• Title/Summary/Keyword: high temperature aging

Search Result 429, Processing Time 0.076 seconds

Effect of Cobalt Contents on the Biocompatibility and Corrosion Properties of Fe-31Cr-27Ni-1.6Mo-1.5W-0.26N Alloy (Fe-31Cr-27Ni-1.6Mo-1.5W-0.26N계 초내식성 스테인리스강의 생체적합성 및 부식특성에 미치는 Co함량의 영향)

  • Jang, Soon Geun;Yoo, Young Ran;Nam, Hee Soo;Shim, Gyu Tae;Kim, Jung Gu;Kim, Young Sik
    • Korean Journal of Metals and Materials
    • /
    • v.46 no.4
    • /
    • pp.209-216
    • /
    • 2008
  • Super austenitic stainless steels shows the high PRE (Pitting Resistance Equivalent) number and the good corrosion resistance. This work controlled the Co contents in Fe-31Cr-1.7Mo-27Ni-0.25N alloys to elucidate the effect of cobalt contents on the biocompatibility and corrosion resistance. Increasing Co contents, the hardness of the annealed alloys tends to be reduced. In aged alloys, cobalt decreased the increments of hardness by aging treatment. Cobalt decreased the critical pitting temperature (CPT) in 6% $FeCl_3$ + 1% HCl solution, but improved the anodic polarization behavior in Hanks' balanced salt solution and artificial saliva solution. Repassivation rate in artificial body solutions was improved by increasing cobalt contents, but didn't show the linear relationship to PRE number of the alloys. The experimental alloys showed the non-cytotoxicity because of its high corrosion resistance.

Adaptation of Feedlot Cattle to a High-energy Ration by Intraruminal Transplantation of Adapted Ruminal Fluid (제1위내용액 이식에 의한 비육우의 농후사료 적응법에 관한 연구)

  • 이현범;탁연빈;성은주;김기석;이영주;정재석;장종식;권오덕
    • Journal of Veterinary Clinics
    • /
    • v.15 no.1
    • /
    • pp.62-74
    • /
    • 1998
  • In feedlot cattle the abrupt change of diet from roughage to a large quantity of grain for the purpose to improve production often results in increased occurrence of rumen acidosis or acute carbohydrate encouragement enterotoxemia, bloats diarrhea liver abscess and laminitis or robot disease. The common management practice to control these problem is to increase the amount of concentrates in the diet in a stepwise manner until the animals are adapted to a high-grain ration. However this practice requires at least about 3 weeks adaptation period and specially prepared adaptation rations which contain various amount of concentrates. Present experiment was undertaken in order to findout the more simple and rapid adaptation method of cattle to a high grain ration. Nineteen Korean calves aging from four to six month were fed artifical hay (Youngchoun Chuk-Hyup, Korea) which contains 10% of concentrates or alfalfa and rye grass hays for two months and randomly alloted to three experimental groups and two control groups. The experimental group-1 was inoculated by stomach tube for two days with li500 ml/day of ruminal fluid fished from Korean beef cattle that had been previously adapted to a high-energy ration. The experimental group-2 was inoculated by trocalization for two days with the same ruminal fluid. The experimental group-3 was inoculated by trocalization with 1,500 ml/day of bacterial culture which contained 2$\times $10$^{9}$/m1 of Gram-negative bacteria derived from adapted luminal fluid. The two control groups were treated with normal saline solution by the same methods. All animals were fed high-energy ration that contained 80% of grain ad libitum for 30-74 days beginning on the third of the treatment. The effect of the inoculation on the adaptation was observed clinicopathologically with the following results; All of the experimental calves inoculated with the ruminal fluid or Gram-negative bacterial culture derived from adapted cattle did not show any signs of rumen acidosis or other related diseases, while most of the control calves did show diarrhea and bloat and a calf laminitis. The average daily weight gain and feed efficiency of experimental calves were slightly improved compared with control calves. Following the feeding of high-grain rational the pH of the ruminal fluid was lowered in both the experimental and control groups. However severe acidosis with the pH of below 5.0 was observed in only a control group-2. The protozoal number in ruminal fluid was markedly decreased during the high-grain feeding in both the experimental and control calves. However the decrease was mere severe in control calves compared with the experimental calves. The activation of the protozoa were completely disappeared within nine hours at the refrigerator temperature (4"C). No significant differences in heamatological and blood chemical values between the experimental and control calves were recognized. However in one control calf which showed clinically laminitis marked elevations of serum glutamic oxaloacetate transaminase and lactic dehydrogenase activities and a decrease of serum glucose level were observed. From these results it would be concluded the intraruminal transplantation of unadapted calves with the adapted ruminal fluid from cattle previously adapted to a high-energy ration prevents disease problem associated with high-grain feeding and improve weight gain and feed efficiency.ency.

  • PDF

Effects of Aging Temperature and Time on the Conversion of Garlic (Allium sativum L.) Components (온도 및 숙성기간이 마늘의 화학적 성분변화에 미치는 영향)

  • Cho, Kang-Jin;Cha, Ji-Young;Yim, Joo-Hyuk;Kim, Jae-Hyun
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.40 no.1
    • /
    • pp.84-88
    • /
    • 2011
  • Some thermally processed foods have higher biological activities due to their various chemical changes during heat treatment. Especially, 5-hydroxymethylfurfural (HMF) is derived from dehydration of sugars and has been identified in processed garlic. The biological function of HMF have revealed as antisickling agent and thyrosinase inhibitor. This study was carried out to examine the formation of HMF and free sugars from the aged garlics when it is treated at 60 and $75^{\circ}C$ and different incubation periods from 7 to 35 days. HMF and free sugars from the hot-water extracts of aged garlics were analyzed with GC/MS, LC/MS, and HPLC. The amount of HMF was higher than at $75^{\circ}C$ and increasing incubation period. Among free sugars, the only fructose except glucose and sucrose was formed and converted to HMF at high temperature and long incubation period. However, fructose formed in low temperature during making of aged garlic was rarely converted to HMF. This result indicates that formation of HMF can be dependent on the temperature and incubation period for making aged garlic.

Antioxidant activity of the Sumaeyaksuk tea extracts prepared with different drying and extract conditions (건조 및 침출 조건에 따른 섬애약쑥 침출물의 항산화활성)

  • Hwang, Cho-Rong;Seo, Weon-Taek;Jung, Min-Jung;Shin, Jung-Hye
    • Food Science and Preservation
    • /
    • v.20 no.4
    • /
    • pp.546-553
    • /
    • 2013
  • In this study, we examined the antioxidant activity of the Sumaeyaksuk (Artemisia argyi) tea extracts from different pre-treatment and extraction methods. Sumaeyaksuk was sun-dried for 3.5 days (control, RC) and aged at a temperature of $60^{\circ}C$ for 3.5 days (HA), 7 days (HB), and 14 days (HC), respectively. Each sample was extracted in $60^{\circ}C$ and $95^{\circ}C$ hot water for 2 minutes. The soluble solids content of HA from the $60^{\circ}C$and $95^{\circ}C$ hot water extraction were $0.52{\pm}0.18%$ and $0.92{\pm}0.18%$, respectively. The soluble solids content was increased by the higher extraction temperature. The reducing sugar content of RC was $9.55{\pm}0.18mg/g$ in the $95^{\circ}C$ extraction, which was significantly higher than in the $60^{\circ}C$ extracted sample. However, the reducing sugar content did not show a remarkable difference based on aging periods. The total phenolic compound content of the $95^{\circ}C$ extracted samples was $3.36{\pm}0.13{\sim}9.88{\pm}0.23mg/g$, which was significantly higher than that of the $60^{\circ}C$ extracted sample. The ABTS radical scavenging activity of the $60^{\circ}C$ extracted RA and HA samples were 35.63% and 95.10%, respectively. Moreover, the radical scavenging activity increased to 63.35% and 96.78%, respectively, in the $95^{\circ}C$ extracted samples. As a result of the high temperature, the extracted sample showed an increase in the FRAP. In the RC sample, the FRAP was two times higher in the $95^{\circ}C$ extracted sample ($181.28{\pm}2.90{\mu}M$) than in the $60^{\circ}C$ extracted sample ($83.88{\pm}0.43{\mu}M$).

Study on Semi-Dry Process Developement of BP's Sludge by Non-Heating Manufacture Method (비가열 제조법에 의한 BP슬러지의 반건조 제조공정 개발에 관한 연구)

  • Kim, Byeong-Ki;Kim, Jae-Hwan;Kang, Seok-Pyo;Kang, Hye-Ju
    • Journal of the Korean Recycled Construction Resources Institute
    • /
    • v.3 no.4
    • /
    • pp.313-319
    • /
    • 2015
  • This study relates to an investigation into semi-dry manufacturing process of BP sludge based on non-heating production method. In this study, we conducted a research into reduction of water content ratio which arose from mixture of BP by-products of high water content ratio(50% or higher) with industrial by-products to use such BP by-products as construction materials in large quantity. We measured the reduction rate of water content ratio at the feeding ratio of water content reduction agent(1:0.5) in BP by-products. The results showed that water content ratio was the lowest with 18.5% in the mixture of PA+CFA(1:0.5). Moreover, water content ratio ranged between approximately 9.2% and 11.4% at the age of 1 day to 2 days at the aging temperature of $20-30^{\circ}C$, suggesting that the water content ratio was in the range within 10% which was a level suitable for use as construction material in this study. Meanwhile, we compared and evaluated the physical properties of non-heated BP by-products based on post-aging pulverization method. The results showed that there was no significant difference, depending on pulverization method. When production efficiency and economic feasibility were taken into consideration, it was found desirable to use fine particle pulverizer or pin mill enabling continuous production.

A Study on the Testing of Weather Resistance of Anti-corrosion Wax Covering Agents in the Locomotive at Jangdan Station of Gyeongui Line (경의선장단역증기기관차의 부식방지를 위한 왁스계 피복제 내후성 시험 연구)

  • Song, Won-Joon;Kim, Mi-Hyun;Ahn, Byong-Chan;Jeong, Hee-Don
    • Journal of Conservation Science
    • /
    • v.25 no.4
    • /
    • pp.373-381
    • /
    • 2009
  • To preserve steel cultural properties on display outdoors, the surface of these relics is processed with a covering treatment, which is a typical anti-corrosion method. Since the registered cultural heritage of Korea No. 78 Locomotive at Jangdan Station of Gyeongui Line will be treated by preservation process and displayed in the open outdoor area, effective surface covering agents were selected through testing to prevent the corrosion of the locomotive. The mixed wax are based on two types of microcrystalline wax which is one of regular surface covering agents for locomotives and bee‘s wax. For the weather resistance test, 3 types of wax were applied to each specimen of the locomotive and the specimens were tested in the Xenon-Arc Accelerated Weathering Tester for 1000 hours in accordance with the ISO 4892-1981 criteria and the test results were compared. As a result, on the surface of the specimen coated with the bee's wax, a whitening event appears after 400 hours which causes aging, and the specimens coated by the microcrystalline wax showed signs of a whitening event after 800 hours. The moisture contact angle with the microcrystalline wax coating was also less than with the bee's wax. Therefore, it was found that the high temperature microcrystalline wax is the most effective coating agent in terms of weather resistance and moisture blocking capability and the high temperature microcrystalline wax was adopted for coating the surface of the locomotive.

  • PDF

Study on Formation Mechanism of Iron Oxide Nanoparticles (산화철 나노입자의 형성 메커니즘에 대한 연구)

  • Kim, Dong-Young;Yoon, Seok-Soo;Takahashi, Migaku
    • Journal of the Korean Magnetics Society
    • /
    • v.22 no.5
    • /
    • pp.167-172
    • /
    • 2012
  • In order to analyze the formation mechanism of iron oxide nanoparticles, we measured the heat flow of $Fe(OL)_3$ precursor with temperature, and TEM images and AC susceptibility of aliquots samples sequentially taken from the reaction solution, respectively. The thermal decomposition of two OL-chain from $Fe(OL)_3$ produced the Fe-OL monomer, which were contributed to the formation of iron oxide nanoparticles. In the initial stage of nanoparticles formation, the small iron oxide nanoparticles had ${\gamma}-Fe_2O_3$ structure. However, as the iron oxide nanoparticles were rapidly growth, the iron oxide nanoparticles showed ${\gamma}-Fe_2O_3$-FeO core-shell structure which the FeO layer was formed on the surface of ${\gamma}-Fe_2O_3$ nanoparticles by insufficient oxygen supply from the reaction solution. These nanoparticles were transformed to $Fe_3O_4$ structure by oxidation during long aging time at high temperature. Finally, the $Fe_3O_4$ nanoparticles with high saturation magnetization and stable in the air could be easily synthesized by the thermal decomposition method.

Failure Analysis on High Pressure Steam Piping of 500 MW Thermal Power Plant (500 MW 화력발전소 고압 증기 배관 손상 원인 분석)

  • Kim, Jeongmyun;Jeong, Namgeun;Yang, Kyeonghyun;Park, Mingyu;Lee, Jaehong
    • KEPCO Journal on Electric Power and Energy
    • /
    • v.5 no.4
    • /
    • pp.323-330
    • /
    • 2019
  • The 500 MW Korean standard coal-fired power plant is the largest standardized power plant in Korea and has played a pivotal role in domestic power generation for over 20 years. In addition to the aging degradation due to long term operation, the probability of failure of power generation facilities is increasing due to frequent startup and stop caused by the lower utilization rate due to air pollution problem caused by coal-fired power plants. Among them, steam piping plays an important role in transferring high-temperature & pressure steam produced in a boiler to turbine for power generation. In recent years, failure of steam piping of large coal-fired power plant has frequently occurred. Therefore, in this study, failure analysis of high pressure piping weld was conducted. We identify the damage caused by high stress due to abnormal supporting structure of the piping and suggest improved supporting structure to eliminate high stress through microstructure analysis and piping stress analysis to prevent the occurrence of the similar failure of other power plant in the case of repetitive damage to the main steam piping system of the 500 MW Korean standard coal-fired power plant.

Storage properties of brown rice cultivar as affected by milling degree and storage conditions

  • Choi, Induck;Yoon, Mi-Ra;Kwak, Jieun;Chun, Areum;Jeon, Yong-Hee;Jeong, Tae-Wook;Kim, Sun-Lim
    • Proceedings of the Korean Society of Crop Science Conference
    • /
    • 2017.06a
    • /
    • pp.262-262
    • /
    • 2017
  • Brown rice contains a variety of nutritional and bio-functional components compared to milled rice. However, low consumer preference for steamed brown rice and short shelf life has been implicated as deterrents to the direct consumption of brown rice. This study was undertaken to determine the effect of degree of milling (DOM) on pasting and aging properties of brown rice cultivar. Short-grain (Japonica type) brown rice cv. Boseogchal (BSC), Baegjinju (BJJ), and Hiami (HIAM) were evaluated every month during 4 months storage. Rice cultivar were categorized into waxy (BSC), medium-waxy (BJJ), and non-waxy (HIAM) of which amylose contents were 6.81%, 10.06%, and 16.69~16.72%, respectively. Peak viscosity was the highest in BJJ followed by HIAM, and BSC, showing peak viscosity was lower at low temperature storage. At storage at room temperature from 60 to 120 days, the FFA content significantly increased in the rice samples with DOM1% followed by 3% and 5%, while not significant increase in DOM0% brown rice: at 120 days, the FFA ranged in 28.35~41.48, 111.99~130.06, 76.87~91.99, and 47.13~62.37 mg KOH/100g for DOM 0%, 1%, 3% and 5%, respectively. It indicated that the fat rancidity was the least in the order of DOM 0%, 5%, 3% and 1%. Storage at low temperature could reduce fat hydrolysis with lower FFA release, but rice grain with 1% MD also released more FFA compared to the other samples. It could be assumed that the most outer bran layer, approximately 1~3%, could provide a strong protection from fat rancidity. Pasting viscosity of rice samples also increased with increasing DOM rate. Results indicated that DOM was the most significant factor for lipid rancidity during storage, resulting in high FFA formation. It suggested that brown rice with DOM 0% and/or more than DOM 5% could provide the best shelf life.

  • PDF

Effects of pre-curing process on improvement of the compressive strength of IGCC-slag-based-geopolymer (IGCC 용융 슬래그로 제조된 지오폴리머의 강도증진에 Pre-curing이 미치는 영향)

  • Park, Soo-bin;Kim, Kang-duk;Kang, Seung-gu
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.27 no.6
    • /
    • pp.295-302
    • /
    • 2017
  • In this study, the effect of pre-curing process on the enhancement of mechanical properties of IGCC-slag-based-geopolymer was studied. Pre-curing is a process in which the green geopolymer is left at room temperature for a certain period of time prior to the high-temperature curing, and it is known as increasing the strength of a specimen. Therefore, in this experiment, the compressive strength of the geopolymers was measured according to various pre-curing conditions, and microstructure and crystal phase changes were observed by SEM and XRD, respectively. The W/S ratio was determined to be 0.26, which can offer the maximum geopolymer strength with easy molding ability, and the concentration of the alkali solution was 15 M. Pre-curing was performed at room temperature for 0 to 27 days. Compressive strength of the geopolymer made with pre-curing process increased by 36~87 % compared with the specimens made with no pre-curing process. Those improved compressive strength for the pre-cured geopolymer was confirmed owing to promotion effect of pre-curing process on generation of C-S-H gel and zeolite phases, which were analyzed using by XRD and SEM measurement.