• 생약학회지
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• 제26권4호
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• pp.327-336
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• 1995

Twelve phenolic components were isolated from the aqueous acetone extract of the leaf of Cornus controversa H. (Cornaceae). On the basis of chemical and spectroscopic evidence, the structures of these components were established as gallic acid, $1-O-galloyl-{\beta}-{_D}-glucose$, $1,6-di-O-galloyl-{\beta}-{_D}-glucose$, $1,2,3-tri-O-galloyl-{\beta}-{_D}-glucose$, $1,2,6-tri-O-galloyl-{\beta}-{_D}-glucose$, 3,4,6-tri-O-galloyl ${_D}-glucose$, eugeniin, gemine D, quercetin, quercitrin, hyperoside and rutin.

• Natural Product Sciences
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• 제6권4호
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• pp.193-198
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• 2000

Phytochemical study of the constitutive polyphenolics of the flower aqueous alcohol extract of Tamarix tetragyna was carried out. The new sulphated flavonol, quercetin 3',4'-dimethyl ether $3-O-KSO_3$ as well as the new natural galloyl glucose, $2-O-galloyl-({\alpha}/{\beta})-^4C_1-glucopyranose$ were isolated and characterized. The known sulphated flavonols, kaempferol 7,4-dimethyl ether $3,5-di-O-KSO_3$, quercetin 7-methyl ether $3,3',4'-tri-O-KSO_3$, quercetin 7,4'-dimethyl ether $3-O-KSO_3$ and quercetin $3-O-KSO_3$ and the known sulphated phenolics, isoferulic acid $3-O-KSO_3$ and ellagic acid 4,4'-dimethyl ether $3-O-KSO_3$ were also separated and identified. The structures were established by conventional methods of analysis and confirmed by $^1H-,\;^{13}C-NMR$ and negative ESI-mass spectrometry. 2D-homonuclear chemical shift correlation NMR experiment was applied for the new natural galloylglucose.

• 생약학회지
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• 제23권4호
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• pp.211-217
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• 1992

Seven hydrolysable tannins and two related compounds have been isolated from the acetone-water(4 : 1) soluble portion of the aerial parts of Euphorbia ebracteolata(Euphorbiaceae). Seven hydrolysable tannins have been determined as 3-O-galloyl-shikimic acid, 1, 3, 4, 6-tetra-O- and $1,\;2,\;3,\;4,\;6-penta-O-galloyl-{\beta}-D-glucose$, corilagin, tercatain, punicafolin and geraniin and two related compounds determinedasgallicacidandellagicacidonthebasisof spectral data and physico-chemical evidence.