• Title/Summary/Keyword: heat treatment processing

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Current Achievement and Perspectives of Seed Quality Evaluation in Soybean (콩 품질평가 현황과 전망)

  • 김용호
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.47
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    • pp.95-106
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    • 2002
  • Soybean is one of the most important sources of protein and oil in the world. Recently, emphasis has been laid on the chemical composition of soybean seeds for the processing soybean foods. Improvement of soybean components has been expected to improve food-processing quality for the processed soybean products such as soymilk and various edible ingredients as well as fur the traditional soyfoods. In Korea, soybean breeding research programmes have been focused on the quality of the products derived from soybean with yield stability, and some new modified soybean varieties haying good food-processing quality were developed recently. So the efforts of establishing standard and standardization of products in soybean are important. Three main categories should be considered in view of soybean seed quality; the marketing value such as grain size, shape, and appearance; the eating and processing value such as dehulled ratio, water absorption rate, and benny flavor; the nutritional value such as protein, lipid, and carbohydrate contents. And the new frontiers in research are looking at the functional nutrients in soybeans and how to improve them. In case marketing value, mainly the appearance is evaluated, therefore, each country has an application of standard related to quality. Each determination of standard class, heat-damaged kernels, splits, and soybeans of other colors is made on the basis of the grain when free from foreign materials. But processing value and nutritional value for standardization were not studied in detail till now. In addition, soybean has potential roles in the prevention and treatment of chronic diseases, most notably cancer, osteoporosis, and heart disease. The functional nutrients include a protease inhibitor, phytic acid, saponins, and isoflavones, etc.. It is believed that standardization of soybean quality should perform to overcome the difficulties, relatively high price of domestic soybean products has weakened the competitive power, in the market related to WTO. So, we should focus on further research into the evaluation and establishment of quality-standard in soybean.

A Study on Microstructure and Mechanical Properties of IF Steel Cube Fabricated by Multi-Axial Diagonal Forging Ver.1 and Ver.2 Processes (다축대각단조(MADF) Ver.1 및 Ver.2 공정으로 가공한 IF Steel의 미세조직 및 기계적 성질에 대한 연구)

  • Jeong, D.H.;Jo, Y.Y.;Kwon, S.C.;Kim, S.T.;Lee, S.;Choi, S.H.;Jeong, H.T.
    • Transactions of Materials Processing
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    • v.30 no.6
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    • pp.306-310
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    • 2021
  • In this study, IF steel, which has a body-centered cubic (BCC) crystal structure, was fabricated as a 25 mm-long cube, and then processed for one cycle without intermediate heat treatment by applying MADF Ver.1 and Ver.2 processes. MADF processing was performed with graphite lubrication for each pass at room temperature. The development of the microstructure and texture was analyzed and compared by the location of the specimen using EBSD measurements of the IF steel. Vickers hardness test and miniature tensile test were also performed to analyze the mechanical properties. The coarse grain size of 742.6 ㎛ of the as-received IF steel was refined to a grain size of 53.0 ㎛ after one cycle of MADF Ver.1 processing and 27.0 ㎛ after MADF Ver.2 processing. Vicker's hardness of the as-received IF steel at 94 Hv was increased to 185.6 Hv and 191.2 Hv after one cycle of MADF Ver.1 and Ver.2 processing, respectively.

Pre-leaching of Lithium and Individual Separation/Recovery of Phosphorus and Iron from Waste Lithium Iron Phosphate Cathode Materials (폐리튬인산철 양극재로부터 리튬의 선침출 및 인과 철의 개별적 분리 회수 연구)

  • Hee-Seon Kim;Boram Kim;Dae-Weon Kim
    • Clean Technology
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    • v.30 no.1
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    • pp.28-36
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    • 2024
  • As demand for electric vehicles increases, the market for lithium-ion batteries is also rapidly increasing. The battery life of lithium-ion batteries is limited, so waste lithium-ion batteries are inevitably generated. Accordingly, lithium was selectively preleached from waste lithium iron phosphate (LiFePO4, hereafter referred to as the LFP) cathode material powder among lithium ion batteries, and iron phosphate (FePO4) powder was recovered. The recovered iron phosphate powder was mixed with alkaline sodium carbonate (Na2CO3) powder and heat treated to confirm its crystalline phase. The heat treatment temperature was set as a variable, and then the leaching rate and powder characteristics of each ingredient were compared after water leaching using Di-water. In this study, lithium showed a leaching rate of approximately 100%, and in the case of powder heat-treated at 800 ℃, phosphorus was leached by approximately 99%, and the leaching residue was confirmed to be a single crystal phase of Fe2O3. Therefore, in this study, lithium, phosphorus, and iron components were individually separated and recovered from waste LFP powder.

Processing and properties of the $SiO_2-ZrO_2-Na_2O-B_2O_3$glass ceramics ($SiO_2-ZrO_2-Na_2O-B_2O_3$계 결정화 유리의 제조와 물성)

  • 안주삼;이원유;채병준;최승철;박영선
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.3
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    • pp.518-523
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    • 1998
  • The fracture toughness and hardness of 62 %$SiO_2-19%ZrO_2-9%Na_2O-10%B_2O_3$(wt%) glass ceramics system were investigated. As a result of DTA study to find crystallization temperature, an exothermic peak near $820^{\circ}C$ was observed. The optimum nucleation temperature and the optimum crystal growth temperature were determined by XRD and SEM analysis, and were approximately $650^{\circ}C$, $840^{\circ}C$ respectively. The fracture toughness of this zirconia glass ceramics was determined by Vickers Indentation Method. The hardness value was not changed with increasing of the heat treatment temperature, but fracture toughness value was increased up to $1.8 MPa{\cdot}m^{1/2}$ at $840^{\circ}C$, with increasing of heat treatment temperature.

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Effects of Various Fabrication Routes on Thermoelectric Properties of n-type Bi2Te2.85Se0.15 Alloys (제조공정에 따른 n형 Bi2Te2.85Se0.15합금의 열전성능 평가)

  • Nagarjuna, C.;Shin, D.W.;Lee, M.W.;Lee, S.H.;Hong, S.J.
    • Journal of the Korean Society for Heat Treatment
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    • v.31 no.3
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    • pp.135-142
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    • 2018
  • In this study, we have fabricated n-type $Bi_2Te_{2.85}Se_{0.15}$ compounds by different processing routes such as crushing, milling and mixing respectively. Subsequently, the obtained powders were consolidated by spark plasma sintering (SPS). The phase crystallinity of bulk samples were identified using X-ray diffraction technique. Powder morphology and fracture surface of bulk samples were observed using the scanning electron microscopy (SEM). The Seebeck coefficient and electrical conductivity values were significantly increased for the milling sample than crushing and mixing samples. As a result, the maximum power factor was obtained $2.4mW/mK^2$, which is thrice than that of crushing process. The maximum figure of merit (ZT) of 0.77 was achieved at 400 K for the milling sample. Furthermore, relatively high hardness and density values were noticed for the different processed samples.

Characterization of PET Thick & Thin Yarns on the Spinning Speed and Over Feed Ratio (방사속도 및 공급률에 따른 PET 태세사(Thick & Thin yarn)의 특성)

  • Park Myung-Soo;Shin Hyun-Sae;Jeong Jin-Soo;Son Jun-Sik
    • Textile Coloration and Finishing
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    • v.18 no.3 s.88
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    • pp.42-48
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    • 2006
  • The aim of this work is to develop Thick-Thin polyester yarn(T-T yarn) with finer than 1 denier mono filament. The manufacture of T-T yarns were carried out in a draw-winder using 85d/72f PET filament with various spinning speed of 2700, 2900, and 3100 m/min, respectively. The structure and physical properties of T-T yarns with spinning speed and over feed ratio were examined by draw-winder processing the sample in $100^{\circ}C$ water for 20 min and drying in 120, 140, 160, and $180^{\circ}C$ of dry air for 20 min. The crystallinity, the birefringence and the initial elasticity modulus of T-T yarns increased with increased spinning speed of filament and the heat treatment temperature but at the temperatures higher than $140^{\circ}C$ the increased rates show a tendency to decrease. Moreover, the initial modulus and the tenacity of T-T yarns increased with decreasing the over feed ratio of filament and the those of T-T yarns decreases with increasing the heat treatment temperature. The shrinkage of T-T yarns decreased with decreasing spinning speed and increased over feed ratio of filaments. Consequently, the results indicate that the best T-T yarn under 1 denier was optimized from PET filament with spinning speed of 2700 m/min and over feed ratio of 0.67

Study on the Fatigue Resistance of Gray Cast Iron in CO2 Laser Surface Hardening (CO2레이저 표면경화(表面硬化) 처리된 회주철(灰鑄鐵)의 피로특성(疲勞特性)에 관한 연구(硏究))

  • Park, K.W.;Han, Y.H.;Lee, S.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.3
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    • pp.169-181
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    • 1995
  • This study has been performed to investigate some effects of the power density and traverse speed of laser beam on the optical microstructure, hardness and fatigue resistance of gray cast iron treated by laser surface hardening technique. Optical micrograph has shown that the dissolution of graphite flakes and the coarsening of lath martensite tend to increase with a small amount of retained austenite as the power density increases under the condition of a given traverse speed. Hardness measurements have revealed that as the power density increases, hardness values of outermost surface layer increases from Hv=620 to Hv=647 in case of traverse speed of 2.0m/min at gray cast iron. Fatigue test has exhibited that the fatigue strength of laser surface hardened specimen is superier compared to that of untreated specimen, showing that values for the fatigue strength at $N_f=10^7$ of gray cast iron laser-surface-hardened at a low power density of $4076w/cm^2$ and a high power density of $8153w/cm^2$ under the condition of a given traverse speed of 2.0m/min are $15kg_f/mm^2$ and $20kg_f/mm^2$, respectively, whereas the fatigue strength of untreated specimen is $11kg_f/mm^2$. Under high stress-low cycle condition a noraml brittleness fracture appears, whereas a ductile fracture with beach mark is observed in the specimen tested under low stress-high cycle condition.

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Studies on the effect of heating conditions on the quality of soybean flours (대두분 품질에 미치는 가열처리조건에 관한 연구)

  • 이성갑;김준평
    • Journal of the Korean Professional Engineers Association
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    • v.17 no.4
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    • pp.28-39
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    • 1984
  • Experiments were carried out for the development of a processing method of soybean into full-fat or defatted flour, using two varieties of soybean (kwangkyo produced in Korea and Bragg produced in India) Samples were subjected to dry dehulling, size reduction and wet heat treatment processes to make soybean flours. The quality of soybean flours were evaluated, and the results obtained were summarized as follows. 1. Crude fiber content of dehulled soybean was under 3.0% which indicated satisfactory dehulling, and there was no significant difference in crude fibre content between two varieties. 2. When dehulled soybean was cracked into soy grits by a hammer mill, 98.71∼98.86% of the soy grit was in the range of 10∼18 mesh which was the optimum size of particle for quick and uniform penetration of heat into the intra-particle air spaces. 3. Moisture content of soy flour after steam treatment at 15 psig for 5 to 30 min was only 0.29∼1.68% which did not hinder the next milling operation. 4. From the color analysis of soy flours, it was observed that the dominant wavelength for all the samples are in a very narrow range from 575 to 581 nm and the color variation was from yellow to yellowish orange. Twenty to twenty five % higher reflectance was observed in the defatted flours than full fat flours. The % chroma of the defatted flour slightly increased as the duration of steaming of soy grits increased, whereas that of the full-fat flour did not. 5. The protein extractability in the defatted flour at pH 7.6 showed progressive decrease in solubility from 48.40% (Bragg), 75.20% (kwangkyo) for untreated flours to 9.75% (Bragg), 26.27% (kwangkyo) for 30 min steaming. But Kwangkyo variety showed twice higher protein extractability than Bragg variety.

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Effect of Heat Treatment on the Microstuctures and Mechanical Properties of TiC Dispersed Ni-base Alloy (TiC 분산된 니켈기 합금의 미세조직 및 기계적 특성에 미치는 열처리 영향)

  • Hong, Seong-Hyeon;Hwang, Keum-Chul;Rhee, Won-Hyuk;Chin, Eog-Yong
    • Journal of Powder Materials
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    • v.9 no.6
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    • pp.455-462
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    • 2002
  • The microstructures and properties of TiC dispersed nickel-base alloy were studied in this work. The alloy prepared by powder metallurgical processing was solution treated, 1st-aged at $880^{\circ}C$ for 16 hours, and then 2nd-aged at $760^{\circ}C$ for 4 hours. Microstucture of sintered specimen showed that TiC particles are uniformly dispersed in Ni base alloy. In the specimen aged at $880^{\circ}C$ for 8 hours, the fine $\gammaNi_3$(Al,Ti) precipitates with round shape are observed and the very fine $\gammaNi_3$(Al,Ti) particles with round shape are precipitated in the specimen aged at $760^{\circ}C$ for 4 hours. The presence of ${\gamma}$precipitates in TiC/Ni base alloy increased the hardness and wear resistance of the specimen. The hardness and wear resistance of the Ni-base with TiC are higher than those of conventional Ni-base superalloy X-750 because of dispersion strengthening of TiC particles. The hardness, transverse rupture strength and resistance of the specimen 2nd-aged at $760^{\circ}C$ for 4 hours are higher than those of 1st-aged specimen due to ultrafine $\gammaNi_3$(Al,Ti) precipitates.

Tensile Properties of Thixoformed Semi-solid A356 Alloy (반용융 성형된 반응고 A356 합금의 인장 특성)

  • Yu, Yeong-Bin;Song, Pal-Yong;Kim, Sang-Sik;Lee, Jae-Hyeon;Lee, Myeong-Ho
    • Korean Journal of Materials Research
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    • v.10 no.1
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    • pp.69-76
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    • 2000
  • Despite the improved formability and processing advantages, the use of semi-solid metals is greatly limited due to the difficulties in controlling the optimum forming parameters. In the present study, the tensile properties of closed die, pressure formed semi-solid A356 alloy were examined. It was demonstrated that the tensile strength of thixoformed A356 alloy could be greatly reduced when the forming parameters were not rigorously controlled. The reduced strength of unappropriately formed products appeared to be related to the coarsening of the primary phases. The possibility of improving tensile properties of as-formed products by simple post heat treatment was also assessed.

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