• Title/Summary/Keyword: heat treatment processing

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Effects of Hydroxy Silicone Oil on Insulation Properties of Silicone Rubber(1) (Hydroxy Silicone Oil이 실리콘 고무의 절연특성에 미치는 영향(1))

  • 강동필;박효열;안명상;이웅재;이후범;오세호
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.11
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    • pp.1001-1007
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    • 2003
  • The silicone fluids have been generally used as processing agent in silicone rubber(SIR) compounding. The addition of hydroxy silicone (HS) fluids to SIR for insulator housing material is required to meet the good electrical performance and the good processability. In this study, SIR with HS fluids was evaluated to investigate how the kinds of them affect insulation properties. The contact angle of the virgin sample of 40-HS SIR was low and its recovery rate was also slow. The recovery rate of 50-HS SIR was the highest being decreased with the viscosity increase of HS fluids. The tracking resistances and the corona aging resistance of 70-HS SIR and 1,040-HS SIR were excellent Tracking resistance depended largely on heat resistance of silicone fluids. But arc resistance didn't depend merely on the kind of silicone fluids.

Mechanical Properties of Refractory Metals at Extremly High Temperatures

  • Fischer, B.;Beschliesser, M.;Hoffmann, A.;Vorberg, S.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.946-947
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    • 2006
  • Driven by the unavailibility of commercial test equipment for tensile and creep testing at temperatures up to $3000^{\circ}C$ a measuring system has been developed and constructed at the University of Applied Sciences, Jena. These temperatures are reached with precision by heating samples directly by electric current. Contact-less strain measurements are carried out with image processing software utilizing a CCD camera system. This paper covers results of creep tests which have been conducted on TZM sheet material (thickness 2 mm) in different heat-treatment conditions in the temperature range between $1200^{\circ}C$ and $1600^{\circ}C$.

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Processing of Cellular SiC Ceramics Using Polymer Microbeads

  • Lee, Sung-Hee;Kim, Young-Wook
    • Journal of the Korean Ceramic Society
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    • v.43 no.8 s.291
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    • pp.458-462
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    • 2006
  • A simple pressing process using a SiC powder, $Al_2O_3-Y_2O_3$ sintering additive, and polymer microbeads for fabricating cellular SiC ceramics is demonstrated. The strategy for making the cellular ceramics involves: (i) forming certain shapes using a mixture of a SiC powder, $Al_2O_3-Y_2O_3$ sintering additive, and polymer microbeads by pressing; (ii) heat-treatment of the formed body to burn-out the microbeads; and (iii) sintering the body. By controlling the microsphere content and sintering temperature, it was possible to adjust the porosity in a range of 16% to 69%. The flexural and compressive strengths of cellular SiC ceramics with $\sim$40% porosity were $\sim$60 MPa and $\sim$160 MPa, respectively.

Development of Carbon-Ceramic Composites using Fly Ash and Carbon Fibers as Reinforcement

  • Manocha, S.;Patel, Rakesh
    • Carbon letters
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    • v.7 no.1
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    • pp.27-33
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    • 2006
  • Carbon-ceramic composites were fabricated by using fly ash and PANOX fibers as reinforcement. Fly ash, because of its small size particles e.g. submicron to micron level can be effectively dispersed along with fibrous reinforcements. Phenolic resin was used as carbon precursor. Both dry as well as wet methods were used for forming composites. The resulting composites were characterized for their microstructure, thermal and mechanical properties. The microstructure and mechanical properties of composites are found to be dependent on type of the fly ash, fibrous reinforcements as well as processing parameters. The addition of fly ash improves hardness and the fibers, which get co-carbonized on heat treatment, increase the flexural strength of the carbon-ceramic composites. Composites with dual reinforcement exhibit about 30-40% higher strength as compared to the composites made with single reinforcement, either with fly ash as filler or with chopped fibers.

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The Effect of Drawing and Heat Treatment on Fatigue Life and Machinability in Free Machining Steel (쾌삭강의 피로수명 및 절삭성에 미치는 인발-열처리의 영향)

  • Suh, C.H.;Kim, D.B.;Oh, S.K.;Jung, Y.C.;Park, M.K.;Kim, Y.S.
    • Transactions of Materials Processing
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    • v.19 no.2
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    • pp.95-100
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    • 2010
  • Drawing and normalizing are efficient means for controlling strength, fatigue and machinability of free machining steel. Normally strength and machinability are conflicting properties which need to be optimized. In this study, the effects of normalizing temperature and reduction of area on strength, fatigue and machinability were investigated. Fine grains were generated at lower normalizing temperature and fatigue life was increased with decreasing grain size. Matrix was work hardened and elongated with increasing reduction of area. Inclusions also were elongated and cross-sectional area of inclusions along drawing axis was decreased. The effects of work hardening and grain size on fatigue life were significant, but only work hardening affected machinability. Shape and distribution of inclusions after drawing had little effect on fatigue life and machinability.

Numerical simlation of nanosecond pulsed laser ablation in air (대기중 나노초 펄스레이저 어블레이션의 수치계산)

  • 오부국;김동식
    • Laser Solutions
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    • v.6 no.3
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    • pp.37-45
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    • 2003
  • Pulsed laser ablation is important in a variety of engineering applications involving precise removal of materials in laser micromachining and laser treatment of bio-materials. Particularly, detailed numerical simulation of complex laser ablation phenomena in air, taking the interaction between ablation plume and air into account, is required for many practical applications. In this paper, high-power pulsed laser ablation under atmospheric pressure is studied with emphasis on the vaporization model, especially recondensation ratio over the Knudsen layer. Furthermore, parametric studies are carried out to analyze the effect of laser fluence and background pressure on surface ablation and the dynamics of ablation plume. In the numerical calculation, the temperature, pressure, density, and vaporization flux on a solid substrate are obtained by a heat-transfer computation code based on the enthalpy method. The plume dynamics is calculated considering the effect of mass diffusion into the ambient air and plasma shielding. To verify the computation results, experiments for measuring the propagation of a laser induced shock wave are conducted as well.

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Thermostability of Polyphenol Oxidase from Potato (Solanum tuberosum L.) (감자 Polyphenol Oxidase의 열안정성)

  • 김나영;이민경;박인식;방극승;김석환
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.30 no.5
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    • pp.844-847
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    • 2001
  • Factors affecting thermostability of polyphenol oxidase (PPO) from potato were studied for the purpose of providing useful information for food processing operations. The enzyme was most stable at pH 7.0 and it was inhibited to 70% after heat treatment at 8$0^{\circ}C$ for 1 min. The z-value for the thermal inactivation of the PPO was 12.17$\pm$0.58$^{\circ}C$. The thermostability of the enzyme was reduced by addition of sodium chloride. And the activity was inhibited by addition of reducing reagents such as 2-mercaptoethanol and dithiothreitol.

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The Formation and Crystallization of Amorphous Ti50Cu50Ni20Al10 Powder Prepared by High-Energy Ball Milling

  • Viet, Nguyen Hoang;Kim, Jin-Chun;Kim, Ji-Soon;Kwon, Young-Soon
    • Journal of Powder Materials
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    • v.16 no.1
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    • pp.9-15
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    • 2009
  • Amorphization and crystallization behaviors of $Ti_{50}Cu_{50}Ni_{20}Al_{10}$ powders during high-energy ball milling and subsequent heat treatment were studied. Full amorphization obtained after milling for 30 h was confirmed by X-ray diffraction and transmission electron microscope. The morphology of powders prepared using different milling times was observed by field-emission scanning electron microscope. The powders developed a fine, layered, homogeneous structure with prolonged milling. The crystallization behavior showed that the glass transition, $T_g$, onset crystallization, $T_x$, and super cooled liquid range ${\Delta}T=T_x-T_g$ were 691,771 and 80 K, respectively. The isothermal transformation kinetics was analyzed by the John-Mehn-Avrami equation. The Avrami exponent was close to 2.5, which corresponds to the transformation process with a diffusion-controlled type at nearly constant nucleation rate. The activation energy of crystallization for the alloy in the isothermal annealing process calculated using an Arrhenius plot was 345 kJ/mol.

Quality characteristics of improvement pellet nuruk inoculated from Aspergillus luchuensis 34-1

  • Jung, Eui-Hyoun;Mun, Ji-Young;Kim, So-Young;Yeo, Soo-Hwan
    • Journal of Biomedical and Translational Research
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    • v.19 no.4
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    • pp.103-109
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    • 2018
  • Aspergillus luchuensis 34-1 was inoculated into wheat pellets with different conditions of raw materials to produce nuruk. The degree of substrate reactivity improvement of steam treated raw materials compared with that of non-heat treated was analyzed. The water content of the pellet was adjusted to 25% and 35%, and steam treatment for 10 minutes improved the substrate reactivity at 2.1-fold and 3.1-fold, and sterilization was also possible. The characteristics of improvement pellet nuruk were investigated according to the degree of crushing and water content of raw materials according to the temperatures and humidities ($23^{\circ}C$, $30^{\circ}C$ and RH 60%, RH 80%). The pH of the pellet nuruk was higher depending on the temperature, humidity and moisture content of the koji were lower, and the pH of the flour-pellet nuruk was lower than that of 2 mm milling wheat-pellet nuruk according to milling degree. It can be seen that the milling degree affects the growth of mold. The acidity and amino acid were generally higher as fermentation time increased. Also, the higher the incubation temperature, humidity and moisture content, the higher the value. Glucoamylase activity was significantly the highest in moisture content 35% D2b nuruk, cultured at $30^{\circ}C$ and 80% RH for 38 hours. This is higher than the previous reports on glucoamylase of rice-koji or commercial nuruk using fungi isolated from traditional nuruk. From these study, it is expected that making of improvement pellet nuruk would save the fermentation time considerably compared with traditional nuruks.

Electron Discharge Machining (EDM) and Hole EDM of Cold Heat-treated Tool Steel Molds (STD11) by using Cu Electrodes (냉간 금형용 공구강의 Cu 전극을 이용한 방전 홀에 관한 연구)

  • Park, In-Soo;Lee, Eun-Ju;Kim, Hwa-Jeong;Wang, Deok-Hyun
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.4
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    • pp.76-82
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    • 2018
  • 3D formed Electrical Discharge Machining (EDM) and hole EDM were conducted for die and mold manufacturing with electrodes which were made by mechanical machining and wire EDM. It is difficult to machine the hardened material after heat treatment and quenching with traditional machining. The only method of machining hardened material is die-sinking EDM. In this research, hole EDM was conducted for heat-treated cold-worked tool steel (SKD11) for use as a die material. The EDM surfaces were analyzed by pulse-on time and peak current of EDM current, according to the machining conditions of EDM. The EDM surface profiles were affected by the peak current. The contribution of each factor is peak current (91.63%) and pulse-on time (0.93%). The best surface roughness was obtained with a $130{\mu}s$ pulse-on time and a 14.2 A peak current. With uniform EDM processing, the surface deteriorated with increasing pulse-on time and peak current. The thickness of the solidified layer induced by EDM was increased as the peak current, crater shapes, and erupted shapes of EDM surfaces were increased. Therefore, microcracking gaps induced by surface tension were increased.