• Title/Summary/Keyword: heat pressing

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Development of Separating Techniques on Quercetin-Related Substances in Onion(Allium cepa L.) 2. Optimal Extracting Condition of quercertin-Related Substances in Onion (양파의 Quercetin 관련 물질의 분리 기술 개발 2. 양파의 Quercetin 물질의 최적 추출조건)

  • 강성구;김용두;현규환;김영환;서재신;박양균
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.27 no.4
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    • pp.687-692
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    • 1998
  • To use onion(Allium cepa L.) residue as raw materials of food product, yields of onion-juice according to various extracting methods and optimal extracting condition of quercetin and its related glycosides were carried out. Onion juices gained by the methods of pressing, rotary crushing, freeze pressing and enzyme treatment. The yield by the method of enzyme treatment was higher than others. The yields of juice from fresh onion and heat-treated onion(8$0^{\circ}C$/10min) by pressing were 66% and 83%, respectively. Ethanol extraction of onion was efficient at 75$^{\circ}C$ and acetic acid extraction was proper at 3% concentration for 3 hours at 11$0^{\circ}C$. The onion extract was fractionated in the order of hexane, chloroform, ethylacetate and butanol to test flavonoids. The highest abundant flavonoids were found in ethylacetate and butanol fraction.

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Thermoelectric Properties of Ni-doped $CoSb_3$ Prepared by Encapsulated Induction Melting and Hot Pressing

  • Kim, Mi-Jung;Park, Kwan-Ho;Jung, Jae-Yong;You, Sin-Wook;Lee, Jung-Il;Ur, Soon-Chul;Kim, Il-Ho
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.688-689
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    • 2006
  • Ni-doped $CoSb_3$ was prepared by the encapsulated induction melting and hot pressing, and its doping effects on the thermoelectric properties were investigated. Single phase $\delta-CoSb_3$ was successfully obtained by the subsequent heat treatment at 773K for 24 hours. Nickel atoms acted as electron donors by substituting cobalt atoms. Thermoelectric properties were remarkably improved by the appropriate doping.

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Thermal-Structural Coupled Field Analysis of the Circumferential Pressing Type Brake Disc (원주가압형 브레이크 디스크의 열-구조 연성해석)

  • Kim, Hyeong-Hoon;Lee, Seong-Wook;Han, Dong-Seop;Han, Geun-Jo
    • Transactions of the Korean Society of Automotive Engineers
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    • v.16 no.4
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    • pp.69-74
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    • 2008
  • The heat generated by the brake system of vehicles results in reduction of friction force on the brake surface and vibration during a braking. To solve these problems, extensive research for the brake shape has been conducted such as drilling cooling holes on the brake disc, accommodating ventilated holes and etc. In this study, we suggest the circumferential pressing type brake disc in order to improve its cooling performance. In order to compare the cooling-down efficiency between the conventional side-pressing type and the circumferential-pressing type, we adopted the FMVSS 105-77 as thermal analysis conditions and This newly proposed concept has been verified using Thermal-structure Coupled Field Analysis along with comparative analysis with the existing ventilated disk.

Effect of Additives on Densification and Grain Growth of Magnesia (마그네시아의 치밀화 및 입자성장에 미치는 첨가물의 영향)

  • Lee, Hae-Weon;Kim, Whan
    • Journal of the Korean Ceramic Society
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    • v.19 no.2
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    • pp.127-132
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    • 1982
  • This experiment has been carried out for the purpose of investigating the effect of additives on densification and grain growth in magnesium oxide by a two-step process; hot pressing and heat treating. MgO powder has been obtained by calcining extra reagent grade MgCO3 at 90$0^{\circ}C$ for 30 minutes, and additives have been added to $MgCO_3$ in the form of soluble salts-Al$(NO_3)_3$$. $9H_2O$ and $Cr(NO_3)_3$.9H_2O$. The hot pressing has been carried out with changes of soaking time at 125$0^{\circ}C$ under the pressure of 250kg/$\textrm{cm}^2$, and the heat treating also at same temperature. The initial particle size of MgO measured by particle size analyzer was 0.86 microns. Densification rate obeyed the equation D=K lnt + C, and grain growth rate obeyed the equation G-G0=kt1/2. It was vaporization of some $Cr_2O_3$ and formation of solid solution that had an influence on desification of MgO containing $Cr_2O_3$. Activation energy for grain growth of pure MgO was 62.4 kcal/mole, therefore grain growth was supposed to be diffusioncontrolled process. But after heat treatmeat, excess additives were expected to slow down the grain growth by the formation of second phase or the solute atoms at grainboundary.

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Microstructure-Properties Relationships of Ti-6Al-4V Parts Fabricated by Selective Laser Melting

  • Mezzetta, Justin;Choi, Joon-Phil;Milligan, Jason;Danovitch, Jason;Chekir, Nejib;Bois-Brochu, Alexandre;Zhao, Yaoyao Fiona;Brochu, Mathieu
    • International Journal of Precision Engineering and Manufacturing-Green Technology
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    • v.5 no.5
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    • pp.605-612
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    • 2018
  • This work investigates the relationships between the static mechanical properties of Ti-6Al-4V manufactured through selective laser melting (SLM) and post-process heat treatments, namely stress relieve, annealing and hot isostatic pressing (HIP). In particular, Ti-6Al-4V parts were fabricated in three different build orientations of X, Z, and $45^{\circ}$ to investigate the multi-directional mechanical properties. The results showed that fully densified Ti-6Al-4V parts with densities of up to 99.5% were obtained with optimized SLM parameters. The microstructure of stress relieved and mill annealed samples was dominated by fine ${\alpha}^{\prime}$ martensitic needles. After HIP treatment, the martensite structure was fully transformed into ${\alpha}$ and ${\beta}$ phases (${\alpha}+{\beta}$ lamellar). Within the realm of tensile properties, the yield and ultimate strength values were found statistically similar with respect to the built orientation for a given heat treatment. However, the ductility was found orientation dependent for the HIP samples, where a lower value was observed for samples built in the X direction.

The Fabrication and Grindability of Diamond Wheel Bonded with Heat Resistance Aluminum Alloy (내열 Al합금 본드 다이아몬드 휠의 제조 및 연삭성)

  • 최성국
    • Journal of Powder Materials
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    • v.2 no.2
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    • pp.142-148
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    • 1995
  • 2219 aluminum alloy bonded diamond wheels containing intermetallic compounds were fabricated by powder metallurgy method. Nickel and titanium were added in aluminum matrix piece. The hot pressing condition was $600^{\circ}C$ and 20 Mpa in the furnace of the electric resistance type. The mechanical properties and grinding tests were carried out to confirm the wheel performance. Aluminum oxide ceramics were chosen for use in the grinding tests. The test proved that the heat resistance 2219 aluminum bonded diamond wheel containing 15 wt% nickel and 15 wt% titanium respectively showed the best performance.

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Rejuvenation Technologies for Hot Gas Path Components made of Nickel Based Superalloys (니켈기 초합금 소재 고온부 부품의 재생정비기술)

  • Kang, Sin-Ho;Choi, Heui-Sook;Kim, Dae-Eun
    • Proceedings of the KSME Conference
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    • 2003.11a
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    • pp.424-429
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    • 2003
  • Hot gas path components, which are made of nickel based superalloys, are subject to periodic replacement due to degradation of thermomechanical properties that might bring catastrophic failure during normal operation of gas turbine units. In order to rejuvenate the metallurgical condition of the serviced components, heat treating techniques such as solution annealing and aging heat treatments have widely been employed. However, the effectiveness of those typical heat treatments is not apparent enough in terms of quantitative grounds. On the other hand the demand of the rejuvenation heat treatment and hot isostatic pressing (HIP) have constantly been raised by the end users. Therefore it is necessary to verify how the typical heat treating techniques affect to the aged and degraded material. As the result of experimental work in this study, GTD-111 and GTD-222 Ni-based superalloys were collected and analyzed quantitatively through microscopic observation, microhardness evaluation and creep test.

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Analysis on the Grain Growth of PLZT Ceramics (PLZT세라믹스에서의 입성장 분석)

  • 송병무;김도연
    • Journal of the Korean Ceramic Society
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    • v.25 no.4
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    • pp.329-334
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    • 1988
  • Kinetics of grain growth in PLZT ceramics during isothermal heat treatment and hot-pressing were investigated and the published data on grain growth were reanalyzed. It was found, in many cases, that the errors were introduced by ignoring the initial grain size. The grain growth of PLZT ceramics was confirmed to follow the parabolic normal growth : D2-Do2=Kt.

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A study on the process for the preparation of Ag/Bi-2223 superconducting tapes by powder in tube methoe (분말충진법에 의한 Ag/Bi-2223고온초전도 선재의 제조공정에 관한 연구)

  • Kim, U-Gon;Lee, Ho-Jin;Won, Dong-Yeon;Hong, Gye-Won
    • Korean Journal of Materials Research
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    • v.4 no.4
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    • pp.406-415
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    • 1994
  • The effects of fabrication method and condition on critical current density of Ag sheathed Bi- 2223 superconducting tapes by powder-in-tube method were studied. The highest critical current density (Jc) in the whole process was measured in the repeative heat treatment of 250 hour and mechanical deformation of 2 times. These results are suggested that the high-Tc phase at the heat treatment of 250 hour was superior and the good grain alignment at the mechanical deformation of 2 times was analyzed by XRD pattern. The highest critical current density obtained by pressing method was $1.05\times 10^4A/\textrm{cm}^2$ and $0.78\times 10^4A/\textrm{cm}^2$ in case of rolling method. The multifilamentary wires with 7 and 49 filaments were fabricated to check the applicability of pressing and rolling method for preparing multifilaments wire. The critical current density of 7 filaments tapes prepared by pressing showed $0.45 \times 10^{4}A/\textrm{cm}^2$ and $0.20 \times 10^{4}A/\textrm{cm}^2$ for 49 filaments tapes prepared by rolling.

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Correlation of the 2223 percentage before the first intermediate pressing and the transport property of the fully processed Bi-2223/Ag tapes

  • Jiang, C.H.;Yoo, J.M.;Ko, J.W.;Kim, Y.K.;Chung, H.S.
    • Progress in Superconductivity
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    • v.4 no.1
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    • pp.94-98
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    • 2002
  • Two kinds of multifilament Bi-2223/Ag tapes, which are different in the precursor calcination temperatures, were heat treated for different time (12, 20, 30, 50, 70, or 100 h) firstly to obtain varied B2223 contents, and then followed by the same pressing and sintering cycles. The relation of the 2223 phase contents after the first sintering and the transport property of the fully processed tapes was studied. The results show that 75-80% 2223 phase formed in tapes before the first cold pressing is beneficial to get a high $I_{c}$ in the final tapes. Compensating the total heat treatment time of the tapes first sintered for 20 h to the same length as that first sintered for 50 h in the subsequent sintering stages, different $I_{c}$ enhancements were observed in these two tapes. No improvement on $I_{c}$ was found in the tape made from the powder calcined at higher temperature, whereas for the tape prepared with the lower temperature calcined powder, the $I_{c}$ was increased to the same level as that first sintered for 50 h. The 2223 contents before the intermediate mechanical work is related to the residual reactants, especially to the liquid phase, which is of vital importance to the phase conversion and healing microcracks, meanwhile, to the size and distribution of the non-superconducting secondary phases. The lower temperature calcined powder resulted in slow formation of 2223 phase, but also provided more reactants and liquid phase for the further phase conversion, as a consequence, for the Improvement of $I_{c}$. c/.

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