• Journal of the Korean Ceramic Society
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• v.28 no.4
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• pp.324-328
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• 1991

Monolithic silica gel and glass were prepared from TMOS solution with high concentration of HCl. Appearance of the dried gels and gelation time varied with content of HCl and H2O were observed in the TMOS-CH3OH-HCl-H2O system. The conversion from gel to glass during heat treatment stage was investigated using TG-DTA, XRD, IR and SEM and characteristics of the gel were examined by measuring bulk density, linear shrinkage and Vicker's hardness. A transparent silica glass was prepared from the gel after heat treatment at 1050℃.

• Journal of Integrative Natural Science
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• v.1 no.3
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• pp.230-233
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• 2008

A simple and rapid method is described for extending the 5'- or 3'-end genomic sequence of a known partial sequence by only a single round of PCR. This method involves digesting and ligating genomic and plasmid DNAs, and amplifying the 5'-upstream or 3'-end downstream sequence of the known DNA sequence, using two primers, one gene specific and the other plasmid specific. A single round of PCR amplification is sufficient to produce gene-specific bands detectable in gels. By using this approach, 5'-end genomic sequence of the D-amoeba sams gene was extended.

• Korean Journal of Microbiology
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• v.13 no.2
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• pp.71-80
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• 1975

The neurotoxin of Clostridium botulinum type B was purified from a liquid culture. The purification steps consist of ammonium sulfate precipitation of whole culture, treatment of Polymin P(0.15%, v/v), gel filtration on Sephadex G-100 at pH5.6 and DEAE-Sephadex charomatography at pH8.0. The procedure recovered 17% of the toxin assayed in the starting culture. The toxin was homogeneous by sodium dodecyl sulfate(SDS)-polyacrylamide gel electrophoresis and had a molecular weight of 163,000. Subunits of 106,000 and 56,000 molecular weight were found when purified toxin was treated with a disulfide-reducing agent and electro phoresed on SDS-polyacrylamide gels.

• Journal of the Korean Ceramic Society
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• v.28 no.12
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• pp.975-980
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• 1991

Chelated titanium alkoxides are hydrolysed showly and stable enough to prepare multicomponent gels of titania without its precipitation due to the fast hydrolysis of Ti alkoxide. The alkoxy groups of chelated titanium alkoxide are hydrolysed as fast as that of titanium alkoxide but the chelating groups are stable even in aqueous solution. The chelating groups showed different rates of hydrolysis in aqueous ammonia solution and water added one. Those rates were monitored with UV-VIS spectrophotometer by using their unique absorption bands before and after hydrolysis.

• Proceedings of the Korean Ceranic Society Conference
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• 2002.10a
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• pp.120.1-120
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• 2002

• Bulletin of the Korean Chemical Society
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• v.28 no.5
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• pp.883-886
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• 2007

• YAKHAK HOEJI
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• v.25 no.4
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• pp.175-179
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• 1981

Rheological studies on the gelatin hydrogels were carried out by rheometer. In the temperature range of $32^{\circ}~90{\circ}C$, the viscosities of the gelatin hydrogels were measured. In order to observe the formation of gel structure, the stress-relaxation tests of the creep-curves were investigated. The structure of viscoelastic substance could be considered of a three dimensional crosslinked matrix. As the result viscoelastic coefficients were obtained by Maxwell element, which are correspond to the network structure. From the relationship between the stress-relaxation time and temperature, activation energy correspond to breaking the formation of gels was calculated to be 13.91kcal/mole.

• Journal of the Korean Ceramic Society
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• v.27 no.5
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• pp.693-697
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• 1990

TIACA has two different side groups(ligands) as iso-propoxy groups and acetylacetonate groups. These two side groups have different hydrolysis rates. The two different rates of hydrolysis confer unique properties on TIACA, which are stability in aqueous solution and easy preparation of TiO2 and its multi components gels without precipitation. Their hydrolysis rates were monitored with I.R. and U.V. spectrophotometer.

• Journal of the Korean Society of Food Science and Nutrition
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• v.20 no.2
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• pp.173-178
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• 1991

The rheological properties of acorn crude starch gel and refined starch gel were investigated by puncture test, back-extrusion test and retrogradation test. Puncture test was a useful method to compare the different gel type and concentration, and to calculate the compression and shear coefficient. Maximum extrustion force and adhesiveness were also examined by performing back-extrustion test. The retrogradation rate was analysed by Avrami equation in retrogradation test.

• Korean journal of food and cookery science
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• v.17 no.6
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• pp.598-603
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• 2001

Gel characteristics of potato starches which were prepared by steeping potato at 10$\pm$ 1$\^{C}$ and 25$\^{C}$$\pm$1$\^{C}$ incubator for 11days were investigated. Results of the instrumental test of potato starch gels showed significantly different strength, hardness, gumminess, chewiness, cohesiveness by steeping time. The light microscope and scanning electron microscope of starch gels showed three-dimensional network including macroporous structure by steeping. The syneresis of potato starch gel was decreased by steeping potato at 24 for 72 hours.