• 제목/요약/키워드: hard magnetic properties

검색결과 89건 처리시간 0.021초

Purification of Iron Oxides and Application to Magnetic Hard Ferrite

  • Kim, Jeong-Seog;Chou, Kyoung-Ho;Kim, Jai-Young
    • The Korean Journal of Ceramics
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    • 제2권3호
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    • pp.125-130
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    • 1996
  • Hematite iron ore and waste iron oxide sludge containing about 3-5 wt% $SiO_2$ were purified by three types of method developed on the basis of the Bayer process which is known as the purification process of bauxite ore. The basic principle of the developed methods lies in the fact that the impurities contained in the iron oxides, such as $SiO_2$ and $Al_2O_3$ are soluble in the alkaline reagents. Reaction of the raw materials with KOH was done in pressure vessel, at atmospheric pressure, and by both of these two. By the pressure vessel method $SiO_2$ content was reduced to below 0.5 wt% in the waste iron oxide sludge, while, in iron ore, $SiO_2$ remained at 2-3 wt%. The atmospheric pressure reaction rendered the waste iron oxide sludge $SiO_2$ content below 0.5wt% when the reaction temperature increased to above 90$0^{\circ}C$. The combined method of two previous methods was the most effective process and rendered the refined iron oxide about 300-400ppm of $SiO_2$. Using some refined iron oxides, Ba-ferrite was produced and magnetic properties were measured. The highest quality of magnetic properties obtained in this study were Br=2.09 G, bHc=1.99 KOe, iHc=4.54 KOe, $(BH)_{max}$=1.06 MGOe. Effect of sintering condition and chemical composition will be discussed.

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CoP합금의 전기도금 시 NH4Cl의 영향에 관한 연구 (Effect of NH4Cl on the Electrodeposition of Cobalt/Phosphorus Alloy)

  • 이관희;정원용
    • 전기화학회지
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    • 제5권2호
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    • pp.57-61
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    • 2002
  • 본 연구에서는 염화암모늄을 함유한 전해질에서 CoP 자성합금 박막을 전기도금 방식으로 제조하고 염화암모늄의 첨가량이 다른 용액에서의 CV 등 전기화학적인 분석을 통해 핵생성과 결정화(electrocrystallization)에 미치는 영향을 고찰하여 자기적 성질과의 상호관계를 밝히고자 하였다. 용액 중에 첨가된 염화암모늄은 첨가량이 많을수록 분극도를 감소시키고, charge transfer에 의해 electrocrystallization과정을 속도론적으로 제어함으로써 결정립의 크기가 커지고 orientation factor가 증가된다. 이러한 구조적, 결정학적 변화가 CoP 도금층의 자기적 성질을 변화시킴을 관찰하였다.

블록 공중합체를 이용한 CoCrPt 나노점 배열의 자기적 성질 연구 (MAGNETIC PROPERTIES OF CoCrPt NANODOTS ARRAY MADE BY PS-PMMA BLOCK COPOLYMER TEMPLATE)

  • Jeong, Jong-Ryul;Im, Mi-Young;Shin, Sung-Chul;Park, Dae-Geun;Kwon, Ki-Young;Jung, Hee-Tae;Yang, Seung-Man
    • 한국자기학회:학술대회 개요집
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    • 한국자기학회 2002년도 동계연구발표회 논문개요집
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    • pp.34-35
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    • 2002
  • CoCrPt alloy films are attracting wide attention for applications to high-density magnetic recording media and hard magnetic layer in spin valve structure due to their high coercivity and strong magnetocrystalline anisotropy. Diblock copolymer templates are one of the most promising candidates for nanoscale patterning otherwise inaccessible by lithographic procedures [1]. In this study, we have investigated magnetic properties of Co$\sub$68/Cr$\sub$18/Pt$\sub$14/ nanodot arrays made by self-assembling polystyrene-block-methyl methacrylate ((PS-b-PMMA), (Mn = 82.5 Kg/mol, with a 1.12 polydispersity)) diblock copolymer. (omitted)

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하드디스크 DLC 필름의 마찰 마모특성에 대한 온도와 습도의 영향 (Effects of Temperature and Humidity on the Friction and Wear Properties of DLC Film on the Hard Disk)

  • 안준양;김대은
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2001년도 추계학술대회논문집A
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    • pp.876-881
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    • 2001
  • DLC(Diamond-like carbon) films possess high hardness, low friction coefficient, and good wear resistance. Due to these properties, DLC films have been used extensively in magnetic hard disk industry. The objective of the present study was to investigate the influence of environmental condition on the tribological behavior of DLC coated hard disk. It is found that the tribological characteristics of DLC films are strongly affected by relative humidity and temperature. Specifically, the friction coefficient increases with increase in temperature at relative humidity of 50%. However, at 20% and 85% RH the effect of temperature was not significant. Also, the degree of wear could be observed using an AFM.

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The Influence of Dehydrogenation Speed on the Microstructure and Magnetic Properties of Nd-Fe-B Magnets Prepared by HDDR Process

  • Cha, Hee-Ryoung;Yu, Ji-Hun;Baek, Youn-Kyoung;Kwon, Hae-Woong;Kim, Yang-Do;Lee, Jung-Goo
    • Journal of Magnetics
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    • 제19권1호
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    • pp.49-54
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    • 2014
  • The influence regarding the dehydrogenation speed, at the desorption-recombination state during the hydrogenation-disproportionation-desorption-recombination (HDDR) process, on the microstructure and magnetic properties of Nd-Fe-B magnetic powders has been studied. Strip cast Nd-Fe-B-based alloys were subjected to the HDDR process after the homogenization heat treatment. During the desorption-recombination stage, both the pumping speed and time of hydrogen were systematically changed in order to control the speed of the desorption-recombination reaction. The magnetic properties of HDDR powders were improved as the pumping speed of hydrogen at the desorption-recombination stage was decreased. The lower pumping speed resulted in a smaller grain size and higher DoA. The coercivity and the remanence of the 200-300 ${\mu}m$ sized HDDR powder increased from 12.7 to 14.6 kOe and from 8.9 to 10.0 kG, respectively. In addition, the remanence was further increased to 11.8 kG by milling the powders down to about 25-90 ${\mu}m$, resulting in $(BH)_{max}$ of 28.8 MGOe.

Electron Holography of Advanced Nanomaterials

  • Shindo, D.;Park, H.S.;Kim, J.J.;Oikawa, T.;Tomita, T.
    • Applied Microscopy
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    • 제36권spc1호
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    • pp.63-69
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    • 2006
  • By utilizing a field emission gun and a biprism installed on a transmission electron microscope (TEM), electron holography is extensively carried out to visualize the electric and magnetic fields of nanomaterials. In the electric field analysis, the distribution of electric potential in a sharp tip made of W coated with $ZrO_2$ is visualized by applying the voltage to the tip. Denser contour lines due to the electric potential are observed with an increase in the bias voltage. In the magnetic field analysis by producing the strong magnetic field with a sharp magnetic needle made of a permanent magnet, the in situ experiment is carried out to investigate the magnetization of hard magnetic materials. The results of these experiments clearly demonstrate that electron holography is a promising advanced transmission electron microscopy technique to characterize the electric and magnetic properties of nanomaterials.

강자성층 사이에 초연자성 NiFeCuMo 중간층을 삽입한 3층 박막구조의 자기적 특성 (Magnetic Properties of Three-layered Ferromagnetic Films with a NiFeCuMo Intermediately Super-soft Magnetic Layer)

  • 최종구;이상석
    • 한국자기학회지
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    • 제20권4호
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    • pp.129-133
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    • 2010
  • 초연자성을 띠는 코네틱(Conetic; NiFeCuMo) 박막을 상호 중간층으로 강자성체인 CoFe 또는 NiFe 박막 사이에 삽입한 코닝 유리(Corning glass)/Ta(5 nm)/[CoFe or NiFe(5 nm-t/2)]/NiFeCuMo(t = 0, 4, 6, 8, 10 nm)/[CoFe or NiFe(5 nm-t/2)]/Ta(5 nm) 3층 박막구조에 대한 자기적 특성을 조사하였다. CoFe와 NiFe 박막의 자기적 특성은 박막의 두께에 따라 크게 결정되므로 자화 곤란축과 자화 용이축으로 측정된 이방성 자기저항 곡선으로부터 얻은 보자력과 자화율을 각각 비교하였다. 특히 3층 박막구조에서 NiFe 박막 사이에 자유층으로 NiFeCuMo 박막을 삽입하면 높은 자기저항비를 유지하면서 향상된 자장감응도를 유지하는 고감도 바이오센서용 거대자기저항-스핀밸브(giant magnetoresistive-spin valves; GMR-SV) 및 자기터널접합(magnetic tunnel junction; MTJ) 소자로 활용할 수 있다.

자성연마슬러리를 이용한 초미립 초경합금(WC-Co 18%)의 나노급 경면가공 특성 (Machining Properties to Nano-Level Mirror Surface Finishing for Fine Grained WC-Co 18% Alloy using Magnetic Polishing Slurry)

  • 곽태수
    • 한국세라믹학회지
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    • 제46권1호
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    • pp.102-107
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    • 2009
  • This study has been focused on an effective surface finishing method combining ELID (ELectrolytic In-process Dressing) and MAP (Magnetic Assisted Polishing) for the nano-precision mirror grinding of glass-lens molding mould. ELID grinding is an excellent technique for mirror grinding of various advanced metallic or nonmetallic materials. A polishing process is also required for elimination of scratches present on ELID grinded surfaces. MAP has been used as polishing method due to its high polishing efficiency and superior surface quality. It also presents some techniques for achieving the nanometer roughness of the hard material such as WC-Co, which are extensively used in precision tooling material.