• 제목/요약/키워드: grain type

검색결과 1,103건 처리시간 0.027초

기계적 합금화법으로 제조한 V-xAl (x=1, 5wt.%) 복합재료의 수소화 반응 거동 (The Hydrogenation Behaviors of V-xAl (x=1, 5wt.%) Composites by Mechanical Alloying)

  • 김경일;홍태환
    • 한국수소및신에너지학회논문집
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    • 제22권4호
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    • pp.458-464
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    • 2011
  • Recently, one of the hydrogen production methods has attracted using dense metallic membrane. It has high hydrogen permeation and selectivity which hardly could adopt industrial product because of high cost, hydrogen embrittlment and thermal stability. Meanwhile, vanadium has high hydrogen solubility and it use to instead of Pd-Ag amorphous membrane. Aluminum carried out blocking hydrogen diffusion on grain boundary therefore protecting hydrogen embrittlement. Most of dense metallic membrane is solution diffusion mechanism. The solution diffusion mechanism was very similar hydrogen storing steps such as steps of metal hydride. Thus, V-Al composites were fabricated to use hydrogen induced mechanical alloying. The fabricated V-Al composites were characterized by XRD, SEM, EDS and simultaneous TG/DSC analyses. The hydrogenation behaviors were evaluated using a Sievert's type automatic PCT apparatus. The hydrogenation behaviors of V-Al composites was evaluated too low hydrogen stored capacity and fast hydrogenation kinetics. In PCI results, V-Al composites had low hydrogen solubility, in spite of that, hydrogen kinetics was calculated very fast and hydrogen absorption/desorption contents were same capacity.

Effect of milling on the electrical properties of Ba(Fe1/2Ta1/2)O3 ceramic

  • Mahto, Uttam K.;Roy, Sumit K.;Chaudhuri, S.;Prasad, K.
    • Advances in materials Research
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    • 제5권3호
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    • pp.181-192
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    • 2016
  • In this work effect of high energy milling on the structural and electrical properties of $Ba(Fe_{1/2}Ta_{1/2})O_3$ (BFT) ceramic synthesized using standard solid-state reaction method were investigated. X-ray diffraction studies indicated that the unit cell structure for all the samples to be hexagonal (space group: P3m1). FTIR spectra also confirmed the formation of BFT without any new phase. The milled (10 h) BFT ceramic showed the formation of small grain sizes (<$2{\mu}m$) which is beneficial for dielectric applications in high density integrated devices. Besides, the milled (10 h) BFT ceramic sample exhibited superior dielectric properties (enhancement in ${\varepsilon}^{\prime}-value$ and reduction in $tg{\delta}-value$) compared to un-milled one. Impedance analysis indicated the negative temperature coefficient of resistance (NTCR) character. The correlated barrier hopping model (jump relaxation type) is found to successfully explain the mechanism of charge transport in present ceramic samples.

부유사 및 하상토 입도분포를 고려한 저수지 퇴사의 장기모의 (Long-Term Simulation of Reservoir Sedimentation Considering Particle-Size Distributions of Suspended Sediment and Bed Materials)

  • 김대근;신광균
    • 한국수자원학회논문집
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    • 제46권1호
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    • pp.87-97
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    • 2013
  • 본 연구에서는 HEC-RAS의 하상변동모형을 이용하여 고농도의 유사가 중소규모의 저수지에 유입하여 삼각주를 형성하는 과정을 유사의 입도분포를 고려하여 해석하였으며, 다음과 같은 결론을 얻을 수 있었다. 먼저, 삼각주의 시공간적인 분포와 년간 저수지에 퇴적되는 입도별 퇴사량을 합리적으로 예측할 수 있었다. 또한 저수지의 특정위치에서 특정시기에 어떤 입도의 유사가 주로 퇴적되는지를 합리적으로 예측할 수 있었다. 이러한 유사의 입도분포를 고려한 모의와 분석은 수자원관련 시설물의 계획 및 유지관리에 필요한 유용한 정보를 제공해 줄 수 있을 것으로 판단된다.

Al-Cu-Mn주조합금의 SCC특성에 미치는 Cd첨가의 영향 (Effect of Cd Addition on the SCC Properties of Al-Cu-Mn Cast Alloys)

  • 이찬희;김경현;김인배
    • 한국재료학회지
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    • 제11권4호
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    • pp.266-271
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    • 2001
  • Al-Cu-Mn 주조합금의 응력부식균열 저항성에 미치는 Cd첨가의 영향을 C-ring test와 전기전도도 시험을 통하여 조사하였다. Cd첨가량이 증가함에 따라 전기전도도가 증가하였고 SCC 저항성도 증가하였다. SCC 시험결과 균열이 입계를 따라 전파되는 입계파괴가 일어났으며, 파면은 취성파괴양상을 나타내었고, 입계를 따라 조대 석출물과 무석출대가 나타난 것으로 보아서 이 합금의 SCC 기구는 anodic dissolution model이라고 판단된다. Cd을 첨가하지 않은 경우 최대경도값은 127Hv였으나, Cd을 첨가한 경우 최대경도값은 138∼146Hv로 증가하였다.

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EFFECT OF ANNEALING ON THE OPTICAL PROPERTY OF RF-SPUTTERED CdTe THIN FILM

  • Lee, Dong-Young;Lee, Soon-Il;Oh, Soo-Ghee
    • 한국표면공학회지
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    • 제29권6호
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    • pp.666-672
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    • 1996
  • The optical property of CdTe thin film is important for applications such as the compound semiconductor type solar cells. CdTe films are prepared by RF sputtering at various substrate temperature between $25^{\circ}C$ and $300^{\circ}C$, then, annealed in argon gas environment at $400^{\circ}C$. The annealing process of the thin film caused variation in the film structure and the composition of films. The deformation of CdTe thin film was observed by X-ray diffractometry. After annealing, the grain size increased and the portion of the non-crystalline CdTe reduced. Futhermore, the structure of sputtered CdTe film grown at the substrate temperature more than $250^{\circ}C$ was enhanced in the (111) direction of zincblend structure. There was a discrepancy, in the spectroscopic ellipsometer spectrum, between the single crystal CdTe and the sputtered CdTe thin films, especially in the region over 3.2eV. An oxidation layer was found on the CdTe thin film by spectroscopic ellipsometry analysis.

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벼 품종별 오존 피해 저항성 차이 (Varietal Difference of Resistance to Ozone Injury in Rice Plant)

  • 손재근;이상철
    • 한국작물학회지
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    • 제42권3호
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    • pp.338-343
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    • 1997
  • 벼 품종의 오존 저항성 판단을 위한 시험에서 오존의 처리농도는 0.3 ppm이 0.1 ppm보다 뚜렷한 결과를 보였고, 처리시간은 2∼4시간이 알맞은 것으로 나타났다. 묘대일수에 따른 저항성 정도는 파종후 3주까지는 생육이 진전될수록 높아지는 경향이었으나 3∼5주간에는 큰 차이가 없었다. 인디카와 통일형 품종들이 자포니카 품종보다 저항성이 높은 경향이었고, 자포니카 품종 중에서 장안벼외 7 품종은 높은 저항성을 나타내었다. 벼의 생육시기에 따른 피해엽율은 간척벼는 유묘기에서 밀양 2003외 4 품종은 최고 분열기에서 가장 높게 나타났고 임실율은 수잉기 처리에서 가장 낮았다.

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Carbon fiber 후막형 열전센서 소자를 이용한 적외선 체열진단 (The Method of Thermograph using Thermoelectric Sensor Device in the Carbon fiber Thick Films)

  • 송민종;동경래;김창복;최성관;박용순
    • 대한디지털의료영상학회논문지
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    • 제12권2호
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    • pp.145-150
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    • 2010
  • Thick films of carbon fiber were prepared by a heating element of plan shape made in Darin co., We have investigated surface morphology of the specimen depending on heat-treatment temperatures. Scanning electron microscope(SEM) image of carbon fiber thick films of the specimen heat treated shows a grain growth at $1200^{\circ}C$ and becomes a poly-crystallization at $1350^{\circ}C$. The variation of resistivity at the thermally annealed specimen above $600^{\circ}C$ depends on type of the substrates. It may be due to a variation of film thickness and a difference of interfacial phenomena. A heating element of features was affected significantly by skin blood and quantity of heat of the body physiological function. After radiation of farinfrared for plate heating element, the function of biometric physiological is considered of skin blood flow and calorie which greatly affects on individuals. Electromagnetic wave was not influence on the body.

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Construction and Operation of High-$T_c$ Scanning SQUID Microscope

  • Baeka, B.;Kim, Ho-chul;Khim, Z.G.;Lee, S.M.;Moon, S.H.;Oh, B.
    • Progress in Superconductivity
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    • 제1권1호
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    • pp.20-25
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    • 1999
  • We constructed a high-$T_c$ scanning SQUID microscope (SSM) operating in the liquid nitrogen. We used a washer-type YBCO SQUID with inner and outer dimensions of $12{\mu}m$ and $36{\mu}m$, respectively, which was grown on the $SrTiO^3$ bicrystal substrate. The sample, rather than SQUID, was scanned using two stepping motors. We also developed readout electronics, stepping motor controller, and the software for system control and data display. We took images of various samples using our SSM and found that the spatial resolution is about $40{\mu}m$ and noise level is lower than $10^{-7}T/{\surd}Hz$ at 100 Hz and higher at lower frequencies. The noise level was much higher than that of a typical SQUID due to the other coupling from the electric parts. We present a simple argument on the inductive coupling between the sample and the SQUID which should be under-stood for the proper interpretation of the obtained images. By comparing the measured data with the simulation results the gap between the SQUID and the sample is estimated to be $40{\mu}m$.

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금속분말 혼합수지를 이용한 쾌속 형 제작에 관한 연구 (A study on the Rapid Tooling Using Metal Powder Filled Resin)

  • 김범수;배원병;정해도
    • 한국정밀공학회지
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    • 제16권6호
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    • pp.36-44
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    • 1999
  • The rapid Tooling technique is classified into two methods: one to directly utilize the model which was made by rapid prototyping technologies for dies, and the other to make a transferred type using the model as a master model and create dies and molds using it. In this study, the Al powder filled resin was made several mixed ratios and meshes sizes, and applied to slurry casting. And, variation of mechanical characteristics such as the shrinkage rate, the tensile strength, the elongation, the hardness, and surface roughness, are measured to compare. Consequently, as higher is the powder mixed ration and as smaller is the grain size of the power, the mechanical characteristics of the final mold are improved. Finally, the metal short fiber which can be fabricated easily and cheaply, if the self-excited vibration of an elastic tool, was also applied to slurry casting. It has been found tat the hardness gets higher, while the shrinkage rate lower, if mixed with short fiber.

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연속 드레싱 공정을 도입한 엔지니어링 세라믹스의 고능률적 연삭 가공에 관한 연구 (A study on the grinding machining of engineering ceramics with high efficiency using "In-process dressing")

  • 강재훈;이재경
    • 오토저널
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    • 제15권2호
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    • pp.130-143
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    • 1993
  • Engineering ceramics have some excellent properties as the material for the mechanical components. It is, however, very difficult to grind ceramics with high efficiency because of their high strength, hardness and brittleness. In this paper, experiments are carried out to obtain the effect of "In-process dressing" to grind the Engineering ceramics with high efficiency. To save running time for dressing process and obtain restraint effect of diamond grain wear, "In-process dressing" system using WA stick type honing stone is proposed. Representative Engineering ceramics, such as AI$_{2}$O$_{3}$, Si$_{3}$N$_{4}$, are ground with diamond wheel. Also bending strength test is carried out to check upward tendancy of mecahnical properties as the result of machining defact restraint through the grinding machining method using "In-process dressing" process. Some results obtained in this study provide useful information to attain the high efficiency grinding and the high mechanical properties of Engineering ceramics.rties of Engineering ceramics.

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