• Title/Summary/Keyword: grain angle

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Microstructures of Friction Stir Lap Weld in A5052-H112 Alloy (A5052-H112 합금의 겹치기 마찰교반접합 조직 특성)

  • Ko, Young-Bong;Lee, Joong-Hun;Park, Kyeung-Chae
    • Journal of Welding and Joining
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    • v.27 no.6
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    • pp.17-24
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    • 2009
  • The Friction Stir Welding(FSW) has mainly been used for making butt joints in Al alloys. Development of Friction Stir Lap Welding(FSLW) would expand the number of applications. Microstructure of FSLW in A5052-H112 alloy was investigated under varying rotation and welding speed. As the rotation speed was increased and the welding speed was decreased, a amount of heat was increased. As a result, bead interval was narrower, bead width are larger, and experimental bead interval was almost similar to theoretical bead interval. Typical microstructures of FSLW A5052-H112 alloy consist of three zones, including Stir Zone(SZ), Thermo-Mechanically Affected Zone(TMAZ) and Heat Affected Zone(HAZ). As a amount of heat was increased, average grain size was larger in three zones. Nevertheless, the aspect ratio was almost fixed for FSLW conditions. The misorientation of SZ, HAZ and TMAZ was examined. A large number of low angle grain boundaries, which were formed by severe plastic deformation, were showed in TMAZ as comparison with SZ and HAZ. Microhardness distribution was high in order of BM, SZ, TMAZ, and HAZ. The Micro-hardness distribution in HAZ, TMAZ of upper plate were lager than lower plate. Relationship between average grain size and microhardness was almost corresponded to Hall-Petch equation.

Effect of Cooling Conditions on Microstructures and Mechanical Properties in API X80 Linepipe Steels (API X80 라인파이프강의 미세조직과 기계적 특성에 미치는 냉각조건의 영향)

  • Han, Seung Youb;Shin, Sang Yong;Lee, Sunghak;Bae, Jin-ho;Kim, Kisoo
    • Korean Journal of Metals and Materials
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    • v.47 no.9
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    • pp.523-532
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    • 2009
  • In this study, four API X80 linepipe steel specimens were fabricated with varying cooling rates and finish cooling temperatures, and their microstructures and crystallographic orientations were analyzed to investigate the effects of cooling conditions on their tensile and Charpy impact properties. All the specimens consisted of acicular ferrite, granular bainite, and secondary phases such as martensite and martensiteaustenite constituent. The volume fraction of secondary phases increased with increasing cooling rate, and the higher finish cooling temperature resulted in the reduction in volume fraction and grain size of secondary phases. According to the crystallographic orientation analysis data, the effective grain size and unit crack path decreased as fine acicular ferrites having a large amount of high-angle grain boundaries were homogeneously formed, thereby leading to the improvement of Charpy impact properties. The specimen fabricated with the higher cooling rate and lower finish cooling temperature had the highest upper shelf energy and the lowest energy transition temperature because it contained a large amount of fine secondary phases homogeneously distributed inside fine acicular ferrites, while its tensile properties well maintained.

Properties of the Green Gold Alloys with Indium Content

  • Song, Jeongho;Song, Ohsung
    • Korean Journal of Materials Research
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    • v.28 no.4
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    • pp.221-226
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    • 2018
  • The property changes of 18, 14, and 8K green gold alloys for jewelry are observed by adding 0.0, 3.0, and 5.0 wt% of indium (In), respectively. To check the composition of the alloys, an energy dispersive spectroscopy (EDS) analysis is conducted. Color and microstructure analysis is executed through bare-eye, macro camera, UV-VIS-NIR-colormeter, and optical microscope. The melting point, wetting angle, and hardness are measured using TGA-DTA, a wetting angle tester, and a Vickers hardness tester. The EDS analysis result demonstrates that each of the green gold alloys was manufactured with purposed contents. The color analysis result shows that the color of the alloys is similar to the color of the conventional 4 wt%-Cd 18K green gold, and the green color improves as the In content increases. The micro structure analysis result demonstrates that grain refinement improves as the amount of In increases. Enhancements in the melting point, wettability, and Vickers hardness changes appear as the In content increases and Au content decreases. The hardness is up to 260, which implies good durability. Therefore, the results suggest that the proposed 18, 14, and 8K In-added green gold alloys enhance the properties of jewelry products with regard to the green color, castability, and durability.

Studies on the Fundamental Properties of the Wood of Gumgangsong(Pinus densoflora for. erecta Uyeki) (Part 1) (강송의 기초적 재질에 관한 연구(제1보))

  • 김정환;이원희;홍선천
    • Journal of the Korea Furniture Society
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    • v.10 no.2
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    • pp.55-61
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    • 1999
  • This research was carried out to investigate the fundamental properties such as the structure of annual ring, density distribution, compressive strength with parallel to grain, relative crystallinity, and microfibril angle of Gumgangsong(Pinus densoflora for. erecta Uyeki). The wood specimens, Gumgangsong and Sonamu(Pinus densiflora S. et Z.), for this experiment were prepared at Ulijingoon Sokwangri and Kyungpook university's forest in Kyungpook province, respectively. Average annual ring width is $2.0mm{\pm}0.3$ in heartwood of Gumgangsong. The respectively of heart wood was over 60 percent in Gumgangsong and 20~50 percent in Sonamu. Heartwood density were ranged from 0.5 to $0.8{\;}g/cm^3$ in Gumgangsong and from 0.4 to $0.5{\;}g/cm^3$ in sonamu. Compressive strength in Gumgangsong and Sonamu was about $30{\pm}5MPa$ and $25{\pm}5MPa$, resepectively. But the relative crystallinity and microfibril angle of two species were not different clearly. From these results of Gumgangsong and Sonamu, therefore, it was considered the main difference factors for both species were annual ring width and heartwood percentage.

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Tests of the interface between structures and filling soil of mountain area airport

  • Wu, Xueyun;Yang, Jun
    • Geomechanics and Engineering
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    • v.12 no.3
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    • pp.399-415
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    • 2017
  • A series of direct shear tests were conducted to investigate the frictional properties of the interface between structures and the filling soil of Chongqing airport fourth stage expansion project. Two types of structures are investigated, one is low carbon steel and the other is the bedrock sampled from the site. The influence of soil water content, surface roughness and material types of structure were analyzed. The tests show that the interface friction and shear displacement curve has no softening stage and the curve shape is close to the Clough-Duncan hyperbola, while the soil is mainly shear contraction during testing. The interface frictional resistance and normal stress curve meets the Mohr-Coulomb criterion and the derived friction angle and frictional resistance of interface increase as surface roughness increases but is always lower than the internal friction angle and shear strength of soil respectively. When surface roughness is much larger than soil grain size, soil-structure interface is nearly shear surface in soil. In addition to the geometry of structural surface, the material types of structure also affects the performance of soil-structure interface. The wet interface frictional resistance will become lower than the natural one under specific conditions.

Deformation Behavior of 6063 Al Alloy Deformed by Shear-Drawing Method (전단-신선 가공된 6063 알루미늄 합금의 변형거동)

  • Ko, Young Gun;Lee, Byung Uk;Shin, Dong Hyuk
    • Korean Journal of Metals and Materials
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    • v.49 no.4
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    • pp.291-297
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    • 2011
  • This work investigated the microstructure and mechanical properties of 6063 Al alloy fabricated by shear-drawing (SD) technique where shear and drawing strains were combined together within a predetermined die. To find the optimum condition for sound deformation, three different dies having different inner angle and diameter of the exit channel were prepared. After single deformation of the present sample, the sound deformation took place without an abrupt failure of the sample if the inner angle would be greater than $135^{\circ}$ in this study, when the channel diameter of the SD die was reduced from 10 to 9 mm. Microstructural observation showed that the inner angle of $135^{\circ}$ was found to be more effective than that of $150^{\circ}$ in terms of the alignment of each grain to the shear direction imposed by SD method. In addition, the yield strength of the SD-deformed sample was twice higher than that of the initial counterpart while loosing ductility in tension.

Structural and Electrical Properties of $CuGaS_2$ Thin Films ($CuGaS_2$ 반도체 박막의 구조적 및 전기적 특성)

  • Park, Gye-Choon;Jung, Hae-Duk;Lee, Jin;Jeong, Woon-Jo;Kim, Jong-Uk;Cho, Young-Dae;Gu, Hal-Bon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.286-289
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    • 2001
  • Single phase CuGaS$_2$ thin film with the highest diffraction peak of (112) at diffraction angle (2$\theta$) of 28.8$^{\circ}$ was made at substrate temperature of 7$0^{\circ}C$, annealing temperature of 35$0^{\circ}C$ and annealing time of 60 min. And second highest (204) peak was shown at diffraction angle (2$\theta$) of 49.1$^{\circ}$. Lattice constant of a and c of that CuGaS$_2$ thin film was 5.37 $\AA$ and 10.54 $\AA$ respectively. The greatest grain size of the thin film was about 1${\mu}{\textrm}{m}$. The (112) peak of single phase of CuGaS$_2$ thin film at annealing temperature of 35$0^{\circ}C$ with excess S supply was appeared with a little higher about 10 % than that of no exces S supply And the resistivity, mobility and hole density at room temperature of p-type CuGaS$_2$ thin film with best crystalline was 1.4 $\Omega$cm, 15 cm2/V . sec and 2.9$\times$10$^{17}$ cm$^{-3}$ respectively. It was known that carrier concentration had considerable effect than mobility on variety of resistivity of the fabricated CuGaS$_2$ thin film, and the polycrystalline CuGaS$_2$ thin films were made at these conditions were all p-type.

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Effect of Texture of Al Single Crystal on the Nanopore Structure of AAO (알루미늄 단결정 집합조직이 AAO의 나노기공 구조에 미치는 영향)

  • Park, B.H.;Kim, I.
    • Transactions of Materials Processing
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    • v.29 no.3
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    • pp.127-134
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    • 2020
  • It is known that the difference of texture of the polycrystalline Al sheet is not a critical parameter for the formation of aligned nanopore arrays in anodic aluminum oxide (AAO). This will be related to the polycrystalline grain in the Al sheet. The texture of each grain in the polycrystalline Al sheet is different. The mixed textures of grains have the mixing effects on the nanopore structure of the AAO. Thus, the effect of Al texture on the nanopore structure of the AAO was investigated using three types of Al single crystals with (111), (200) and (220) textures in this paper. These three types of AAO layers were fabricated by the two-step anodizing method at 40 V and temperature of 0-5℃ in oxalic acid solution. In the nanopores formed on the AAO, the average area of one nanopore and the average roundness of one nanopore were measured were measured based on the SEM images. In the hexagon obtained by connecting nanopores on the AAO, the average standard deviation of one angle deviated from 120° was measured. In the AAO nanopores with texture of (111), (200) and (220) single crystal samples, the average area of one nanopore of (200) single crystal sample was the widest, followed by (111), (220) single crystals. The average circularity of one nanopore of (200) single crystal sample was the best, followed by (111), (220) single crystals. The average standard deviation of an angle from 120° of (220) single crystal sample was the largest, followed by (111) and (200) single crystals.

Microfabrics of omphacite and garnet in eclogite from the Lanterman Range, northern Victoria Land, Antarctica

  • Kim, Daeyeong;Kim, Taehwan;Lee, Jeongmin;Kim, Yoonsup;Kim, Hyeoncheol;Lee, Jong Ik
    • Geosciences Journal
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    • v.22 no.6
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    • pp.939-953
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    • 2018
  • We examined the microfabrics of omphacite and garnet in foliated eclogite to determine the influence of the layered structure on seismic observations in subduction zone. The analyzed eclogite, from the Lanterman Range, northern Victoria Land, Antarctica, is characterized by layering in which the modal abundances of garnet and omphacite vary. For garnet, the low aspect ratios, similar angular distribution of long axes relative to the foliation in both layers, uniform grain size distribution, near-random crystallographic preferred orientations (CPOs), and misorientation angle distributions are indicative of passive behavior during deformation. In contrast, omphacite shows relatively high aspect ratios, a low angle between the long axes of crystals and the foliation, a wide grain-size distribution, and distinctive CPOs, suggesting dislocation creep as the main deformation mechanism. The results of fabric analyses are consistent with strain localization into omphacite or omphacite-rich layers rather than garnet or garnet-rich layers. The single-crystal seismic anisotropy of garnet is very weak ($AV_P=0.2%$, $AV_S=0.5-0.6%$), whereas that of omphacite is much stronger ($AV_P=3.7-5.9%$ and $AV_S=2.9-3.8%$). Seismic anisotropy of the omphacite-rich layers shows an increase of 329% for $AV_P$ and 146% for $AV_S$ relative to the garnet-rich layers. Our results demonstrate the importance of the layered structure in strain localization and in the development of the seismic anisotropies of subducting oceanic crust.

Comparison of the physical characteristics according to the varieties of perilla for the development of a high-quality, high-efficiency cleaner and stone separator

  • Park, Jong Ryul;Park, Heo Man;Park, Hye Rin;Yang, Gye Hoon;Lee, Jung Hyun
    • Korean Journal of Agricultural Science
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    • v.47 no.4
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    • pp.717-726
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    • 2020
  • The physical characteristics of the major varieties of perilla were analyzed to use as basic data for the design of a high-quality, high-efficiency perilla cleaner and stone separator. Because the size, thousand-grain weight, angle of repose, angle of friction, bulk density and terminal velocity of perilla have significant differences according to the perilla variety, the different of characteristics by variety should be considered for performance improvement of a perilla cleaner and stone separator. Therefore the cleaner and stone separator using a sieve could be improved by the application of a detachable sieve or by using equipment such as a 2 - 3 stage sieve and regulating the slope. Moreover, because differences in the terminal velocity occur due to the differences in the size and thousand-grain weight according to the perilla variety, a blower with an adjustable fan speed was considered for the design of the improved cleaner. Additionally, it was shown that the length of perilla has the greatest correlation based on a comparison of the coefficients of the other characteristics. Accordingly, the length of perilla could be used as a major factor for the fine adjustment and parts replacement of the device. These results can be used as basic data for a high-quality, high-efficiency perilla cleaner and stone separator. In the future, the development of the machine and follow-up studies based on the basic data are needed to determine the optimized operating conditions and mechanism of action.