• Korean Journal of Food Science and Technology
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• v.27 no.2
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• pp.199-204
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• 1995

The changes of nucleotide and their related compounds, TMAO, TMA and total creatinine content of mackerel, pacific saury, yellow croaker and brown sole were investigated on heating conditions. The results were as follows. The content of inosine was the highest in all fish commonly, and white muscle fish showed higher than that of red muscle fish. The content of hypoxanthine showed increase by heat treatment but other compounds showed decrease. The contents of TMAO showed 31.1, 26.2, 49.4 and 58.5 mg% in each sample of raw materials, and brown sole showed the highest content than other fishes and TMAO contents showed decrease by heat treatment. The contents of TMA showed 3.7, 5.8, 22.9 and 16.9 mg% in each sample, and pacific saury showed the highest content than other fishes but TMA contents showed increase by heat treatment. The contents of total creatinine showed 341.2, 469.8, 52.3 and 87.6 mg% in each sample, and red muscle fish showed higher than that of white muscle fish and the highest content was shown in yellow croaker. All fish species showed decrease in contents of flavoring by heat treatment.

• Transactions of Materials Processing
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• v.30 no.1
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• pp.43-48
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• 2021

The success of warm forming of Mg alloy sheet is greatly influenced by friction at elevated temperature, depending on the surface treatment of the tool. The tool coating affected the frictional characteristics of AZ31B Mg alloy sheet at elevated and room temperatures. The frictional behavior of the Mg alloy sheet at room temperature was not significantly affected by surface treatment conditions of the tool, but was significantly affected at elevated temperature. When the contact pressure is high, a few surface-treated tools exhibit a higher coefficient of friction than those without surface treatment. It is important to select the surface treatment conditions of the tool in order to ensure appropriate friction during warm forming of Mg alloy sheet.

• Carbon letters
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• v.6 no.4
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• pp.234-242
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• 2005

Bending and tensile properties of 2D cross-ply C/C composites with processing heat treatment temperature (HTT) are evaluated. C/C composites used are made from two types of PAN based T700 and M40 carbon fibers with phenolic resin as carbon matrix precursor. Both the types of composites are heat treated at different temperatures (ranging from 750 to $2800^{\circ}C$) and characterized for bending and tensile properties. It is observed that, real density and open porosity increases with HTT, however, bulk density does show remarkable change. The real density and open porosity are higher in case T-700 carbon fiber composites at $2800^{\circ}C$, even though the density of M40 carbon fiber is higher. Bending strength is considerably greater than tensile strength through out the processing HTT due to the different mode of fracture. The bending and tensile strength decreases in both composites on $1000^{\circ}C$ which attributed to decrease in bulk density, thereafter with increase in HTT, bending and tensile strength increases. The maximum strength is in T700 fiber based composites at HTT $1500^{\circ}C$ and in M40 fiber based composites at HTT $2500^{\circ}C$. After attending the maximum value of strength in both types of composite at deflection HTT, after that strength decreases continuously. Decrease in strength is due to the degradation of fiber properties and in-situ fiber damages in the composite. The maximum carbon fiber strength realization in C/C composites is possible at a temperature that is same of fiber HTT. It has been found first time that the bending strength more or less 1.55 times higher in T700 fiber composites and in M40 fiber composites bending strength is 1.2 times higher than that of tensile strength of C/C composites.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.20 no.2
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• pp.51-57
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• 2021

The quality of the ceramic sintered coating on a metal surface through laser surface treatment is affected by the laser irradiation pattern. Depending on the laser irradiation pattern, the amount of residual stress and heat applied or accumulated on the surface increases or decreases, affecting the thickness attained in the ceramic sintering area. When the heat energy accumulated in the sintering area is high, the ceramic and the metal alloy melt and sufficiently mix to form a homogeneous and thick bonding interface. In this study, the thermal energy accumulation in the region sintered with zirconia was controlled using four types of laser processing patterns. The thickness of the diffusion region is analyzed by laser-induced breakdown spectroscopy of Mg-ZrO2 generated by laser sintering zirconia powder on the magnesium alloy surface. On the basis of the analysis of the Mg and Zr present in the sintered region through LIBS, the effect of the irradiation pattern on the sintering quality is confirmed by comparing and analyzing the heat and mass transfer tendency of the diffusion layer and the degree of diffusion according to the irradiation pattern. The derived diffusion coefficients differed by up to 9.8 times for each laser scanning pattern.

• Transactions of Materials Processing
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• v.33 no.3
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• pp.161-168
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• 2024

Aluminum alloy sheets, compared to conventional steel sheets, face challenges in press forming due to their lower elongation. To enhance their formability, extensive research has focused on forming technologies at elevated temperatures, specifically warm forming at around 300℃ and hot forming at approximately 500℃. This study proposes that the formability of aluminum alloy sheets can be significantly enhanced using a multi-stage hot forming technique. The research also investigates whether the strength of the A6061 aluminum alloy, known for its precipitation hardening, can be maintained when formed below the precipitate solid solution temperature. In the experiments, the A6061-T6 sheet underwent heating and rapid cooling between 250 and 500℃. The mechanical properties were evaluated at each stage of the process. The findings revealed that when the initial heat treatment was below 350℃, the strength of the material remained unchanged. However, at temperatures above 400℃, there was a noticeable decrease in strength coupled with an increase in elongation. Conversely, when the secondary heat treatment was conducted at temperatures of 350℃ or lower, the strength remained comparable to that of the initial heat treated material. However, at higher temperatures, a reduction in strength and an increase in elongation were observed.

• Journal of the Korean Ceramic Society
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• v.50 no.2
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• pp.122-126
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• 2013

The surface roughness of the inner and outer surfaces of a tube is an important requirement for nuclear fuel cladding. When an inner SiC clad tube, which is considered as an advanced Pressurized Water Cooled Reactor (PWR) clad with a three-layered structure, is fabricated by Chemical Vapor Deposition (CVD), the surface roughness of the substrate, graphite, is an important process parameter. The surface character of the graphite substrate could directly affect the roughness of the inner surface of SiC deposits, which is in contact with a substrate. To evaluate the effects of the surface roughness changes of a substrate, SiC deposits were fabricated using different types of graphite substrates prepared by the following four polishing paths and heat-treatment for purification: (1) polishing with #220 abrasive paper (PP) without heat treatment (HT), (2) polishing with #220 PP with HT, (3) #2400 PP without HT, (4) polishing with #2400 PP with HT. The average surface roughnesses (Ra) of each deposited SiC layer are 4.273, 6.599, 3.069, and $6.401{\mu}m$, respectively. In the low pressure SiC CVD process with a graphite substrate, the removal of graphite particles on the graphite surface during the purification and the temperature increasing process for CVD seemed to affect the surface roughness of SiC deposits. For the lower surface roughness of the as-deposited interlayer of SiC on the graphite substrate, the fine controlled processing with the completed removal of rough scratches and cleaning at each polishing and heat treating step was important.

• Korean Journal of Metals and Materials
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• v.49 no.1
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• pp.17-24
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• 2011

To investigate the relationship between heat treatment in zirconium alloy tubing process and metallurgical characteristics of Zr-1Nb-0.69Sn-0.11Fe alloy tubes, mechanical and oxidation behaviors of tubes heat treated at different temperatures after the final pilgering were investigated. The stress strain curves exhibited the saturation behaviors in all heat treatment conditions ($460{\sim}600^{\circ}C$) in this study with the onset strain of saturation increased with increase of post-pilgering annealing temperature. The strength fell off rapidly with increasing annealing temperature. The ultimate strength of the low tin Zr-1Nb-0.69Sn-0.11Fe alloy with slightly higher iron and oxygen contents in this study was found to be higher than Zr-1Nb-1Sn-0.1Fe alloy. The oxidation experiments in steam condition revealed that the corrosion resistance of low tin Zr-1Nb-0.69Sn-0.11Fe alloy was better than the Zr-1Nb-1Sn-0.1Fe alloy with a higher Sn content. The weight gain of low tin Zr-1Nb-0.69Sn-0.11Fe alloy tubes gradually increased with the increasing annealing temperature possibly due to the decreased Nb content in the matrix because of the formation of ${\beta}-Nb$ particles.

• Proceedings of the IEEK Conference
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• 2001.10a
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• pp.154-158
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• 2001

The heat treatment of PVC film containing PVC 65%, DOP(Dioctyl Phthalate) 32% as plasticizer, Ca-Zn stearates and surface agent was peformed under several conditions to study the degradation behavior of PVC sheet. In the case of H$_2$SO$_4$, the dehydrochlorination was ca.100% at 25$0^{\circ}C$ for 3h. The char involving the smaller pores was produced with hydrothermal treatment. The pore size became small with increasing the treatment time and temperature. In the case of treatment with Ca(OH)$_2$, the sizes of pores produced in char were about sever ~ 10${\mu}{\textrm}{m}$ at 2$25^{\circ}C$ for 12h. In the case of H$_2$SO$_4$, the size of pores were about 1${\mu}{\textrm}{m}$ in 5M H$_2$SO$_4$for 12h.

• Proceedings of the IEEK Conference
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• 2001.10a
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• pp.746-750
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• 2001

The heat treatment of PVC film containing PVC 65%, DOP(Dioctyl Phthalate) 32% as plasticizer, Ca-Zn stearates and surface agent was peformed under several conditions to study the degradation behavior of PVC sheet. In the case of H$_2$SO$_4$, the dehydrochlorination was ca.100% at 25$0^{\circ}C$ for 3h. The char involving the smaller pores was produced with hydrothermal treatment. The pore size became small with increasing the treatment time and temperature. In the case of treatment with Ca(OH)$_2$, the sizes of pores produced in char were about sever ~ 10${\mu}{\textrm}{m}$ at 2$25^{\circ}C$ for 12h. In the case of H$_2$SO$_4$, the size of pores were about l${\mu}{\textrm}{m}$ in 5M H$_2$SO$_4$for 12h.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2005.10a
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• pp.202-205
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• 2005

Effect of processing condition on the hot extrusion of Al-Zn-Mg-Sc alloy was investigated. For this purpose, hot compression test and FE-simulation were conducted via Thermecmasteer-Z and DEFORM-3D, respectively. The microstructure evolution during hot extrusion and post heat-treatment was investigated and deformation mechanisms were analyzed by constructing processing map. FE-simulation results show that the temperature difference between container and billet has considerable influence on the final shape of extruded T-shape bar. The relation between applied load and processing time was predicted by the FE-analysis as well as punch speed vs. stroke chart.