• 제목/요약/키워드: grain-size distribution

검색결과 651건 처리시간 0.024초

기계적 밀링법으로 제조된 마그네슘 분말의 밀링시간에 따른 미세구조 변화와 부식거동 (Corrosion Behavior and Microstructural Evolution of Magnesium Powder with Milling Time Prepared by Mechanical Milling)

  • 안진우;황대연;김긍호;김혜성
    • 대한금속재료학회지
    • /
    • 제49권6호
    • /
    • pp.454-461
    • /
    • 2011
  • In this study, the relationship between corrosion resistance and microstructural characteristics such as grain size reduction, preferred orientation, and homogenous distribution of elements and impurity by mechanical milling of magnesium powder was investigated. Mechanical milling of pure magnesium powder exhibited a complex path to grain refinement and growth together with preferred orientation reversal with milling time. It was also found that anisotropic formation of dislocation on the basal plane of magnesium was initially the dominant mechanism for grain size reduction. After 60 hrs of milling, grain coarsening was observed and interpreted as a result of the strain relaxation process through recrystallization. In spite of the finer grain size and strong (002) texture developed in the sample prepared by spark plasma sintering at $500^{\circ}C$ for 5 min after mechanical milling for 2hrs, the sample showed a higher corrosion rate. The results from this study will be helpful for better understanding of the controlling factor for corrosion resistance and behaviors of mechanical milled magnesium powders.

MnO2첨가가 Y2O3 doped BaTiO3 반도체 세라믹스의 소결 및 PTCR특성에 미치는 영향 (Effect of MnO2 Addition on Sintering and PTCR Properties in Y2O3 doped BaTiO3 Semiconducting Ceramics)

  • 이준형;박금덕;김정주;조상희
    • 한국세라믹학회지
    • /
    • 제27권1호
    • /
    • pp.7-12
    • /
    • 1990
  • The influence of MnO2 on the sintering property and PTCR behavior of(Ba0.8Sr0.2)TiO2 has been investigated. And the densities, grain sizes and electrical resitivities of specimens were measured as a function of doping with Mn ion of varying concentration. The density and grain size of the sintered specimens were almost the same regardless of MnO2 addition up to 0.2mol% MnO2. But in the case of 0.25mol% MnO2 addition, abnormal grain growth was appeared. So the grain size distribution was wide and density decreased greatly. The room-temperature resistivity increased as Mn content increased and the temperature coefficient of resistivity was highest in the case of 0.15mol% MnO2 addition.

  • PDF

용융드래그방법으로 제작한 마그네슘합금 박판의 특성에 미치는 기본적인 공정조건 확립 (Establishment of Fundamental Process Conditions on Properties of Magnesium Alloy Thin Plates Fabricated by the Melt Drag Method)

  • 한창석;이찬우
    • 한국재료학회지
    • /
    • 제32권7호
    • /
    • pp.326-331
    • /
    • 2022
  • AZ31 magnesium alloy was used to manufacture a thin plate using a melt drag method. The effects of roll speed, molten metal temperature, and molten metal height, which are the basic factors of the melt drag method, on the surface shape, the thickness of the thin plate, Vickers hardness, and microstructure of the thin plate were investigated. It was possible to manufacture AZ31 magnesium alloy thin plate at the roll speed range of 1 to 90 m/min. The thickness of the thin plate, manufactured while changing only the roll speed, was about 1.8 to 8.8 mm. The shape of the solidified roll surface was affected by two conditions, the roll speed and the molten metal height, and the Vickers hardness of the manufactured magnesium alloy thin plate value ranged from Hv38~Hv60. The microstructure of the thin plate produced by this process was an equiaxed crystal and showed a uniform grain size distribution. The grain size was greatly affected by the contact state between the molten metal and the solidification roll, and the amount of reactive solids and liquids scraped at the same time as the thin plate. The average grain size of the thin plate fabricated in the range of these experimental conditions changed to about 50-300 ㎛.

수축공극크기분포를 이용한 지반의 수리학적 물성치 산정 (Estimating Hydraulic Properties of Soil from Constriction-pore Size Distribution)

  • 신호성
    • 한국지반공학회논문집
    • /
    • 제38권3호
    • /
    • pp.27-34
    • /
    • 2022
  • 지반내 물의 흐름은 입자 사이의 공극 분포에 의존하므로 입자의 크기를 이용한 수리학적 물성치의 예측은 정확도가 낮다. 본 논문은 Silveria의 방법을 이용하여 입도분포곡선으로부터 수축 공극크기분포를 산정하고, 포화-불포화 수리학적 물성치를 산정하는 방법을 제시하였다. 입도분포가 양호한 흙은 단봉의 공극크기분포를 보이고, 입도분포가 불량한 흙은 쌍봉의 공극크기분포를 보였다. 공극크기분포를 이용한 이론적 포화투수계수 모델식 중에서 Marshall 모델이 실내실험결과와 가장 부합되었다. 불포화토 수리해석에 필요한 함수특성곡선과 불포화투수계수에 대한 모델식을 공극크기분포를 이용하여 제안하였다. 개발된 모델식을 다양한 흙에 적용하여 수리학적 물성치의 예측에 적합한 모델을 선정하는 지속적인 연구가 필요하다.

6.4cm 크기의 일방향 성장된Y$Ba_2$$Cu_3$$O_x$ 제조 (Fabrication of 6.4 cm single grain $YBa_2$$Cu_3$$O_x$)

  • 박병삼;한상철;한영희;정년호;윤희중;김경진;성태현;오제명
    • Progress in Superconductivity
    • /
    • 제5권2호
    • /
    • pp.114-117
    • /
    • 2004
  • We fabricated large single grain YBa$_2$Cu$_3$O$_{x}$ (Y-123) superconductors. The single grain Y-123 was grown by top seeded melt growth (TSMG) method. In a conventional box furnace with uniform temperature distribution, it was very difficult to grow large single grain Y-123 superconductors due to the size limitation in growth. To overcome the size limitation, we applied a radial thermal gradient (lower temperature at sample center and higher temperature on the sample edge) to the TSMG process. In this case, large single grain Y-123 could be easily grown. This is attributed that the liquid of the sample edge was maintained at the high temperature compared to the growth front. Using this method, we successfully fabricated a large single grain Y-123 of 6.4 cm X6.4 cm

  • PDF

국내 해안의 해빈-해안사구 지형 및 퇴적물 특성과 입도기반 사구유형 분석 (Morphological and Textural Characteristics of the Beach-dune System in South Korea, with the Possibility of a Dune Type Scheme Based on Grain-size Trend)

  • 류호상;강지현
    • 한국지형학회지
    • /
    • 제27권3호
    • /
    • pp.53-73
    • /
    • 2020
  • Morphology and grain size distribution of coastal dunes should be well documented because they are critical to dune's buffering capacity and resilience against storm surges. The nationwide coastal dune survey produced the dataset, including beach-dune topographic profiles and grain size parameters for frontal beaches, foredunes, and inland dunes. This research investigated the dataset to describe geomorphic and textural properties of coastal dunes: foredune slopes, dune heights above approximately highest high water, mean size, and sorting, together with associated variables of coastal setting that influence coastal dunes. It also explores the possibility of a dune type scheme based on gran size trends. The results are as follows. First, the coast in which dunes are developed is the primary control on foredune morphology and sediment texture. Coastal dunes on the east coast were developed more alongshore rather than inland, with gentler slopes on the higher ground and out of coarser sand. The shore aspect contributes to this pattern because the east coast cannot benefit from prevailing northwesterly. Second, grain size trends from beaches through foredunes to inland dunes were little identified. Third, 12 dune types were identified from 69 dunes, showing the indicative capability for the status of beaches and dunes. We confirmed that the dataset could increase our understanding of the overall characteristics of coastal dune morphology and texture, though there is something to be improved, for example, establishing the refined and comprehensive field survey protocol.

남동광석(Azurite) 원료 천연 광물 안료의 입도분포 특징 (The Characteristics of Particle Size in Natural Mineral Pigment for Azurite Raw Material)

  • 고인희;정혜영;박주현;정서린;조아현
    • 보존과학회지
    • /
    • 제31권4호
    • /
    • pp.331-339
    • /
    • 2015
  • 본 연구에서는 천연 안료 중 남동광(Azurite)으로 제조된 청색계열 안료 입도의 단계별 분포특성을 파악하고자 국내 외 청색계열 안료 57종을 선정, Malvern사의 Mastersizer2000을 이용하여 입도분석을 실시하였다. 실험 결과, 국내 외에서 시판되고 있는 청색 안료 일부를 제외하고는 비교적 단계별 입도 분리가 잘 되어 있으며, 안료의 입도가 작아질수록 Span 값은 증가하고 입도 분포 범위는 넓어지는 특징을 확인할 수 있었다. Friedman and Sanders가 제안한 Grain size를 기준으로 보면 대부분의 안료는 주로 모래와 실트영역에 해당하였으며 B-100은 72.2%가 점토영역에 해당되었고 A-14는 자갈에 해당하는 영역이 2.5%를 차지하였다. 나아가 동일 성분의 안료라 할지라도 입자 크기에 따라 안료의 발색특성이 다르며 흡유량, 비중, 작업성 등 중요물성에 밀접한 영향을 미친다. 이에 대한 추가적 실험이 필요하며 물리적 특성과 입도분포 특징에 대한 정보는 천연 안료의 취급을 위한 기초자료로 활용될 수 있을 것이다.

함평만 조간대 해조류 분포지역의 퇴적 및 저서환경 특성 (Sedimentary and Benthic Environment Characteristics in Macroalgal Habitats of the Intertidal Zone in Hampyeong Bay)

  • 황동운;고병설
    • 한국수산과학회지
    • /
    • 제45권6호
    • /
    • pp.694-703
    • /
    • 2012
  • To understand the characteristics of sedimentary and benthic environments in habitats of naturally-occurring intertidal benthic macroalgae, various geochemical parameters of sediment (grain size, ignition loss [IL], chemical oxygen demand [COD], and acid volatile sulfur [AVS]) and pore water (temperature, salinity, pH, and nutrients) were measured in the southern intertidal zone of Hampyeong Bay at two month intervals from April to October 2009. Ecological characteristics including the distribution and biomass of benthic macroalgae were also investigated. Benthic macroalgae were distributed below 4 to 5 m depth from mean sea level near the lower portion of the intertidal zone where air exposure time is relatively short. The distribution area and biomass of benthic macroalgae gradually decreased during the study period. The surface sediments in the benthic algal region were mainly composed of finer sediments, such as slightly gravelly mud and mud. The temperature, salinity, pH, and nutrient concentrations (except dissolved inorganic nitrogen) in pore water did not differ in regions with and without benthic macroalgae, whereas the mean grain size and the concentrations of IL, COD, and AVS in sediments were much higher in regions harboring benthic macroalgae. The correlation between mean grain size and IL in sediments displayed two distinct gradients and the slope was much steeper in regions harboring benthic macroalgae, indicating that the content of organic matter in benthic algal region is not solely dependent on mean grain size. Our results indicate that the benthic macroalgae in the southern intertidal zone of Hampyeong Bay play an important role in the accumulation of organic matter in sediment.

주파수 종속성을 갖는 고주파 해저면 반사손실 모델 (Frequency Dependence of High-Frequency Bottom Reflection Loss Model)

  • 박순식;윤관섭;나정열;석동우;주진용;조진석
    • 한국음향학회지
    • /
    • 제23권5호
    • /
    • pp.362-369
    • /
    • 2004
  • 수층과 사질 퇴적층이 이루는 경계면이 평탄할지라도 고주파수 (30∼120 ㎑) 음파의 반사손실은 퇴적물의 입도와 입사파의 파장에 따라 거친 경계면에서의 반사 효과를 갖게 된다. 경계면 거칠기 영향은 음향학적 거칠기 (acoustical roughness, g/sub R/)로 표현하며 사질 퇴적물의 경우 g/sub R/∼ O(1)이고 주파수에 따른 종속성을 가진다. 따라서 입도분포에 따른 반사손실의 편차 (deviation)와 주파수에 따른 종속성을 포함하는 개선된 해저면 반사손실 모델 (HYBRL 모델, Hanyang University Bottom Reflection Loss model)을 제안한다. 그리고 주파수 종속성과 해저면 물성이 갖는 편차를 포함하는 반사손실 모델을 검증하기 위해 수조실험과 해상실험을 실시하였다. 수조실험 및 해상실험에서 측정된 해저면 반사손실 결과 사질 퇴적물에서 모델의 특성을 잘 반영한다.

포획된 부유물질의 입도분포를 고려한 탁도계 검교정 (Turbidity Meter Calibrations Based on Grain Size Distribution of Trapped Suspended Material)

  • 조홍연;김백운
    • 한국해안해양공학회지
    • /
    • 제15권1호
    • /
    • pp.33-38
    • /
    • 2003
  • 가덕도 인근 연안해역에서 채취된 해저 퇴적물과 연직방향으로 배열된 표사포획장치로부터 획득된 부유물질을 이용하여 탁도계 검교정을 수행하였다. 포획된 부유물질은 모래 함량이 약 6%인 해저 퇴적물에 비하여 주로 실트 및 점토로 조성되었으며, 해저면으로부터의 놀이가 증가함에 따라 세립화하는 경향을 보였다. 해저 퇴적물에 대한 탁도계 검교정 선형 회귀식의 기울기는 최소값으로 나타났으며, 수심별로 포획된 부유물질에 의한 선형 회귀식의 기울기는 포획 고도가 증가함(즉, 입도가 감소함)에 따라서 점진적으로 증가하였다. 이러한 결과는 해저 퇴적물에 대한 탁도계 검교정 결과로부터 부유물질 농도를 환산할 경우 과대추정의 오차가 발생되며, 본 연구해역의 경우에는 그 오차가 최대 25%까지 증가할 수 있다는 것을 보여준다. 따라서 해저 퇴적물보다는 수층에서 포획된 부유물질의 입도분포를 고려하여 보정된 검교정식을 적용하는 것이 부유물질 농도의 측정오차를 최소화하는 방법으로 사료된다.