• Title/Summary/Keyword: grain direction

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Grain Growth Behavior of Heat Treated Mg-0.6wt.%Zn-0.6wt.%Ca Alloy Sheet Manufactured via Twin Roll Casting and Hot Rolling (트윈롤 주조 후 열간압연된 Mg-0.6wt.%Zn-0.6wt.%Ca 합금 판재의 열처리에 따른 결정립 성장 거동)

  • Lee, Hee Jae;Park, No Jin
    • Journal of the Korean Society for Heat Treatment
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    • v.35 no.2
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    • pp.74-81
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    • 2022
  • This study aims to mitigate the microstructural heterogeneity arising from the manufacture of magnesium alloy plates using the twin roll casting (TRC) process. Homogenization was introduced through hot rolling and heat treatment, followed by confirmation of observed changes in the microstructure. Following the TRC process, the hot rolled 2mm plate exhibited a dendritic cast structure tilted in the roll rotation direction, while central segregation were developed. This nonuniform structure and central segregation disappeared upon heat treatment, followed by recrystallization to form uniform and fine grains. Abnormal grain growth (AGG) was observed over the course of heat treatment; grains exhibiting AGG occupied up to 75% of the total area after having held the sample at 400℃ for 64 h. The formation of coarse grains was also observed during heat treatment at 340℃ over a relatively long duration, though the maximum grain size was significantly smaller than that corresponding to the heat treatment at 400℃. AGG in the 400℃ heat treatment occurred because of movement of the grain boundary, which had been fixed prior as a result of the grain boundary fixing effect of the precipitation phase. The re-dissolution of the Ca2Mg5Zn5 precipitated phase over the long duration of the high-temperature annealing process caused the surrounding grains to disappear and regrow.

Effects of Initial Nucleation Condition at the Start Block on the Grain Size and Growth Direction in Directionally Solidified CM247LC Superalloy (CM247LC 초내열합금에서 일방향응고 스타트 블록의 초기 핵생성 조건에 따른 결정립 성장)

  • Yoon, Hye-Young;Lee, Je-Hyun;Jung, Hyeong-Min;Seo, Seong-Moon;Jo, Chang-Young;Gwon, Seok-Hwan;Chang, Byeong-Moon
    • Korean Journal of Metals and Materials
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    • v.49 no.1
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    • pp.58-63
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    • 2011
  • The grain size and growth direction of a directionally solidified turbine blade were evaluated by the initial nucleation condition at the start block of directional solidification. The initial nucleation condition was controlled by inserting a Ni foil on the directional solidification plate of the directional solidification furnace. Fine grains with good orientation were obtained in the faster cooling condition at the start block. The nucleus number was compared with the cooling rate of the start block by electron back scattered diffraction (EBSD). DSC (differential scanning calorimeter) analysis was performed to compare the melting point and undercooling for nucleation of the coarse nuclei and fine nuclei of the start block. The faster cooling condition at the start block showed more undercooling for nucleation and smaller size of nuclei which resulted in a fine grain with good orientation in the directional turbine blade.

Effects of an External Magnetic Field During Electrodeposition on the Magnetic Properties of CoPtP Alloys (전기도금 시 외부자기장이 CoPtP 합금의 자기 특성에 미치는 영향)

  • Jeung, W.Y.;Park, H.D.
    • Journal of the Korean Magnetics Society
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    • v.15 no.5
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    • pp.276-281
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    • 2005
  • We have investigated the effects of an external magnetic field on the growth direction and the grain size of electrochemically prepared CoPtP alloys. Electrodeposited CoPtP alloys were synthesized by appling an external magnetic field with 0 to 1 T to the perpendicular direction of the films. In the electrodeposited CoPtP alloys without external magnetic field, the growth direction of the alloys was mixed by fcc (111) and hop (002), but only hop (002) was observed in the alloys with 1 T external magnetic field. CoPtP alloys were grown as the columnar growth and the grain size increases with growing the alloys. With appling an external field, the grain size of the alloys was controlled less than 20 nm which is smaller than single domain of Co, and the easy axis of alloys, hcp (002) direction, was grown perpendicular to the films up to 200 nm. We could obtain the optimal thickness of the alloys and electrodeposition condition from the above results. Coercivity and squareness of CoPtP alloys taken out-of-plane are 6.1 kOe and 0.9, respectively. The magnetic properties of CoPtP alloys were measured by VSM, and the microstructural characterization and crystalline orientation measurement of the alloys were carried out by TEM and XRD.

Genetic Studies on Grain Shape and Quality in Rice - I. Genetic Analysis of Grain Size, Weight and Shape (벼 입형(粒型)과 미질(米質)에 관련(關聯)된 형질(形質)의 유전연구(遺傳硏究) - I. 정조(正租)의 크기와 무게 및 모양에 대(對)한 유전분석(遺傳分析))

  • Park, Gyu Hwan;Kim, Hyun Tae;Choi, Soon Ho
    • Current Research on Agriculture and Life Sciences
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    • v.6
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    • pp.25-30
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    • 1988
  • Seven rice varieties and $42F_1$ hybrids of $7{\times}7$ diallel cross were used in genetic analysis for grain size, weight and shape. Effects of average heterosis for grain length and shape showed significantly negative values. GCA, SCA and RCA variances were significant for all characters and also additive variance was more important than dominance variance for grain length, width, thickness and weight. GCA effects of BG 2 and Arborio were highly positive for grain size and weight, and those of BG 2 and Nagdongbyeo were highly negative for grain shape. Partial dominance was observed for all characters. The direction of dominance was negative for grain length, width and shape, and ambidirections for grain thickness and weight. The effective gene number was two for grain length and shape. Both narrow and broad sense heritability were high in all characters.

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A Study on Knit Flare Skirts of Hem for 3D Virtual Clothing System - Focused on the Angle of Flare Skirt - (가상착의 시스템을 통한 니트 플레어스커트의 드레이프 형상에 관한 연구 - 각도에 따른 플레어스커트를 중심으로 -)

  • Ki, Hee-Sook
    • Journal of the Korea Fashion and Costume Design Association
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    • v.15 no.2
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    • pp.77-89
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    • 2013
  • This study investigated the formation of silhouette and hemline shape of knit flare skirts according to the properties of knit material through virtual clothing with a 3D virtual clothing system called i-Designer of Technoa, thus building a database of the property data of knit material to reduce the number of sample making steps repeated and implemented several times in the process of clothes making. The results would help to estimate a silhouette in advance, offer assistance to the development of original knit wear, and explore ways to provide basic data for the development of the knit industry of the nation. The investigator made 12 kinds of experimental clothes to the angles(width of skirt: $90^{\circ}$ and $180^{\circ}$), gauge(7G, 12G, and 15G), and grain directions(wale and bias direction) of experimental clothes for virtual clothing. The dynamic characteristics of knit skirt samples according to each gauge were measured with the KES-FB system. Draper shapes were analyzed with the sectional shape data of hemline based on i-Designer. As for the measurements of the sectional shape of hemline and the formation of silhouette, the number of nodes, the average height of node mountains and valleys, and the hemline width right and left and before and after increased at the angle of $180^{\circ}$ than $90^{\circ}$. As gauges multiplied, the number of nodes, and silhouette angle dropping. When considering grain directions, the number of nodes and silhouette index increased in the wale direction at the angle of $90^{\circ}$ with the number of nodes and silhouette angle increasing in the wale direction at the angle of $180^{\circ}$.

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Microstructure and Mechanical Property in Thickness Direction of a Deoxidized Low-Phosphorous Copper Sheet Processed by Two-Pass Differential Speed Rolling (2-pass 이주속압연된 인탈산동판재의 두께방향으로의 미세조직 및 기계적 특성)

  • Lee, Seong-Hee;Jang, Jun-Hyuk;Utsunomiya, Hiroshi
    • Korean Journal of Materials Research
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    • v.23 no.7
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    • pp.392-398
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    • 2013
  • A two-pass differential speed rolling(DSR) was applied to a deoxidized low-phosphorous copper alloy sheet in order to form a homogeneous microstructure. Copper alloy with a thickness of 3 mm was rolled to 75 % reduction by two-pass rolling at $150^{\circ}C$ without lubrication at a differential speed ratio of 2.0:1. In order to introduce uniform shear strain into the copper alloy sheet, the second rolling was performed after turning the sample by $180^{\circ}$ on the transverse direction axis. Conventional rolling(CR), in which the rotating speeds of the upper roll and lower roll are identical to each other, was also performed by two-pass rolling under a total rolling reduction of 75 %, for comparison. The shear strain introduced by the conventional rolling showed positive values at positions of the upper roll side and negative values at positions of the lower roll side. However, samples processed by the DSR showed zero or positive values at all positions. {100}//ND texture was primarily developed near the surface and center of thickness for the CR, while {110}//ND texture was primarily developed for the DSR. The difference in misorientation distribution of grain boundary between the upper roll side surface and center regions was very small in the CR, while it was large in the DSR. The grain size was smallest in the upper roll side region for both the CR and the DSR. The hardness showed homogeneous distribution in the thickness direction in both CR and DSR. The average hardness was larger in CR than in DSR.

Development of High Efficiency Self Diagnosis Type Neon Transformer using Groin Direction of Non-Oriented Silicon Steel Strip (압연 방향을 적용한 자체 진단형 고효율 네온관용 변압기)

  • 변재영;김윤호
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.17 no.1
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    • pp.17-24
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    • 2003
  • In this paper, a high efficiency leakage transformer for neon tube is developed to improve its power factor, to reduce its core loss and weight by using a technique of shape optimization and grain direction of non-oriented silicon steel strip. A protection circuit is designed for all types of neon transformer loaded with one or more neon tubes. Whenever the neon tube fails to be started up or comes to the life end, or encounters faults with open-circuits at the output terminals of the neon transformer, the electronic type protection circuit will be initiated to avoid more critical hazards. These neon transformers need a electronic type protection circuit to prevent from current stresses on circuit components by neon tube fail. The input of the transformer is automatically cut on when the abnormal condition occurs, preventing waste of no-load power.

Enhancement of Grain Refinement and Formability of Cross-Roll-Rolled Ni-10Cr Alloy (교차롤압연된 Ni-10Cr 합금의 결정립 미세화와 성형성 향상)

  • Song, Kuk-Hyun;Kim, Won-Yong;Son, Hyun-Taek
    • Korean Journal of Materials Research
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    • v.22 no.6
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    • pp.303-308
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    • 2012
  • This study evaluated the enhancement of microstructural and mechanical properties of a cross rolled Ni-10Cr alloy, comparing with conventionally rolled material. Cold rolling was carried out to 90% thickness reduction and the specimens were subsequently annealed at $700^{\circ}C$ for 30 min to obtain a fully recrystallized microstructure. Cross roll rolling was carried out at a tilted roll mill condition of $5^{\circ}$ from the transverse direction in the RD-TD plane. In order to observe the deformed microstructures of the cold rolled materials, transmission electron microscopy was employed. For annealed materials after rolling, in order to investigate the grain boundary characteristic distributions, an electron back-scattering diffraction technique was applied. Application of cold rolling to the Ni-10Cr alloy contributed to notable grain refinement, and consequently the average grain size was refined from 135 ${\mu}m$ in the initial material to 9.4 and 4.2 ${\mu}m$ in conventionally rolled and cross rolled materials, respectively, thus showing more significantly refined grains in the cross rolled material. This refined grain size led to enhanced mechanical properties such as yield and tensile strengths, with slightly higher values in the cross rolled material. Furthermore, the <111>//ND texture in the CRR material was better developed compared to that of the CR material, which contributed to enhanced mechanical properties and formability.

High Temperature Grain Growth Behavior of Aerosol Deposited BaTiO3 Film on (100), (110) Oriented SrTiO3 Single Crystal (상온분사분말공정에 의해 SrTiO3 (100), (110) Seed에 코팅된 BaTiO3의 고온 성장 거동 분석)

  • Lim, Ji-Ho;Lee, Seung Hee;Kim, Ki Hyun;Ji, Sung-Yub;Jung, Suengwoon;Park, Chun-kil;Jung, Han-Bo;Jeong, Dae-Yong
    • Korean Journal of Materials Research
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    • v.29 no.11
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    • pp.684-689
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    • 2019
  • Single crystals, which have complexed composition, are fabricated by solid state grain growth. However, it is hard to achieve stable properties in a single crystal due to trapped pores. Aerosol deposition (AD) is suitable for fabrication of single crystals with stable properties because this process can make a high density coating layer. Because of their unique features (nano sized grains, stress inner site), it is hard to fabricate single crystals, and so studies of grain growth behavior of AD film are essential. In this study, a $BaTiO_3$ coating layer with ${\sim}9{\mu}m$ thickness is fabricated using an aerosol deposition method on (100) and (110) cut $SrTiO_3$ single crystal substrates, which are adopted as seeds for grain growth. Each specimen is heat-treated at various conditions (900, 1,100, and $1,300^{\circ}C$ for 5 h). $BaTiO_3$ layer shows different growth behavior and X-ray diffraction depending on cutting direction of $SrTiO_3$ seed. Rectangular pillars at $SrTiO_3$ (100) and laminating thin plates at $SrTiO_3$ (110), respectively, are observed.

Microscopic Analysis of the Rock Cleavage for Jurassic Granite in Korea (주라기 화강암에 발달하는 결의 현미경학적 분석)

  • 박덕원;서용석;정교철;김영기
    • The Journal of Engineering Geology
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    • v.11 no.1
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    • pp.51-62
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    • 2001
  • Jurassic granites of three sites, Pocheon, Geochang and Habcheon, were analysed with respect to the characteristics of the rock cleavage. Microscopic analysis for the oriented thin sections of the specimens was conducted by using the scanline survey technique to measure microcrack direction, spacing and length. The results showed that the preferred orientations of microcrack developed in quartz and feldspar arc coincident with the orientation of quarry planes. The length of microcrack is related to grain size. The length of microcrack in coarse-grained granite is longer than that in relatively fine-grained granite. In all granites, microcracks related to the preferred orientations are well developed in order of rift, grain and hardway planes in number, length and density.

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