• Title/Summary/Keyword: hardening effects

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Mechanical Properties of Elastomeric Composites with Atmospheric-Pressure Flame Plasma Treated Multi-Walled Carbon Nanotubes and Carbon Black (대기압 화염 플라즈마 처리한 다중벽 탄소나노튜브 및 카본블랙 강화 고무복합재료의 기계적 특성 연구)

  • Sung, Jong-Hwan;Lee, Dong-Joo;Ryu, Sang-Ryeoul;Cho, Yi-Seok
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.9
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    • pp.1209-1215
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    • 2010
  • The effects of multi-walled carbon nanotube (MWCNT) content, carbon black (CB) content, atmospheric-pressure flame plasma (APFP) treatment, and acid treatment on the mechanical properties of elastomeric composites were investigated. For pure or filled rubbers with the given amount of CB (20 and 40 phr), the tensile strength and modulus of the elastomeric composites increase similarly with the MWCNT content. A composite with APFP-treated MWCNTs shows a hardening effect (high strength, high modulus, and high ductility) unlike the one with untreated MWCNTs. On the other hand, a composite with APFP-treated CB shows a softening effect (high strength, low modulus, and high ductility), which is unlike a composite with untreated CB. As the refluxing time increases from 1 h to 2 h and the sulfuric acid concentration increases from 60% to 90%, the tensile strength and modulus of a composite decrease. Thus, it is found that the MWCNT content, CB content, APFP treatment, sulfuric acid concentration, and refluxing time have an important effect on the mechanical properties of NBR composites.

Effect of Press Temperature and Time on Physical Properties of Larch Particleboard (압체온도(壓締温度)와 시간(時間)이 낙엽송(落葉松) 파티클 보오드의 물리적(物理的) 특성(特性)에 미치는 영향(影響))

  • Lee, Phil Woo;Chung, Gyun
    • Journal of Korean Society of Forest Science
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    • v.63 no.1
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    • pp.12-20
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    • 1984
  • This research was performed to estimate the properties of particleboard based on the press time and temperature which was made of chip of larch that grows in Korea. The results in this study were as follows: 1) Even though the chips, 1:1-35 ratio between length and thickness, are relatively bad condition, the surface smoothness that can easily spread the adhesive evenly and thoroughly and bonding ability of chips can give proper physical properties. 2) It shows more mechanical properties at the press time of 10 min. in MOR (Modulus of Rupture), MOE (Modulus of Elasticity) and SHA (Screw Holding Ability). 3) It is not significant according to the press time 20 min. in MOR, IBS (Internal Bonding Strength) and SHA, for the reciprocal actions between the accelerating aging effect of chip and the softening effect of adhesion are occured. 4) IBS is rising according to the increasing temp at the press time of 10 min. Because it needs to transfer the plate heat to make the proper hardening temp. In the layer. 5) The heat treatment effects have greatly influenced the stahility of dimension by falling the absorption, anisotropy and inhomegenity. As a result of these the values of thickness and linear expansion ratio were respectively dropped by the increase of press temp and the time and so did absorption.

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Application of Slow-Freezing Cryopreservation Method for the Conservation of Diverse Potato (Solanum tuberosum L.) Genotypes

  • Zhao Mei-Ai;Dhital Shambhu P.;Fang Yi-Lan;Khu Dong-Man;Song Ye-Su;Park Eung-Jun;Kang Chang-Won;Lim Hak-Tae
    • Journal of Plant Biotechnology
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    • v.7 no.3
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    • pp.183-186
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    • 2005
  • Cryopreservation has been recognized as a practical and efficient tool for the long-term storage of vegetatively propagated plants. This study was conducted to investigate the effects of slow-freezing techniques on the cryopreservation of potato. In vitro plantlets of the potato genotypes of 'Atlantic', 'Superior’, 'Namseo', 'J138', and 'CTO5-5' were cold acclimated, and the excised axillary buds were precultured, osmoprotected, exposed to plant vitrification solution, frozen slowly to $-40^{\circ}C$ and then rapidly plunged into liquid nitrogen, thawed and finally plated on the regeneration medium. It was found that the higher the sucrose concentrations in the subculture medium of donor plantlets, the higher the survival rates of shoot tips after cryopreservation, and the highest survival (20%) was observed in the medium added with 0.25 M sucrose. As for the effect of cooling, $0.3^{\circ}C/min$ cooling speed showed the highest survival (25%). Different varieties showed different responses over different cryopreservation treatments. Survival rate was increased by slow-freezing technique method as compared with that of the basic cryopreservation method of vitrification alone in the diverse potato genotypes. Leaf and tuber morphologies of potatoes regenerated after cryopreservation using slow freezing technique were similar to those derived from the in vitro stock plantlets.

Evaluation of the Properties of an Environment-Friendly De-icing Agent Based on Industrial By-Products (산업부산물을 활용한 친환경제설제의 특성평가)

  • Heo, Hyung-Seok;Lee, Byung-Jae
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.6
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    • pp.132-139
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    • 2017
  • A huge amount of de-icing agent is sprayed during winter to promote traffic safety in cold regions, and the quantity of de-icing agent sprayed has increased each year. The main ingredients in commonly used de-icing agents are chlorides, such as calcium chloride($CaCl_2$) and sodium chloride(NaCl). While calcium chloride is mostly used in Korea and sodium chloride is usually used in the U.S. and Japan, all de-icing agents include chloride ions. The chlorides included in sprayed calcium chloride-based de-icing agents have severe adverse effects, including the corrosion of reinforcing steels through salt damage by infiltrating into road structures, reduced structural performance of pavement or damage to bridge structures, and surface scaling, in combination with freezing damage in winter, as well as water pollution. In addition, the deterioration of paved concrete road surface that occurs after the use of calcium chloride-based de-icing agent accelerates the development of visual problems with traffic structures. Therefore, the present study was performed to prepare an environment-friendly liquid de-icing agent through a reaction between waste organic acids and calcium-based by-products, which are industrial by-products, and to analyze the properties of the de-icing agent in order to evaluate its applicability to road facilities.

Study on Viscoelastic Properties of Rice Plant (벼줄기의 점탄성(粘彈性) 특성(特性)에 관(關)한 연구(硏究))

  • Huh, Yun Kun
    • Korean Journal of Agricultural Science
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    • v.13 no.2
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    • pp.255-264
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    • 1986
  • The objectives of this study were to examine the viscoelastic behaviour of stem samples of rice in force-relaxation and rheological model to represent its relaxation behaviour, and to study the effects of rate of deformation and initial deformation on the relaxation time. The results were as follows; 1. In the process of loading and unloading, there is any plastic deformation so called elasto-plastic hysterisis. 2. Loading and unloading of stem of rice for several cycles has also shown the reduction of plastic or residual deformation and work hardening. 3. The relaxation behaviour of stem of rice in compression may be described by a generalized Maxwell model consisting of three Maxwell units in parallel. The rheological equation of such a model is given as $$F(t)=C_1e^{{-t/{\tau}}_1}+C_2e^{{-t/{\tau}}_2}+C_3e^{{-t/{\tau}}_3}$$ 4. Force relaxation always increased with increasing rates of deformation and initial deformation.

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Life Prediction of Low Cycle Fatigue for Ni-base Superalloy GTD111 DS at Elevated Temperature (Ni기 초내열합금 GTD111 DS의 고온 저주기 피로수명 예측)

  • Kim, Jin Yeol;Yoon, Dong Hyun;Kim, Jae Hoon;Bae, Si Yeon;Chang, Sung Yong;Chang, Sung Ho
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.41 no.8
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    • pp.765-770
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    • 2017
  • GTD111 DS of nickel base superalloy has been used for gas turbine blades. In this study, low cycle fatigue test was conducted on the GTD111 DS alloy by setting conditions similar to the real operating environment. The low cycle fatigue tests were conducted at room temperature, $760^{\circ}C$, $870^{\circ}C$, and various strain amplitudes. Test results showed that fatigue life decreased with increasing total strain amplitude. Cyclic hardening response was observed at room temperature and $760^{\circ}C$; however, tests conducted at $870^{\circ}C$ showed cyclic softening response. Stress relaxation was observed at $870^{\circ}C$ because creep effects occurred from holding time. A relationship between fatigue life and total strain range was obtained from the Coffin-Manson method. The fratography using a SEM was carried out at the crack initiation and propagation regions.

Changes in Growth, Active Ingredients, and Rheological Properties of Greenhouse-cultivated Ginseng Sprout during its Growth Period (하우스에서 재배된 새싹인삼의 재배시기별 생육, 유효성분 및 물성의 변화)

  • Seong, Bong Jae;Kim, Sun Ick;Jee, Moo Geun;Lee, Hee Chul;Kwon, A Reum;Kim, Hyun Ho;Won, Jun Yeon;Lee, Ka Soon
    • Korean Journal of Medicinal Crop Science
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    • v.27 no.2
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    • pp.126-135
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    • 2019
  • Background: The ginseng ginsenosides, which have various physiological activities, are known to be more abundant in the leaves than in the roots, and the consumers' interest in ginseng sprout as a functional vegetable has been increasing. Methods and Results: The aim of this study was to investigate the effects of growth period on growth properties, active ingredients and rheology of ginseng sprouts cultivated in a non-heated greenhouse equipped with a shade net for 60 days, starting from the end of May to the middle of July. The chlorophyll content of the leaves decreased, but their length and width increased with increasing cultivation days. In particular, growth increased significantly until 40 days, but only slightly after 50 days. The stem length did not increase greatly from the 20 th to the 30 th day of cultivation, but increased significantly from the 30 th to the 40 th day, and then further increased gradually. The weight of the leaves, stems, and roots increased slightly, but not change significantly. After 40 days of cultivation, the total ginsenoside content increased by 1.07 times in the leaves and decreased by 0.80 times in the roots with increasing cultivation days. The leaf contents of ginsenosides $Rg_1$, Re, $Rb_1$, Rc, $F_3$ and $F_4$ increased with increasing cultivation days. The rheological properties of ginseng sprout showed the greatest influence on stem hardening with increasing cultivation days. Conclusions: Therefore, based on the growth characteristics, active ingredients and physical properties, 40 days after sowing was considered to be an appropriate harvesting time for ginseng sprouts.

Simulation of the effect of inclusions length and angle on the failure behavior of concrete structure under 3D compressive test: Experimental test and numerical simulation

  • Mohammad Saeed, Amini;Vahab, Sarfarazi;Kaveh, Asgari;Xiao, Wang;Mojtaba Moheb, Hoori
    • Steel and Composite Structures
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    • v.46 no.1
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    • pp.53-73
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    • 2023
  • Man-made structure materials like concrete usually contain inclusions. These inclusions affect the mechanical properties of concrete. In this investigation, the influence of inclusion length and inclination angle on three-dimensional failure mechanism of concrete under uniaxial compression were performed using experimental test and numerical simulation. Approach of acoustic emission were jointly used to analyze the damage and fracture process. Besides, by combining the stress-strain behavior, quantitative determination of the thresholds of crack stress were done. concrete specimens with dimensions of 120 mm × 150 mm × 100 mm were provided. One and two holes filled by gypsum are incorporated in concrete samples. To build the inclusion, firstly cylinder steel tube was pre-inserting into the concrete and removing them after the initial hardening of the specimen. Secondly, the gypsum was poured into the holes. Tensile strengths of concrete and gypsum were 2.45 MPa and 1.5 MPa, respectively. The angle bertween inclusions and axial loadind ary from 0 to 90 with increases of 30. The length of inclusion vary from 25 mm to 100 mm with increases of 25 mm. Diameter of the hole was 20 mm. Entirely 20 various models were examined under uniaxial test. Simultaneous with experimental tests, numerical simulation (Particle flow code in two dimension) were carried out on the numerical models containing the inclusions. The numerical model were calibrated firstly by experimental outputs and then failure behavior of models containing inclusions have been investigated. The angle bertween inclusions and axial loadind vary from 0 to 90 with increases of 15. The length of inclusion vary from 25 mm to 100 mm with increases of 25 mm. Entirely 32 various models were examined under uniaxial test. Loading rate was 0.05 mm/sec. The results indicated that when inclusion has occupied 100% of sample thickness, two tensile cracks originated from boundaries of sample and spread parallel to the loading direction until being integrated together. When inclusion has occupied 75% of sample thickness, four tensile cracks originated from boundaries of sample and spread parallel to the loading direction until being integrated together. When inclusions have occupied 50% and 25% of sample thickness, four tensile cracks originated from boundaries of sample and spread parallel to the loading direction until being integrated together. Also the inclusion was failed by one tensile crack. The compressive strength of samples decease with the decreases of the inclusions length, and inclusion angle had some effects on that. Failure of concrete is mostly due to the tensile crack. The behavior of crack, was affected by the inclusion length and inclusion number.

Effects of Surface Finishes on the Low Cycle Fatigue Characteristics of Sn-based Pb-free Solder Joints (금속패드가 Sn계 무연솔더의 저주기 피로저항성에 미치는 영향)

  • Lee, Kyu-O;Yoo, Jin
    • Journal of the Microelectronics and Packaging Society
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    • v.10 no.3
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    • pp.19-27
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    • 2003
  • Surface finishes of PCB laminates are important in the solder joint reliability of flip chip package because the types and thicknesses of intermetallic compound(IMC), and compositions and hardness of solders are affected by them. In this study, effects of surface finishes of PCB on the low cycle fatigue resistance of Sn-based lead-free solders; Sn-3.5Ag, Sn-3.5Ag-XCu(X=0.75, 1.5), Sn-3.5Ag-XBi(X=2.5, 7.5) and Sn-0.7Cu were investigated for the Cu and Au/Ni surface finish treatments. Displacement controlled room temperature lap shear fatigue tests showed that fatigue resistance of Sn-3.5Ag-XCu(X=0.75, 1.5), Sn-3.5Ag and Sn-0.7Cu alloys were more or less the same each other but much better than that of Bi containing alloys regardless of the surface finish layer used. In general, solder joints on the Au/Ni finish showed better fatigue resistance than those on the Cu finish. Cross-sectional fractography revealed microcracks nucleation inside of the interfacial IMC near the solder mask edge, more frequently on the Cu than the Au/Ni surface finish. Macro cracks followed the solder/IMC interface in the Bi containing alloys, while they propagated in the solder matrix in other alloys. It was ascribed to the Bi segregation at the solder/IMC interface and the solid solution hardening effect of Bi in the $\beta-Sn$ matrix.

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Effects of Accelerated Curing on the Strength of Mortar Using Briquette Ash. (촉진양생(促進養生)이 연탄재를 사용(使用)한 Mortar의 강도(强度)에 미치는 영향(影響))

  • Kim, Seong Wan;Kang, Sin Up;Sung, Chan Yong
    • Korean Journal of Agricultural Science
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    • v.8 no.2
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    • pp.185-194
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    • 1981
  • This study was carried out to determine the effect of accelerated curing on the strength of standard sand mortar and briquette ash mortar. The standard sand mortars and the briquette ash mortars made by mixture of the standard sand:cement and the briquette ash:cement at the ratio of 2 : 1, 3: 1 and 4 : 1, respectively, were cured at 4 different temperature of $20^{\circ}C$, $60^{\circ}C$, $80^{\circ}C$ and $100^{\circ}C$. The compression and tensil strength of mortars were measured at ${\sigma}_3$, ${\sigma}_7$, ${\sigma}_28$. The results obtained are summarized as follows; 1. At each age of curing and each curing temperature, the compression and tensile strength of the mortars made by the mixture of cement and standard sand was significantly higher than that of the mortars made by the mixture of cement and briquette ash. But the increasing rate of strength in compression and tension was significantly higher at the mortars of cement and briquette ash than those of cement and standard sand. 2. The strength of mortars which showed lower strength than Korean Standard at ordinary curing temperature was significantly increased and showed higher value than Korean Standard by the accelerated curing at high temperature. The increasing rate of strength by the accelerated curing was higher at the mortars containing less amount of cement than those containing more cement. The hardening of the mortars containing less amount of cement was significantly promoted by the accelerated curing in high temperature. 3. When the briquette ash was substituted for the materials of cement mortar, decline of the mortar strength is. unavoidable. But the enhancement of the mortar strength is still expected by the experimental results that the strength of cement-briquette ash mortar showed an increase of 137.6% by the accelerated curing at $60^{\circ}C$, 164.1% at $80^{\circ}C$ C and 183.8% at $100^{\circ}C$, respectively, compared with the strength of mortar cured at $20^{\circ}C$ for 28 days. 4. As the strength of cement briquette mortar is lower than that of cement standard sand mortar, the cement briquette ash mortar is expected to be increased in strength by the accelerated curing at high temperature. The cement briquette mortar is expected to be utilized to the production of secondary mortar goods or the constructions which need low strength of mortar.

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