• 열처리공학회지
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• 제12권2호
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• pp.157-165
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• 1999

Grain size of steels is one of the most important parameters which influence yield strength and fracture toughness. Ultrasonic wave propagating in polycrystalline materials is mostly attenuated by scattering at grain boundary. Effect of ultrasonic attenuation on average ferrite grain size of carbon steels with tensile strength $40{\sim}60kgf/mm^2$ consisting of multi phases such as ferrite + pearlite and ferrite + pearlite + bainite was evaluated. The attenuation of these steels rapidly increased with average ferrite grain diameter. Average ferrite grain diameter ($D_{av}$, ${\mu}m$) could be expressed as $1.79+22.97*a^{1/2.03}$, where a is attenuation with unit of nepers/cm. From this study, it was confirmed that nondestructive ultrasonic method could be used in measuring average ferrite grain size indirectly.

• Journal of Magnetics
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• 제3권3호
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• pp.96-98
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• 1998

In this paper a structurally coupled and magnetically decoupled Ba-ferrite thin film medium is proposed to evade the superparamagnetic limit and reduce media noise. The proposed medium consists of ferrimagnetic Ba-ferrite nano-grains (< 10 nm) and a non-magnetic grain boundary material. Magnetic grains are crystallographically matched with the grain boundary material. Spherical or cubic shaped Ba-ferrite particle is also proposed for above 100 Kfci particulate recording application.

• 한국재료학회지
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• 제14권6호
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• pp.379-388
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• 2004

To investigate the effect of D-ferrite on the hot workability and surface defect of STS 304 billets containing 3 wt. % Cu, microstructure observations and high temperature mechanical properties test were carried out for the specimens extracted mainly from raw or oxidized billets. It was found that the total $\delta$-ferrite content has little influence on the hot workability, even though the fracture cracks due to high temperature tension or compression test were initiated and propagated mostly along $\delta$/${\gamma}$ boundary in the specimens. On the other hand, it was supposed that the direct causes of surface defects in the wire rolled from the as-continuously cast billet were the grain boundary embrittlement arose from the deep diffusion of oxygen into the grain boundary, and the oxidation of $\delta$-ferrite connected by a grain boundary to the surface during the billet reheating process as well.

• 대한금속재료학회지
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• 제48권11호
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• pp.1021-1027
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• 2010

The charpy impact property was lower at the surface and middle regions than that at the root region in metal welded by Tandem EGW of 82 mm thick EH40-TM steel plates. Temperature distribution in the weld sample and the heating/cooling temperature throughout the various regions in the weld metal were estimated by the commercial weld simulation program SYSWELD. The microstructure of the weld metal consisted of acicular ferrite and grain boundary ferrite. Grain boundary ferrite in the acicular ferrite matrix was found more in the surface and middle regions than in the root region, and the acicular ferrite was also coarser in the surface and middle regions where the impact toughness was lower and the input temperature was higher. Our results indicated that the impact toughness property was related to the microstructure morphology, the distribution of grain boundary ferrite, and the acicular ferrite.

• Journal of Welding and Joining
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• 제31권6호
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• pp.112-118
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• 2013

In this study, constant loading test (CLT) was performed to evaluate the hydrogen embrittlement resistance for multipass FCA weld metals of 600MPa tensile strength grade. The microstructures of weld metal-2 having the smallest carbon equivalent (Ceq=0.37) consisted of grain boundary ferrite and widmanstatten ferrite in the acicular ferrite matrix. The weld metal-1 having the largest Ceq=0.47, showed the microstructures of grain boundary ferrite, widmanstatten ferrite and the large amount of bainite (vol.%=19%) in the acicular ferrite matrix. The weld metal-3 having the Ceq=0.41, which was composed of grain boundary ferrite, widmanstatten ferrite, and the small amount of bainite (vol.%=9%) in the acicular ferrite matrix. Hydrogen desorption spectrometry (TDS) used to analyze the amount of diffusible hydrogen and trapping site for the hydrogen pre-charged specimens electrochemically for 24 hours. With increasing the current density of hydrogen pre-charging, the released amount of diffusible hydrogen was increased. Furthermore, as increasing carbon equivalent of weld metals, the released diffusible hydrogen was increased. The main trapping sites of diffusible hydrogen for the weld metal having a low carbon equivalent (Ceq=0.37) were grain boundaries and those of weld metals having a relatively high carbon equivalent (Ceq: 0.41~0.47) were grain boundaries and dislocation. The fracture time for the hydrogen pre-charged specimens in the constant loading test was decreased as the carbon equivalent increased from 0.37 to 0.47. This result is mainly due to the increment of bainite that is vulnerable to hydrogen embrittlement.

• Journal of Welding and Joining
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• 제32권1호
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• pp.22-27
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• 2014

In the past, cold crack was commonly observed in the HAZ(heat affected zone) of high-strength steels. Applying to TMCP(thermo-mechanical controlled process) and HSLA(high strength low alloy) steels, cold crack tends to increase the occurrence in the weld metal. It is generally understood that cold crack occurs when the following factors are present simultaneously : diffusible hydrogen in the weld metal, a susceptible microstructure and residual stress. In particular, many studies investigated the microstructural effect on the cold crack in HAZ and the cold crack in weld metals starts to receive the special attendance in modern times. The purpose of the study is to review the effect of weld microstructures (grain boundary ferrite, Widm$\ddot{a}$nstatten ferrite, acicular ferrite, bainite and martensite) on cold crack in the weld metals. Among various microstructures of weld metals, acicular ferrite produced the greatest resistance to the cold crack due to the fine interlocking nature and high-angle grain boundary of the microstructure.

• Journal of Welding and Joining
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• 제22권2호
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• pp.78-84
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• 2004

Effects of manganese and carbon on the HAZ microstructural evolution in 500㎫ grade titanium oxide steels were investigated. Microstructural evolution primarily depends on supercooling. When cooled at 3$^{\circ}C$/s in 0.15%C-1.5%Mn steel, grain boundary and Widmanst tten ferrite formed at 640 and 62$0^{\circ}C$, respectively, followed by competitive formation of acicular ferrite and upper bainite inside of grain at 58$0^{\circ}C$. With an increase of manganese, degree of supercooling increased while critical cooling rate for the formation of gain boundary ferrite decreased. Consequently, the amount of acicular ferrite in HAZ was decreased in 2.0%Mn after initial increase in 1.0 and 1.5%Mn. Therefore, optimum supercooling should be maintained to accelerate acicular ferrite formation in titanium oxide steels. Low carbon steel, 0.11%C-1.5%Mn, showed larger amount of acicular ferrite than higher carbon steel because of effectiveness of diffusionless transformation in low carbon steel.

• Journal of Welding and Joining
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• 제17권3호
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• pp.96-101
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• 1999

Microstructures and mechanical properties of weldments were studied for EH36 TMCP higher-strength hull steel with electrogas welding jprocess. In case of a newly designed EH36 TMCP steel for large heat input welding process, the Microstructures of HAZ shows more narrow width of grain coarsed region than that of conventional EH36 TMCP weldments, the amount of acicular ferrite, which is beneficial to impact toughness, increased while the amount of grain-boundary ferrite decreased. Charpy V-notched impact tests show that a newly designed EH36 TMCP steel weldment satisfies all the requirement of specifications, especially at the fusion line +2mm where the conventional EH36 TMCP steel fails to exceed the requirement.

• 열처리공학회지
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• 제35권4호
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• pp.211-219
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• 2022

It is known that superplastic materials with ultrafine grains have high elongation mainly due to grain boundary sliding. Therefore, in the present study we examined the influence of grain refinement, caused by a repetitive cold rolling and annealing process, on both superplastic elongation and superplastic deformation mechanism. The cold rolling and annealing process was repetitively applied up to 4 times using Fe-10Mn-3.5Si alloy. High-temperature tensile tests were conducted at 763 K with an initial strain rate of 1 × 10^-3 s^-1 using the specimens. The superplastic elongation increased with the number of the repetitive cold rolling and annealing process; in particular, the 4 cycled specimen exhibited the highest elongation of 372%. The primary deformation mechanism of all specimens was grain boundary sliding between recrystallized α-ferrite and reverted γ-austenite grains. The main reason for the increase in elongation with the number of the repetitive cold rolling and annealing process was the increase in fractions of fine recrystallized α-ferrite and reverted γ-austenite grains, which undergo grain boundary sliding.

• 한국세라믹학회:학술대회논문집
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• 한국세라믹학회 2000년도 추계총회,초청강연,특별강연,연구발표회
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• pp.89.2-89
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• 2000