) as a fiber forming polymer. According to the melt spinning test results of PLA, the optimal spinning temperature was 258℃. However, it needs to note that relatively high pack pressure was required for spinning at 258℃. At an elevated temperature, 262℃, mono filament was broken easily due to hydrolysis of PLA at a higher temperature. In case of fiber strength, it was confirmed that the draw ratios of 2.7 to 3.3 were optimal for maximum strength of melt spun PLA. Above the draw ratio, 3.3, the strength of the PLA fibers was lowered. It was presumed that cleavage of the PLA polymer chain over maximum elongation. The heat setting temperature of GR (Godet roller) showed that the maximum strength of the PLA fibers was revealed around 100℃. The degree of crystallinity and the strength of the PLA fibers were decreased above 100℃. The optimal take-up speed (Spinning speed) was around 4,000m/min. Thermal analysis of PLA showed 170℃ and 57℃ as Tm (melting temperature) and Tg (glass transition temperature), respectively.

• Journal of the Korean Society of Visualization
• /
• v.22 no.1
• /
• pp.79-84
• /
• 2024

As microchips' degree of integration is getting higher, its cooling problem becomes important more than ever. One of the promising methods is using fractal microchannel heat sink by mimicking nature's Murray networks. However, most of the related works have been progressed only by numerical analysis. Perhaps such lack of direct experimental studies is due to the technical difficulty of the temperature and heat flux measurement in complex geometric channels. Here, we demonstrate the direct visualization of in situ temperature profile in a fractal microchannel heat sink. By using the temperature-sensitive fluorescent dye and a transparent Polydimethylsiloxane window, we can map temperature profiles in silicon-based fractal heat sinks with various fractal scale factors (a=1.5-3.5). Then, heat transfer rates and pressure drops under a fixed flow rate were estimated to optimize hydrodynamic and thermal characteristics. Through this experiment, we found out that the optimal factor is a=1.75, given that the differences in heat transfer among the devices are marginal when compared to the variances in pumping power. This work is expected to contribute to the development of high-performance, high-efficiency thermal management systems required in various industrial fields.

• Journal of Hydrogen and New Energy
• /
• v.20 no.3
• /
• pp.256-263
• /
• 2009

The operating range of HCCI engine is narrow due to excessive rate of pressure rise on high load. The fuel stratification is proposed to solve the problem. The purpose of this study is to gain a better understanding of the effects of fuel stratification on reducing the pressure-rise rate at high load in HCCI combustion and to investigate that the operating range is expanded for fuel stratification in the preceding condition of initial temperature and equivalence ratios. The engine is fueled with Di-Methyl Ether (DME) which has unique 2-stage heat release. The computations were conducted using SENKIN application of the CHEMKINll kinetics rate code. Calculation result shows that proper fuel stratification prolongs combustion duration and reduce pressure rise rate.

• Journal of Korean Society for Atmospheric Environment
• /
• v.19 no.3
• /
• pp.297-306
• /
• 2003

Works were focused on back pressure characteristics of ceramic fiber filter on DPF (Diesel Particulate Filter) system and experiments were performed to select appropriate filter which can filter particulates. Filters were installed on metal -support tube which has openings for exhaust gas flow. Ceramic fiber filters with high specific surface area and adequate high temperature strength are commercially available for filtration of diesel particulates and in -situ hot regeneration. Thus, ceramic blanket and ceramic board which are used as insulating media were applied to filter and filtration apparatus was installed on exhaust gas line connected to 2.0 L diesel engine. Alternating filter structure to adapt DPF system, collection efficiency test of diesel particulates was measured. In case of ceramic blanket, pressure drop was low, caused by the destruction of soft structures. Also, particulate collection efficiency was decreased depending on loading time. In case of ceramic board, structure design was altered to reduce back pressure on DPF system. Structure design was altered to induce Z-flow by making 10 mm and 5 mm holes on the surface of media. Alteration of 5 mm hole showed that media have low back pressure but particulate collection efficiency was 77%, while 10 mm hole showed that of 90%.