• Title/Summary/Keyword: heat treatment parameter

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Synthesis of Yttrium Oxide Nanowire by Hydrothermal Method (수열합성법을 이용한 이트륨 산화물 나노와이어의 합성)

  • Kim, Kyung-Ki;Kim, Yong-Jin;Ahn, Jung-Ho
    • Journal of Powder Materials
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    • v.18 no.1
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    • pp.73-77
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    • 2011
  • $Y(OH)_3$ nanowires were synthesized by a hydrothermal reaction of metallic Y with aqueous solution of LiOH. The morphology and the size of the nanowires changed with varying the volume of the LiOH solution inside the autoclave. $Y(OH)_3$ nanowires transformed to $Y_2O_3$ by a subsequent heat-treatment without morphological change. By a proper control of hydrothermal reaction parameter and heat-treatment, the yield of pure $Y_2O_3$ nanowires up to 97% was attained.

Charge/discharge characteristics by heat treatment condition of cathode active material LiMn$_2$O$_4$ for Li rechargeable batteries (리튬 2차 전지용 정극 활물질 LiMn$_2$O$_4$의 열처리 조건에 따른 충방전 특성)

  • 정인성;구할본
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1996.11a
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    • pp.369-372
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    • 1996
  • We prepared LiMn$_2$O$_4$ by reacting stoichiometric mixture of LiOH.$H_2O$ and MnO$_2$ (mole ratio 1 : 1) and heating at 80$0^{\circ}C$ for 24h, 36h, 48h, 60h and 70h. We obtained through X-ray diffraction that lattice parameter varied as function of heat treatment time. heated cathode active materials at 80$0^{\circ}C$ for 36h, (111)/(311) peak ratio was 0.37. It expected good charge/discharge characteristics. When (111)/(311) peak ratio was 0.37, it will be that crystal structure is farmed very well. In the result of charge/discharge test When heated at 80$0^{\circ}C$ for 36h, charge/discharge characteristic of LiMn$_2$O$_4$is the most property. It agree with our expectation.

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The ionization energy and lattice parameters of Co- and Ce-doped cubic zirconia (YSZ) single crystal (Co와 Ce를 첨가한 큐빅지르코니아(YSZ) 단결정의 이온화에너지 및 격자상수)

  • Seok, Jeong-Won
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.20 no.4
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    • pp.159-163
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    • 2010
  • Co-(0.5 mol%) and Ce-(0~0.3 mol%) doped cubic zirconia ($ZrO_2:Y_2O_3$=64:36 mol%) single crystals grown by a skull melting method were heat-treated in $N_2$ at $1200^{\circ}C$ for 3 hrs. The brown-colored as-grown single crystals were changed into either green or blue color after the heat treatment. Before and after the heat treatment, the YSZ (yttriastabilized zirconia) single crystals were cut for wafer form (${\phi}7mm{\times}t2mm$) and round brilliant cut ($\phi$ 12 mm). The optical and structural properties were examined by UV-VIS spectrophotometer and X-ray diffraction. Absorption by $Ce^{3+}(^2F_{5/2},\;_{7/2}(4f){\rightarrow}^2T_g(5d^1)),\;Co^{2+}(^4A_2(^4F){\rightarrow}^4T_1(^4F)$ or $^4T_1(^4P))$ and $Co^{3+}$, change of ionization energy and lattice parameter were confirmed.

Characterization of Live Fire Load in Buildings - Heat Release Characteristics of Typical Live Fire Load in Bookstore - (건축물의 적재가연물 특성에 관한 연구 -대형서점의 적재가연물 연소발열성상-)

  • Nam, Dong-Gun;Yuji, Hasemi;Jung, Jong-Jin;Lim, Woo-Sub;SaKong, Seong-Ho
    • Proceedings of the Korea Institute of Fire Science and Engineering Conference
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    • 2008.11a
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    • pp.3-6
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    • 2008
  • Heat release characteristics of live fire load are an important parameter for performance oriented fire safety design of a building. While investigations have been carried out on the fire load and its burning behavior in office, residential and commercial buildings and so on, little effort has been paid for the rational treatment of fire load in bookstore. In this report, burning behavior of typical combustible objects in bookstore are studied by measuring heat release rates of bookshelf with book.

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Effects of Projection Height and Post Treatment on the Resistance Projection Weldability of Zn Coated Sheet Steels (아연도금 강재의 용접성에 미치는 돌기 성형 및 피복조건의 영향)

  • 김기철;이목영
    • Journal of Welding and Joining
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    • v.17 no.5
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    • pp.83-88
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    • 1999
  • In this paper resistance projection weldability of Zn coated steels with post treatment has been discussed. Projection welding was performed by a condenser discharge type power source which was equipped with welding parameter monitoring system. Mechanical test results indicated that the effect of post coatings on the projection front changed showing very small very small spattering at the weld strength was negligible. However, contamination rate of the block electrode varied depending on the post treatment coatings. Test results also showed that projection height before welding should be kept to be 80-100% of the specimen thickness as far as the surface quality was taken into consideration. Based on the high speed photography, discharge condition at the beginning stage of the welding process. It was considered that the spattering reduced the weld strength slightly at the optimum heat input range.

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Effects of the Surface Roughness of a Graphite Substrate on the Interlayer Surface Roughness of Deposited SiC Layer (SiC 증착층 계면의 표면조도에 미치는 흑연 기판의 표면조도 영향)

  • Park, Ji Yeon;Jeong, Myung Hoon;Kim, Daejong;Kim, Weon-Ju
    • Journal of the Korean Ceramic Society
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    • v.50 no.2
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    • pp.122-126
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    • 2013
  • The surface roughness of the inner and outer surfaces of a tube is an important requirement for nuclear fuel cladding. When an inner SiC clad tube, which is considered as an advanced Pressurized Water Cooled Reactor (PWR) clad with a three-layered structure, is fabricated by Chemical Vapor Deposition (CVD), the surface roughness of the substrate, graphite, is an important process parameter. The surface character of the graphite substrate could directly affect the roughness of the inner surface of SiC deposits, which is in contact with a substrate. To evaluate the effects of the surface roughness changes of a substrate, SiC deposits were fabricated using different types of graphite substrates prepared by the following four polishing paths and heat-treatment for purification: (1) polishing with #220 abrasive paper (PP) without heat treatment (HT), (2) polishing with #220 PP with HT, (3) #2400 PP without HT, (4) polishing with #2400 PP with HT. The average surface roughnesses (Ra) of each deposited SiC layer are 4.273, 6.599, 3.069, and $6.401{\mu}m$, respectively. In the low pressure SiC CVD process with a graphite substrate, the removal of graphite particles on the graphite surface during the purification and the temperature increasing process for CVD seemed to affect the surface roughness of SiC deposits. For the lower surface roughness of the as-deposited interlayer of SiC on the graphite substrate, the fine controlled processing with the completed removal of rough scratches and cleaning at each polishing and heat treating step was important.

Heat Release Characteristics of Typical Live Fire Load in Large Bookstore (대형서점 적재가연물의 초기 연소발열성상)

  • Nam, Dong-Gun
    • Fire Science and Engineering
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    • v.25 no.2
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    • pp.88-94
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    • 2011
  • Heat release characteristics of live fire load are an important parameter for performance oriented fire safety design of a building. While investigations have been carried out on the fire load and its burning behavior in office, residential and commercial buildings and so on, little effort has been paid for the rational treatment of fire load in bookstore. In this report, burning behavior of typical combustible objects in bookstore are studied by measuring heat release rates of bookshelf with book. Based on the results, it has reviewed fire safety when a fire accident occurs on the large bookstore and suggested peak heat release rate per burning surface, fire growth rate, etc of the live fire load required for fire safety design in bookstore.

Immersion Corrosion Characteristic of SUS420J2 Steel with a Material for Fish Pre-Processing Machinery (어류 전처리 가공기계용 재료 SUS420J2강의 침지부식 특성)

  • 김선진;안석환;최대검;정현철;김상수
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.38 no.1
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    • pp.79-88
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    • 2002
  • 13%Cr martensitic stainless steel has been used mainly with a material for fish pre-processing machinery. However, it has not very nice cutting section because of little of the carbon content. Therefore, SUS420J2 steel that contents 0.3%C with high-strength in spite of the rust is used with a material for fish pre-processing machinery. However, studies on the corrosion characteristics of SUS420J2 steel are relatively rare. Especially, the corrosion phenomenon may cause serious degradation because the fish pre-processing machinery is exposed always to seawater environment. In this paper, the immersion corrosion test was carried out at seawater environment (pH=7.52) on SUS420J2 steel specimens that have various post-treatment conditions and its corrosion characteristics were evaluated. From test results, the specimens such as base metal, vacuum heat treatment, electrolytic polishing and tempering after quenching tend somewhat sensitive from the corrosion. In the case of vacuum heat treatment specimen of continuous immersion during 360 days, the weight loss ratio was high about seven times when compared with the different specimens. On the contrary, SUS420J2 steel specimen that has the heat treatment of tempering after quenching and the electrolytic polishing was less sensitive from the corrosion, and the weight loss ratio was very low.

Effect of suitable dietary glycine supplementation on growth production, meat quality, serum parameters, and stress alleviation of broiler under heat stress condition

  • Jiseon Son;Woo-Do Lee;Hyunsoo Kim;Eui-Chul Hong;Hee-Jin Kim;Yeon-Seo Yun;Hwan Ku Kang
    • Korean Journal of Agricultural Science
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    • v.50 no.4
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    • pp.603-616
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    • 2023
  • This study was conducted to investigate the productivity, meat quality, blood variables, stress responses, and litter quality of broilers offered feed with different levels of Glycine (Gly) supplementation under heat stress condition. A total of 760 one-day-old Ross 308 broiler males were randomly assigned to one of the four dietary treatment groups: (1) basal diet (control; CON); (2) basal diet + Gly 0.1% (Gly 0.1%); (3) basal diet + Gly 0.2% (Gly 0.2%); and (4) basal diet + Gly 0.3% (Gly 0.3%). The environments for all the treatments groups were maintained according to broiler rearing guidelines from day 1 to day 21, and heat stress condition (32 ± 1℃, 60 ±5%) was created from day 22 to the end. The addition of Gly increased weight gain and affected feed intake (p < 0.05). Gly 0.1% group had higher pH and ferric reducing antioxidant power (FRAP) in the chicken meat and lower heterophil (HE)/lymphocyte (LY) ratio in the blood (p < 0.05). In particular, Gly 0.2% treatment group had lower serum corticosterone level (p < 0.05) than other groups. For jejunum morphology, the addition of Gly 0.2% significantly reduced the depth of the crypts (p < 0.05). However, the addition of Gly did not significantly affect litter quality (p > 0.05). In conclusion, the addition of glycine improved productivity and meat quality, alleviated heat stress, and improved intestinal function. Further studies are needed to determine the optimal level and mechanism of action of the additive when ingested.

Creep Properties of Aircraft Gas Turbine Materials in relation to Heat Treatment (항공기용 가스터빈 재료의 열처리에 따른 크리프 특성)

  • Kong, Yu-Sik;Oh, Sae-Kyoo;Park, No-Kwang
    • Journal of Ocean Engineering and Technology
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    • v.13 no.4 s.35
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    • pp.112-117
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    • 1999
  • In this paper, the creep properties and creep life prediction by Larson-Miller Parameter method for Udimet 720 to be used for aircraft gas turbine engines or other high temperature components were presented at the elevated temperatures of 538, 649 and $704^{\circ}C$. It was confirmed experimentally and quantitatively that a creep life predictive equation at such various high temperatures was well derived by LMP.

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