• Title/Summary/Keyword: high strength materials

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Pore Structure Changes in Hardened Cement Paste Exposed to Elevated Temperature (고온 환경에 노출된 시멘트 경화체의 공극 구조 변화)

  • Kang, Seung-Min;Na, Seung-Hyun;Kim, Kyung-Nam;Song, Myong-Shin
    • Journal of the Korean Ceramic Society
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    • v.52 no.1
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    • pp.48-55
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    • 2015
  • Hardened cement-based materials exposed to the high temperatures of a fire are known to experience change in the pore structure as well as microstructural changes that affect their mechanical properties and tend to reduce their durability. In this experimental investigation, hardened Portland cement pastes were exposed to elevated temperatures of 200, 400, 600, 800, and $1000^{\circ}C$ for 60 minutes, and the resulting damage was studied by thermogravimetry (TG), mercury intrusion porosimetry (MIP) and density measurements. These results revealed that the residual compressive strength is increased at temperatures greater than $400^{\circ}C$ due to a small pore size of 3 nm and/or rehydration of the dehydrated cement paste. However, a loss of the residual strength occurs at temperatures exceeding 500 and $600^{\circ}C$. This can be attributed to the decomposition of hydrates such as portlandite and to an increase in the total porosity.

Effect of Radiation Intensity on Mechanical Properties of UV-cured Vinylester/Unsaturated Polyester Blend System (UV 경화가 비닐에스터와 불포화폴리에스터 블랜드 시스템의 물성 특성에 미치는 영향)

  • Lee, Jae-Rock;Kim, Young-Mi;Park, Soo-Jin
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.10a
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    • pp.269-272
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    • 2002
  • UV curing technology becomes important in various sectors of applications due to the high efficiency, environmental protection, and saving of energy. The effect of different proportion of vinylester (VE) and unsaturated polyester (UP) for VE/UP blend system was investigated in context of mechanical properties. The compositions of VE/UP blend were varied within 0:100, 20:80, 40:60, 60:40, 80:20, and 100:0 by weight percent. 1 wt% 1-hydroxy-cyclohexyl-phenyl-ketone was used as photoinitiator. The used intensity of UV light was in the range of $40~70 mW/\textrm{cm}^2$. The flexural strength of vinylester was not sensitive to the intensity of UV light. But the unsaturated polyester was very sensitive to the intensity of UV light. The flexural strength of vinylester was always superior to that of unsaturated polyester. The addition of the vinylester increased the flexural strength of blend system.

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Flexural properties of a light-cure and a self-cure denture base materials compared to conventional alternatives

  • Mumcu, Emre;Cilingir, Altug;Gencel, Burc;Sulun, Tonguc
    • The Journal of Advanced Prosthodontics
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    • v.3 no.3
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    • pp.136-139
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    • 2011
  • PURPOSE. A new light curing urethane dimethacrylate and a cold curing resin with simpler and faster laboratory procedures may have even improved flexural properties. This study investigated the 3-point flexural strengths and flexural moduli of two alternate base materials. MATERIALS AND METHODS. A cold curing resin (Weropress) and a light curing urethane dimethacrylate base material (Eclipse). Along with Eclipse and Weropress, a high impact resin (Lucitone199) and three conventional base materials (QC 20, Meliodent and Paladent 20) were tested. A 3-point bending test was used to determine the flexural strengths and flexural moduli. The mean displacement, maximum load, flexural modulus and flexural strength values and standard deviations for each group were analyzed by means of one-way analysis of variance (ANOVA) (with mean difference significant at the 0.05 level). Post hoc analyses (Scheffe test) were carried out to determine the differences between the groups at a confidence level of 95%. RESULTS. Flexural strength, displacement and force maximum load values of Eclipse were significantly different from other base materials. Displacement values of QC 20 were significantly different from Lucitone 199 and Weropress. CONCLUSION. The flexural properties and simpler processing technique of Eclipse system presents an advantageous alternative to conventional base resins and Weropress offers another simple laboratory technique.

Comparison of Polyphenylene Sulfide Composites Having Different Processing Temperatures and Glass Fibers

  • Jeong, Do Yeon;Yoo, Seung Yong;Jung, Chan-Gyu;Lee, Jaeyong;Kim, Sang Hoon;Lee, Pyeong-Chan;Lee, Hyun Wook;Ha, Jin Uk
    • Elastomers and Composites
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    • v.54 no.4
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    • pp.308-312
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    • 2019
  • Polyphenylene sulfide (PPS) is a well-known super engineering plastic with a high melting temperature (above 290℃). It is generally insoluble under regular conditions. Therefore, it can be used for replacing metallic materials. Many researchers are looking at the possibility of replacing aluminum in the engine compartment of an automobile. However, studies on PPS are not common as compared to conventional engineering plastics because only a few companies produce super engineering plastics. In this research, the material properties of PPS composites containing two different kinds of glass fibers and produced under different processing temperatures were investigated. The tensile strength of the PPS composites increased as the processing temperature increased. Although glass fibers with similar aspect ratios were compounded under the same processing condition, one of them yielded a higher mechanical strength.

The Effect of Acid Treatment Time for Ni Plating on the Joint of α-Al2O3 and Ni Metal (α-Al2O3와 Ni 금속 접합을 위한 Ni 무전해 도금시 산처리의 영향)

  • YI, EUNJEONG;AN, YONGTAE;CHOI, BYUNGHYUN;JI, MIJUNG;HWANG, HAEJIN
    • Journal of Hydrogen and New Energy
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    • v.27 no.3
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    • pp.306-310
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    • 2016
  • In Na-base Battery for ESS, ${\alpha}-Al_2O_3$ and metal bonding was used to prevent direct reaction between electrolyte and electrode. The hard metal was metalized at $1600^{\circ}C$ in a flowing hydrogen gas for high bonding strength. In this study, instead of hard metal metalizing, Ni was plated on ${\alpha}-Al_2O_3$ by electroless Ni plating technique and then bonded with metal. To enhance the bonding strength, surface of ${\alpha}-Al_2O_3$ was treated with $H_3PO_4$. The effects of strength and leakage of joining as a function of acid treatment time on ${\alpha}-Al_2O_3$ are described.

Effects of the Coiling Temperature and Anisotropy on the Tensile Properties of High-Strength API X70 Linepipe Steel

  • Dong-Kyu Oh;Seung-Hyeok Shin;Sang-Min Lee;Byoungchul Hwang
    • Archives of Metallurgy and Materials
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    • v.67 no.4
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    • pp.1487-1490
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    • 2022
  • In this study, the effect of the coiling temperature on the tensile properties of API X70 linepipe steel plates is investigated in terms of the microstructure and related anisotropy. Two coiling temperatures are selected to control the microstructure and tensile properties. The API X70 linepipe steels consist mostly of ferritic microstructures such as polygonal ferrite, acicular ferrite, granular bainite, and pearlite irrespective of the coiling temperature. In order to evaluate the anisotropy in the tensile properties, tensile tests in various directions, in this case 0° (rolling direction), 30°, 45° (diagonal direction), 60°, and 90° (transverse direction) are conducted. As the higher coiling temperature, the larger amount of pearlite is formed, resulting in higher strength and better deformability. The steel has higher ductility and lower strength in the rolling direction than in the transverse direction due to the development of γ-fiber, particularly the {111}<112> texture.

Effect of High Temperature Degradation on Microstructure and High Temperature Mechanical Properties of Inconel 617 (Inconel 617의 고온열화에 따른 미세구조 및 고온 기계적 특성)

  • Jo, Tae-Sun;Lee, Seung-Ho;Kim, Gil-Su;Kim, Se-Hoon;Kim, Young-Do
    • Korean Journal of Materials Research
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    • v.17 no.5
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    • pp.268-272
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    • 2007
  • Inconel 617 is a candidate tube material for high temperature gas-cooled reactors(HTGR). The microstructure and mechanical properties of Inconel 617 were studied after exposure at high temperature($1050^{\circ}C$). The dominant oxide layer was Cr-oxide. The internal oxide and Cr-depleted region were observed below the Cr-oxide layer. The depth of Cr-depleted zone and internal oxide increased with exposure time. The major phases of carbides are $M_{23}C_6\;and\;M_6C$. The composition of $M_{23}C_6\;and\;M_6C$ were determined to be Cr-rich and Mo-rich, respectively. $M_6C$ carbide is more stable than $M_{23}C_6$ at high temperature. From the results of high temperature compression test, there were no significant changes in hardness and yield strength upon increasing exposure time.

Stress-strain behavior and toughness of high-performance steel fiber reinforced concrete in compression

  • Ramadoss, P.;Nagamani, K.
    • Computers and Concrete
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    • v.11 no.2
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    • pp.149-167
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    • 2013
  • The complete stress-strain behavior of steel fiber reinforced concrete in compression is needed for the analysis and design of structures. An experimental investigation was carried out to generate the complete stress-strain curve of high-performance steel fiber reinforced concrete (HPSFRC) with a strength range of 52-80 MPa. The variation in concrete strength was achieved by varying the water-to-cementitious materials ratio of 0.40-0.25 and steel fiber content (Vf = 0.5, 1.0 and 1.5% with l/d = 80 and 55) in terms of fiber reinforcing parameter, at 10% silica fume replacement. The effects of these parameters on the shape of stress-strain curves are presented. Based on the test data, a simple model is proposed to generate the complete stress-strain relationship for HPSFRC. The proposed model has been found to give good correlation with the stress-strain curves generated experimentally. Inclusion of fibers into HPC improved the ductility considerably. Equations to quantify the effect of fibers on compressive strength, strain at peak stress and toughness of concrete in terms of fiber reinforcing index are also proposed, which predicted the test data quite accurately. Compressive strength prediction model was validated with the strength data of earlier researchers with an absolute variation of 2.1%.

Flexural Strength of RC Beam Strengthened by Partially De-bonded Near Surface-Mounted FRP Strip

  • Seo, Soo-yeon;Choi, Ki-bong;Kwon, Young-sun;Lee, Kang-seok
    • International Journal of Concrete Structures and Materials
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    • v.10 no.2
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    • pp.149-161
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    • 2016
  • This paper presents an experimental work to study the flexural strength of reinforced concrete (RC) beams strengthened by partially de-bonded near surface-mounted (NSM) fiber reinforced polymer (FRP) strip with various de-bonded length. Especially, considering high anchorage capacity at end of a FRP strip, the effect of de-bonded region at a central part was investigated. In order to check the improvement of strength or deformation capacity when the bonded surface area only increased without changing the FRP area, single and triple lines of FRP were planned. In addition, the flexural strength of the RC member strengthened by a partially de-bonded NSM FRP strip was evaluated by using the existing researchers' strength equation to predict the flexural strength after retrofit. From the study, it was found that where de-bonded region exists in the central part of a flexural member, the deformation capacity of the member is expected to be improved, because FRP strain is not to be concentrated on the center but to be extended uniformly in the de-bonded region. Where NSM FRP strips are distributed in triple lines, a relatively high strength can be exerted due to the increase of bond strength in the anchorage.

Comparison of Strength-Maturity Models Accounting for Hydration Heat in Massive Walls

  • Yang, Keun-Hyeok;Mun, Jae-Sung;Kim, Do-Gyeum;Cho, Myung-Sug
    • International Journal of Concrete Structures and Materials
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    • v.10 no.1
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    • pp.47-60
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    • 2016
  • The objective of this study was to evaluate the capability of different strength-maturity models to account for the effect of the hydration heat on the in-place strength development of high-strength concrete specifically developed for nuclear facility structures under various ambient curing temperatures. To simulate the primary containment-vessel of a nuclear reactor, three 1200-mm-thick wall specimens were prepared and stored under isothermal conditions of approximately $5^{\circ}C$ (cold temperature), $20^{\circ}C$ (reference temperature), and $35^{\circ}C$ (hot temperature). The in situ compressive strengths of the mock-up walls were measured using cores drilled from the walls and compared with strengths estimated from various strength-maturity models considering the internal temperature rise owing to the hydration heat. The test results showed the initial apparent activation energies at the hardening phase were approximately 2 times higher than the apparent activation energies until the final setting. The differences between core strengths and field-cured cylinder strengths became more notable at early ages and with the decrease in the ambient curing temperature. The strength-maturity model proposed by Yang provides better reliability in estimating in situ strength of concrete than that of Kim et al. and Pinto and Schindler.