• Title/Summary/Keyword: heat pressing

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Recyclable Polymeric Composite with High Thermal Conductivity (재활용 가능한 고방열 고분자 복합소재 개발)

  • Shin, Haeun;Kim, Chae Bin;Ahn, Seokhoon;Kim, Doohun;Lim, Jong Kuk;Goh, Munju
    • Composites Research
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    • v.32 no.6
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    • pp.319-326
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    • 2019
  • To address tremendous needs for developing efficiently heat dissipating material with lightweights, a new class of polymer possessing recyclable and malleable characteristics was synthesized for incorporating model functional hexagonal boron nitride (h-BN) filler. A good interfacial affinity between the polymer matrix and the filler along with shear force generated upon manufacturing the composite yielded the final product bearing highly aligned filler via simple hot pressing method. For this reason, the composite exhibited a high thermal conductivity of 13.8 W/mK. Moreover, it was possible to recover the h-BN from the composite without physical/chemical denaturation of the filler by chemically depolymerizing the matrix, thus the recovered filler can be re-used in the future. We believe this polymer could be beneficial as matrix for incorporating many other functional fillers, thus they may find applications in various polymeric composite related fields.

Vapor Permeation Characteristics of TiO2 Composite Membranes Prepared on Porous Stainless Steel Support by Sol-Gel Method

  • Lee, Yoon-Gyu;Lee, Dong-Wook;Kim, Sang-Kyoon;Sea, Bong-Kuk;Youn, Min-Young;Lee, Kwan-Young;Lee, Kew-Ho
    • Bulletin of the Korean Chemical Society
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    • v.25 no.5
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    • pp.687-693
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    • 2004
  • Composite membranes with a titania layer were prepared by soaking-rolling method with the titania sol of nanoparticles formed in the sol-gel process and investigated regarding the vapor permeation of various organic mixtures. The support modification was conducted by pressing $SiO_2$ xerogel of 500 nm in particle size under 10 MPa on the surface of a porous stainless steel (SUS) substrate and designed the multi-layered structure by coating the intermediate layer of ${\gamma}-Al_2O_3$. Microstructure of titania membrane was affected by heat-treatment and synthesis conditions of precursor sol, and titania formed at calcination temperature of 300$^{\circ}C$ with sol of [$H^+$]/[TIP]=0.3 possessed surface area of 210 $m^2$/g, average pore size of 1.25 nm. The titania composite membrane showed high $H_2/N_2$ selectivity and water/ethanol selectivity as 25-30 and 50-100, respectively. As a result of vapor permeation for water-alcohol and alcohol-alcohol mixture, titania composite membrane showed water-permselective and molecular-sieve permeation behavior. However, water/methanol selectivity of the membrane was very low because of chemical affinity of permeants for the membrane by similar physicochemical properties of water and methanol.

Investigation of a Novel Rubber-Forming Process Inducing Uniform Surface Pressure for the Fabrication of a Thin Bent Plate with Corrugated Structure (균일압력 유도에 의한 꺾임 구조를 가진 미세주름 박판구조물 성형을 위한 고무성형 공정연구)

  • Kim, Min-Hoon;Park, Sang-Hu;Jeong, Ho-Seung;Cho, Jong-Rae;Ha, Man-Yeung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.35 no.8
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    • pp.933-940
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    • 2011
  • Thin sheets with a corrugated structure are generally used for the fabrication of heat exchangers for electronics, airplanes, and vehicles. However, it is difficult to fabricate corrugated structures, especially those with a bent angle, using the conventional stamping process because of its intrinsic formation mechanism. We propose a novel rubber-forming process for the effective pressing of the both tilted sides of a plate under the same pressure to form exact corrugated shapes. We use finite element analysis and experiments to study the rubber-forming process parameters, and we evaluate the maximum allowable bent angle for high-quality formation. We show that the proposed method is effective for the fabrication of bent plates with low cost.

Thermal Emissivity Changes as a Function of Degree of Flakes Alignment on the Graphite Surface (흑연표면의 열방사율 측정시 결정립 배향성의 영향)

  • Roh, Jae-Seung;Ahn, Jai-Sang;Kim, Beom-Jun;Jeon, Ho-Yeon;Seo, Seung-Kuk;Kim, Suk-Hwan;Lee, Sang-Woo
    • Journal of the Korean institute of surface engineering
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    • v.42 no.2
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    • pp.95-101
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    • 2009
  • This study is the research on the thermal emissivity depending on the bulk graphite's alignment degree. Bulk graphites were manufactured by uni-axial pressing and subsequent heat treatment of natural graphite flakes with organic binder. The samples were prepared to be $0^{\circ}$ (relative to the 002 c-face), $45^{\circ}$, and $90^{\circ}$ (relative to the 100 a-face) for measuring alignment degree. The alignment degree of the sample was measured by XRD. The thermal emissivity was measured by infrared thermal image camera at $100^{\circ}C$ and compared with the value obtained by Infrared spectroscopy. The alignment degree and thermal emissivity of $0^{\circ}$ sample were measured to be 0 and 0.70 respectively. And those of $90^{\circ}$ sample were 0.73 and 0.80 respectively. The emissivity value was correlated with obtained by IR spectroscopy. Therefore it was considered that the thermal emissivity of the bulk graphite is correlated with the alignment degree.

Effect of Cobalt Contents on the Microstructure and Charpy Impact Properties of Ferritic/martensitic Oxide Dispersion Strengthened Steel (페라이트/마르텐사이트계 산화물분산강화강의 미세조직 및 샤르피 충격특성에 미치는 코발트 함량의 영향)

  • Kwon, Daehyun;Noh, Sanghoon;Lee, Jung Gu
    • Journal of Powder Materials
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    • v.27 no.4
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    • pp.311-317
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    • 2020
  • In this study, the effects of Co content on the microstructure and Charpy impact properties of Fe-Cr-W ferritic/martensitic oxide dispersion strengthened (F/M ODS) steels are investigated. F/M ODS steels with 0-5 wt% Co are fabricated by mechanical alloying, followed by hot isostatic pressing, hot-rolling, and normalizing/tempering heat treatment. All the steels commonly exhibit two-phase microstructures consisting of ferrite and tempered martensite. The volume fraction of ferrite increases with the increase in the Co content, since the Co element considerably lowers the hardenability of the F/M ODS steel. Despite the lowest volume fraction of tempered martensite, the F/M ODS steel with 5 wt% Co shows the highest micro-Vickers hardness, owing to the solid solution-hardening effect of the alloyed Co. The high hardness of the steel improves the resistance to fracture initiation, thereby resulting in the enhanced fracture initiation energy in a Charpy impact test at - 40℃. Furthermore, the addition of Co suppresses the formation of coarse oxide inclusions in the F/M ODS steel, while simultaneously providing a high resistance to fracture propagation. Owing to these combined effects of Co, the Charpy impact energy of the F/M ODS steel increases gradually with the increase in the Co content.

Effects of Alloying Elements on the Microstructure and Tensile Properties of Rapidly Solidified Al-Mg Alloys (급속응고한 Al-Mg 합금의 미세조직 및 인장특성에 미치는 첨가원소의 영향)

  • Park, Hyun-Ho;Park, Chong-Sung;Kim, Myung-Ho
    • Journal of Korea Foundry Society
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    • v.17 no.4
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    • pp.356-364
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    • 1997
  • In order to study effects of Cu and Be on the microstructure and tensile properties of rapidly solidified Al-Mg alloys, Al-Mg-Cu-Be alloys have been rapidly solidified by inert gas atomization process. Microstructure of rapidly solidified Al-Mg-Cu-Be powders exhibited refinement and good dispersion of Be particles as increasing of solidification rate. Solidification rate of atomized powders was estimated to be about $5{\times}10^{3{\circ}}C/s$. Inert gas atomized Al-Mg-Cu-Be powders were hot-processed by vacuum hot pressing at $450^{\circ}C$ under 100 MPa and hot extruded with reduction ratio in area of 25: 1 at $450^{\circ}C$. The extruded Al-Mg-Cu-Be powders consisted of recrystallized fine Al grains and homogeneously dispersed fine Be particles, and exhibited improved tensile properties with increase in Cu content. $Al_2CuMg$ compounds precipitated in grain and grain boundaries of Al-Mg-Cu-Be alloys with aging heat treatment after solution treatment. Hardness and tensile properties were improved by increasing Cu content and Be addition. Compared with extruded Al-Mg-Cu powders, the extruded Al-Mg-Cu-Be powders exhibited finer recrystallized grains and improved tensile properties by dispersion hardening of Be and subgrain boundaries pinned by fine Be particles. After aging treatment, hardness and tensile properties were improved due to restricted precipitation by increasing of dislocation density around Be particles in matrix.

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A Review of the Chinese Traditional Medicine Thesis on the Treatment of Hyperopia (원시(遠視) 치료에 관한 중의(中醫) 논문 고찰)

  • Kang, Jae-Hyun;Hong, Jin-Young;Seo, Hyung-Sik
    • The Journal of Korean Medicine Ophthalmology and Otolaryngology and Dermatology
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    • v.34 no.4
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    • pp.37-48
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    • 2021
  • Objectives : The purpose of this study is to investigate treatment trends on hyperopia of chinese traditional medicine. Methods : We searched papers using CNKI and Pubmed. The keyword used on searching was 'Hyperopia' combined with 'Chinese medicine', 'Acupuncture' and 'herbal medicine'. Searching duration was not specified. The search was conducted from January 2020 to July 2021, and the final selected papers were from 1983 to 2014. Results : Studies found in CNKI were 27 and 20 sutdies were excluded. Studies found in Pubmed were 57 and 57 studies were excluded. Finally 7 sutdies were selected and analyzed. Five studies of selected ones were case reports and two were review papers. Among 5 case reports, two of them used herbal medicine with pressing auricular acupoints with beans. Another one used electronic plum acupuncture only. Another one used acupuncture with electronic heat and pulsed current stimulation. The other one compared acupuncture alone and acupuncture combined with massage. All studies report high efficacy rates on treatments. Conclusions : According to this study we found the possibility of acupuncture and herbal medicine on hyperopia. We expect that further studies will be conducted and the results of them could be actively applied to clinical treatments.

Characteristics of Electric Resistance Dual Spot Welding Process of AZ31 Magnesium Alloy Sheets (AZ31 마그네슘 합금 판재의 전기저항 이중 스폿용접 특성)

  • Sun, Xiao-Guang;Jin, In-Tai
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.21 no.3
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    • pp.1-11
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    • 2022
  • In this study, an electric resistance dual-spot welding process using a copper electrode inserted in a heating electrode is suggested for the spot welding of AZ31 magnesium sheets. This spot-welding process involves two heating methods for welding at the interfacial zone between the magnesium sheets, one of which is the heating method by thermal conduction from the heating electrode heated by the welding current induced to the steel electrode, and the other heating method uses the electric resistance between the contacted surfaces of the two sheets by the welding current induced to the copper electrode. This welding process includes the welding variables, such as the current induced in the heating electrode and the copper electrode, and the outer diameters of the heating electrode. This is because the heat conducted from the heating electrode can be maintained at a higher temperature in the welding zone, which has a slow cooling effect on the nugget of the melted metal after the welding step. The pressure exerted during the pressing of the magnesium sheets by the heating electrode can be increased around the nugget zone at the spot-welding zone. Thus, it not only reduces the warping effect of the elastoplastic deformation of sheets, but also the corona bond can make it less prone to cracking at the welded zone, thereby reducing the number of nuggets expelled out of the corona bond. In conclusion, it was known that an electric resistance dual spot welding process using the copper electrode inserted in the heating electrode can improve the welding properties in the electric resistance spot welding process of AZ31 magnesium sheets.

Superconducting Characteristics of Melt Spun $YBa_2Cu_3Ag_{15}$ and $YbBa_2Cu_3Ag_x$ (x=5, 16 and 53) Microcomposites (융체방사법으로 제작한 $YBa_2Cu_3Ag_{15}$$YbBa_2Cu_3Ag_x$ (x=5, 16 and 53)미세복합재의 초전도 특성)

  • Song, Myeong-Yeop
    • Korean Journal of Materials Research
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    • v.5 no.7
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    • pp.880-887
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    • 1995
  • Melt spun YB $a_2$C $u_3$A $g_{15}$ and YbB $a_2$C $u_3$A $g_{x}$(x=5, 16 and 53) precursor alloy ribbons were oxidized at 263~322$^{\circ}C$, and heat-treated at 872~89$0^{\circ}C$ under 1.0atm oxygen pressure. In addition, about ten ribbons were stacked and coupled by pressing, and then followed the same heat treatment. YB $a_2$C $u_3$ $O_{7-{\delta}}$(1-2-3) or YbB $a_2$C $u_3$ $O_{7-{\delta}}$(1-2-3) phase was formed in both the ribbons and the multilayered specimens. The formed 1-2-3 phases were not texturized in all the ribbons, but slightly texturized in the multilayered specimens. $J_{c}$ was not achieved in all the ribbons at 77K and zero magnetic field. Among the multilayered specimens, YB $a_2$C $u_3$A $g_{15}$ and YbB $a_2$C $u_3$A $g_{16}$ showed $J_{c}$ of 260 and 180A/$\textrm{cm}^2$, respectively. YB $a_2$C $u_3$A $g_{15}$ and YbB $a_2$C $u_3$A $g_{16}$ are considered to be the appropriate compositions in producing textured superconducting oxides with improved $J_{c}$ by pressing. Onset critical temperature ( $T_{on}$ ) of the multilayered YB $a_2$C $u_3$A $g_{15}$ was 92K while those of YbB $a_2$C $u_3$A $g_{x}$(x=5 , 16 and 53) were 88~90K. , 16 and 53) were 88~90K.

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Brewing and Quality Characteristics of New Grape Cultivar 'Okrang' Wine in Fermentation Process (포도 신품종 '옥랑'을 이용한 와인 발효 및 품질 특성)

  • Park, Hye Jin;Choi, Wonil;Park, Jung-Mi;Jeong, Changwon;Kim, Sidong;Yoon, Hyang-Sik
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.46 no.5
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    • pp.622-629
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    • 2017
  • This study was carried out to investigate the effects of cold maceration and heat treatment prior to alcohol fermentation on the quality characteristics of wine made from Okrang grape cultivar. The results of this study show that alcohol contents of wines increased as fermentation period increased, whereas $^{\circ}Brix$ values decreased. The pH levels of wines ranged from 3.17 to 3.42 while the total acidities of wines ranged from 0.49~0.99%. The free sugar contents of wines tended to decrease as fermentation period increased. In particular, free sugar content of wine pre-treated at low temperature prior to alcohol fermentation slowly. Total polyphenol content of wine heat-treated prior to alcohol fermentation was higher than those of other wines and reached a maximum value after fermentation for 2 days. Campbell Early wine showed the strongest antioxidant effect, measured based on DPPH free radical scavenging activity, followed by Okrang wine pressing after fermentation. These results indicate that pre-treatment before wine fermentation greatly affects wine quality and biofunctional activities.