• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.529-530
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• 2006

This paper concerned with SPS (spark plasma sintering), hot pressing of sinter nanometer WC-Co powder and discussed the density, hardness, microstructures and grain sizes of the alloys sintered. The results showed that the two sintered techniques could produce high density alloys and play well on the grain growth, but SPS could lower the sintering temperature and shorten sintering time. Besides, the hardness of the sintered cemented alloys that was dependent on the grain size and densification could also be improved.

• 한국분말재료학회지
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• 제11권3호
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• pp.233-241
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• 2004

In this study, bottom-up type powder processing and top-down type SPD (severe plastic deformation) approaches were combined in order to achieve both full density and grain refinement of Al-20 wt% Si powders without grain growth, which was considered as a bottle neck of the bottom-up method using the conventional powder metallurgy of compaction and sintering. ECAP (Equal channel angular pressing), one of the most promising method in SPD, was used for the powder consolidation. The powder ECAP processing with 1, 2, 4 and 8 passes was conducted for 10$0^{\circ}C$ and 20$0^{\circ}C$ It was found by microhardness, compression tests and micro-structure characterization that high mechanical strength could be achieved effectively as a result of the well bonded powder contact surface during ECAP process. The SPD processing of powders is a viable method to achieve both fully density and nanostructured materials.

• 소성∙가공
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• 제29권1호
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• pp.37-43
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• 2020

Increasing the critical current density of superconducting wire is one of the difficult challenges in the field of superconductivity. It is well known that the higher volume fraction of uniformly dispersed α-Ti is able to enhance the critical current density of superconducting material NbTi because α-Ti serves as a flux pinning center. The volume fraction of α-Ti highly depends on the grain size of NbTi because α-Ti precipitates at the grain boundaries or triple points. For this purpose, we investigated the effect of initial microstructures of NbTi obtained from hot rolling in various temperature conditions on the critical current density. In addition, subsequent heat treatment was assigned to precipitate α-Ti and groove rolling/cold drawing was adopted to produce a wire with a diameter of about 1.0 mm. It was observed that the band structure was formed after hot rolling at 500~600℃. It was also found that the volume fraction of α-Ti after hot rolling at 500~600℃ was higher and it led to the highest critical current density.

• 한국분말재료학회지
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• 제15권1호
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• pp.31-36
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• 2008

In this study, the bottom-up powder metallurgy and the top-down severe plastic deformation (SPD) techniques for manufacturing bulk nanomaterials were combined in order to achieve both full density and grain refinement without grain growth of rapidly solidified Al-20 wt% Si alloy powders during consolidation processing. Continuous equal channel multi-angular processing (C-ECMAP) was proposed to improve low productivity of conventional ECAP, one of the most promising method in SPD. As a powder consolidation method, C-ECMAP was employed. A wide range of experimental studies were carried out for characterizing mechanical properties and microstructures of the ECMAP processed materials. It was found that effective properties of high strength and full density maintaining nanoscale microstructure are achieved. The proposed SPD processing of powder materials can be a good method to achieve fully density and nanostructured materials.

• 한국작물학회지
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• 제39권4호
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• pp.353-358
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• 1994

초형이 다른 옥수수의 재식밀도에 대한 반응차이를 구명하고자 직립형 초형과 수평형 초형 교잡종을 재식밀도를 달리하여 재배하고 종실수량 및 주요형질을 조사한 결과를 요약하면 다음과 같다. 1. 공시된 4교잡종 모두 고밀식(10,000주 /10a)하에서 종실수량이 감소하였으나 직립형 교잡종보다 수평형 교잡종인 Ga209${\times}$Ki14A에서 감소의 폭이 더커서 초형간에 차이가 있었다. 2. 재식밀도 증가에 따라 초장은 짧아지고 착수고는 높아졌으나 초형간의 차이는 유의성이 없었다. 3. 수장, 열수, 및 열당입수는 재식밀도 증가에 따라 감소하였고 초형간에는 차이가 없었다. 4. 잎의 각도는 재식밀도에 따라 차이가 없었으며 종실수량, 수장, 열수 및 열당입수와 부의 상관을 보였다.

• Journal of Advanced Marine Engineering and Technology
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• 제27권3호
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• pp.453-459
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• 2003

In this study, the effect of heat treatment to the electrochemical polarization resistance for the Ti-6Al-4V alloy was measured. The solution heat treatments were carried out at $1066^{circ}E, 966^{\circ}$E$, followed by aging heat treated $550^{circ}E, 600^{circ}E, and 650^{circ}E$. The electrochemical polarization resistance behavior was measured by potentio-dynamic polarization in the 1N $HNO_3$ + 15ppm HF solution. The obtained results were as follows. 1. As solution heat temperature increased. the corrosion potential was increased, whereas passive current density and critical current density were decreased. 2. As aging heat temperature increased, the corrosion potential was almost constant, but passive current density was decreased 3. The results of composition test measured by EDS at grain boundary and near $\gamma'$ precipitates indicated that S, Cl. and Si which originated from base metal were segregated at the grain boundaries Al and Ti which were the main alloying element in $\gamma'$ were depleted at the $\gamma'$ precipitated. The depletion of Al and Ti in $\gamma'$ was caused to early breakdown of passive film.

• 한국분말재료학회지
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• 제14권1호
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• pp.26-31
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• 2007

Manufacturing bulk nanostructured materials with least grain growth from initial powders is challenging because of the bottle neck of bottom-up methods using the conventional powder metallurgy of compaction and sintering. In this study, bottom-up type powder metallurgy processing and top-down type SPD (Severe Plastic Deformation) approaches were combined in order to achieve both real density and grain refinement of metallic powders. ECAP (Equal Channel Angular Pressing), one of the most promising processes in SPD, was used for the powder consolidation method. For understanding the ECAP process, investigating the powder density as well as internal stress, strain distribution is crucial. We investigated the consolidation and plastic deformation of the metallic powders during ECAP using the finite element simulations. Almost independent behavior of powder densification in the entry channel and shear deformation in the main deformation zone was found by the finite element method. Effects of processing parameters on densification and density distributions were investigated.

• E2M - 전기 전자와 첨단 소재
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• 제8권5호
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• pp.640-647
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• 1995

In this study, the BaTiO$\sub$3/ capacitor add to MnO$\sub$2/ like depressor and shifter were investigated for temperature or voltage compensation by structural and electrical analysis. The relative density of BCTM, generating poly crystall and formation of lattice defect, has a 90[%] over as the CaTiO$\sub$3/ come out to control grain size. The current density of BCTM2 increased non-ohmic in high-electric field but that BCTM3 and BCTM4 had a few changing. The BCTM3 and BCTM4 unformated grain boundary shown temperature compensation properties, so that the dielectric constant was low value. The curie point was near 140[.deg. C] in BCTM1 and BCTM4, but BCTM3 and BCTM4 not shown the curie point. It is found that the charging energy of BCTM4 was changed 6[%] according to rising temperature from room temperature to 417[K]. The formation of BaMnO$\sub$3/ was low dielectric constant to change frequency and temperature.

• 한국작물학회:학술대회논문집
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• 한국작물학회 1991년도 춘계 학술대회지
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• pp.20-21
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• 1991

• The Journal of Advanced Prosthodontics
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• 제5권2호
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• pp.161-166
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• 2013

PURPOSE. This study aimed to identify the effects of the sintering conditions of dental zirconia on the grain size and translucency. MATERIALS AND METHODS. Ten specimens of each of two commercial brands of zirconia (Lava and KaVo) were made and sintered under five different conditions. Microwave sintering (MS) and conventional sintering (CS) methods were used to fabricate zirconia specimens. The dwelling time was 20 minutes for MS and 20 minutes, 2, 10, and 40 hours for CS. The density and the grain size of the sintered zirconia blocks were measured. Total transmission measurements were taken using a spectrophotometer. Two-way analysis of variance model was used for the analysis and performed at a type-one error rate of 0.05. RESULTS. There was no significant difference in density between brands and sintering conditions. The mean grain size increased according to sintering conditions as follows: MS-20 min, CS-20 min, CS-2 hr, CS-10 hr, and CS-40 hr for both brands. The mean grain size ranged from 347-1,512 nm for Lava and 373-1,481 nm for KaVo. The mean light transmittance values of Lava and KaVo were 28.39-34.48% and 28.09-30.50%, respectively. CONCLUSION. Different sintering conditions resulted in differences in grain size and light transmittance. To obtain more translucent dental zirconia restorations, shorter sintering times should be considered.