• 한국주조공학회지
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• 제12권6호
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• pp.450-457
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• 1992

The study aims to investigate the influence of alloying elements(V,Ti) and heat treatment on the mechanical properties in hypo-eutectic chromium cast iron. Before heat treatment, all of the specimen were fully annealed(950$^{\circ}C{\times}5Hr$) to homogenize their structures. The influence of heat treatment and alloying elements(V,Ti) on hardness, retained austenite volume, and charpy impact energy as well as tensile strength of the specimen was tested systematically. Retained austenite decreased with the increase of V and Ti, but incresed with the increase of number of cycles. The impact energy decreased, and hardness and tensile strength increased with the increase of alloying elements (V,Ti) and the decrease of the number of cycles. The hardness and tensile strength increased, but impact energy decreased with the increase of V and Ti elements and the temperature of destabillization heat treatment. After the destabillization heat treatment at the same temperature, the impact energy is increased, while hardness and tensile strength decreased as the increase of tempering temperature. Retained austenite increased with increase of destabilizatoin heat treatment temperature, while decrease with the increase of tempering temperature.

• 한국분말재료학회지
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• 제28권4호
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• pp.301-309
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• 2021

In this study, an AISI 316 L alloy was manufactured using a selective laser melting (SLM) process. The tensile and impact toughness properties of the SLM AISI 316 L alloy were examined. In addition, stress relieving heat treatment (650℃ / 2 h) was performed on the as-built SLM alloy to investigate the effects of heat treatment on the mechanical properties. In the as-built SLM AISI 316 L alloy, cellular dendrite and molten pool structures were observed. Although the molten pool did not disappear following heat treatment, EBSD KAM analytical results confirmed that the fractions of the low- and high-angle boundaries decreased and increased, respectively. As the heat treatment was performed, the yield strength decreased, but the tensile strength and elongation increased only slightly. Impact toughness results revealed that the impact energy increased by 33.5% when heat treatment was applied. The deformation behavior of the SLM AISI 316 L alloy was also examined in relation to the microstructure through analyses of the tensile and impact fracture surfaces.

• 한국분말재료학회지
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• 제18권6호
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• pp.552-561
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• 2011

This study attempted to manufacture a Cu-15 at.%Ga coating layer via the cold spray process and investigated the effect of heat treatment environment on the properties of cold sprayed coating material. Three kinds of heat treatment environments, $5%H_2$+argon, pure argon, and vacuum were used in this study. Annealing treatments were conducted at $200{\sim}800^{\circ}C$/1 hr. With the cold sprayed coating layer, pure ${\alpha}$-Cu and small amounts of $Ga_2O_3$ were detected in the XRD, EDS, EPMA analyses. Porosity significantly decreased and hardness also decreased with increasing annealing temperature. The inhomogeneous dendritic microstructure of cold sprayed coating material changed to the homogeneous and dense one (microstructural evolution) with annealing heat treatment. Oxides near the interface of particles could be reduced by heat treatment especially in vacuum and argon environments. Vacuum environment during heat treatment was suggested to be most effective one to improve the densification and purification properties of cold sprayed Cu-15 at.%Ga coating material.

• 한국주조공학회지
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• 제36권5호
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• pp.167-173
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• 2016

The effect of various types of heat-treatment on the mechanical properties of cast Alloy 718 has been investigated. Cast Alloy 718 bars were subjected to 'standard heat-treatment'_(SHT), 'HIP (Hot Isostatic Pressing) heat-treatment'_(HHT), and 'HIP-simulated heat-treatment'_(HS). In the absence of long time high temperature heat-treatment, a small amount of Laves phase remained in the 'SHT' specimen, and needle shaped ${\delta}$ precipitated in the vicinity of the Laves phase. Due to the formation of the Laves and ${\delta}$ phases in the 'SHT' specimen, it exhibited lower tensile properties than those of the others_specimens. On the other hand, the Laves phase was completely dissolved into the matrix after 'HHT' and 'HS' treatments. It is known that isostatic pressure reduces the self-diffusion coefficient, because of the lower self-diffusivity under HIP conditions in the interdendritic region, Nb segregation and the high amount of ${\gamma}^{{\prime}{\prime}}$ precipitation that occurs. Due to the higher fraction of coarse ${\gamma}^{{\prime}{\prime}}$ phases, the 'HHT' treated Alloy 718 showed excellent tensile strength.

• 청정기술
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• 제28권2호
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• pp.110-116
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• 2022

본 연구에서는 NdFeB 영구자석 스크랩으로부터 회수한 철(Fe) 부산물을 이용하여 산화철(FeO_x) 나노입자를 합성하였고, 열처리 온도가 FeO_x 나노입자의 물성에 미치는 영향을 관찰하였다. 이를 위해 D.I. water에 약 10 wt%로 희석한 철 부산물 용액에 2.0 M 암모니아(NH₄OH) 용액을 투여하여 산화철 전구체를 석출하였고, 이를 300 ℃, 400 ℃, 500 ℃ 및 600 ℃로 각각 열처리하여 FeO_x 나노 입자를 합성, 열처리 온도에 따른 FeO_x 나노 입자의 물성을 관찰하였다. X-ray diffraction (XRD) 분석 결과 열처리 온도가 증가할수록 <104> 회절 피크가 성장하여 500 ℃ 이상에서 α-Fe₂O₃ 결정구조와 일치하는 회절 피크가 검출되었다. BET (Brunauer-Emmett-Teller) 비표면적 분석 결과 400 ℃ 이상에서 열처리 온도가 증가할수록 비표면적이 감소하는 경향을 나타내었다. HRTEM (high resolution transmission electron microscope) 관찰 결과 rod 형 나노입자가 관찰되었고, 열처리 온도 증가에 따라 나노입자의 크기가 증가하는 경향을 나타내었다.

• 열처리공학회지
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• 제23권6호
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• pp.344-349
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• 2010

Silicon carbide nanowires were grown by heat treatment of the films at $1200^{\circ}C$ after amorphous SiC thin films were deposited on graphite substrate by radio frequency magnetron sputtering at $600^{\circ}C$. It was confirmed that SiC nanowires with the diameter of 20-60 nm and length of about 50nm were grown from Field Emission Scanning Election Microscope (FE-SEM) and Transmission Election Microscope (TEM) observation. The diameter of nanowires was increased as heat treatment time is increased. The nanowires were identified to ${\beta}$-SiC single crystalline from X-Ray Diffraction(XRD) analysis. It was observed from this study that deposition temperature of samples was critical to the crystallization of nanowires. On the other hand, the effect of deposition time was insignificant.

• Journal of the Korean Wood Science and Technology
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• 제23권4호
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• pp.67-73
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• 1995

This study was undertaken to investigate the effect of heat treatment on the dynamic viscoelasticity of three species of Phyllostachys bambusoides, Phyllostachys nigra var. henonis and Phyllostachys pubescens, grown in southern Korea. The bamboo was treated for 3~24 hours at $60{\sim}180^{\circ}C$, and then was treated in a climatic chamber for 3~48 hours at $40^{\circ}C$ and 95% relative humidity. The results obtained are summarized as follows : 1. Dynamic Young's modulus decreased with increasing temperature and duration of the heat treatment. 2. Internal friction decreased with increasing treatment duration. 3. Moisture absorption decreased with increasing temperature and duration of the heat treatment. 4. Dynamic viscoelasticity decreased, whereas internal friction slowly increased, with increasing moisture content.

• 한국전기전자재료학회논문지
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• 제11권7호
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• pp.502-507
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• 1998

The purpose of this study is to investigate the breakdown properties in joint interface of power cables with heat treatment. The specimens have the structure of XLPE/EPDM interface like the joint of distribution power cable. The breakdown characteristics of the SLPE/EPDM joint were studied with crosslinking by=products. AC breakdown voltages were measured with heat treatment time and interfacial materials and crosslinking by-products as testing factors. This study has shown that crosslinking by-product gases play an important role at the insulation properties of cable joints by heating. The dielectric strength shows the lowest values at 4 hours heat treatment. The AC breakdown strength in the untreated sample was increased with heat treatment time.

• Journal of Welding and Joining
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• 제4권2호
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• pp.21-29
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• 1986

The influence of welding heat input variation(600-900J/cm) and heat-treatment condition after welding on tensile strength of butt welded joint in $175Kg/mm^2$ strength level Maraging steel(Co-free and Co-containing) sheets was investigated on the basis of hardness distribution, microstructure of weld metal and fracture surface. The obtained main results are as follows; 1. The strength of weldment (UTS, NTS), joint efficiency showed a little decreasing tendency with the increase in welding heat input, and the elongation showed a little increasing tendency with the increase in the width of weld metal. It was considered because of the plastic constraint of the high strength base metal. 2. The strength of weldment was better in the solution treatment and aging than the aging only after welding due to the disappearance of almost denverite in weld metal. 3. The hardness distribution in weldment after welding and heat-treatment was almost similar to both Co containing and Co free Maraging steel with change in welding heat input. 4. The fracture was occurred at weld metal, and the fracture surface showed a relatively shallow dimples in both Co containing and Co free Maraging steel.

• Journal of Welding and Joining
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• 제14권4호
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• pp.89-98
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• 1996

This study was performed to establish the characteristics of the heat affected zones from view point of the repair weldability for a damaged CrMoV steam turbine rotor steel. Characterization of the heat affected zones of the weldment was conducted with respect to various of postweld heat treatment temperatures, $566^{\circ}C$, $621^{\circ}C$ and $677^{\circ}C$. The evaluations of the heat affected zones were carried out in terms of microstructural characterization, microhardness measurements, Charpy v-notch impact, tensile and stress-rupture tests. The results indicated that the effect of the postweld heat treatment at $677^{\circ}C$ exhibited the favorable microstructure and mechanical properties for the stability of the heat affected zones. While the heat affected zone of the weldment, produced without postweld heat treatment, displayed the inferior toughness and microstructure indicating localized carbide precipitations on the grain boundary. It was also indicated that the stability of the heat affected zones were deteriorated by the formation of the cavitation on the grain boundaries.