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A Study of Practical and Optimized Mineral Quantification (실용적이고 최적화된 광물정량분석법 연구)

  • Son, Byeong-Kook;An, Gi-O
    • Korean Journal of Mineralogy and Petrology
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    • v.34 no.4
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    • pp.227-239
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    • 2021
  • A practical and effective method of X-ray powder diffraction analysis was investigated for quantitative analysis of the mineral content of natural samples. Sample mounting experiments were conducted to select the best randomly oriented powder sample mount. A comparative experiment was also made between a reference intensity ratio (RIR) method, which compares a single peak intensity with standard material, and the Rietveld method, which calculates a full X-ray diffraction pattern, to search for the effective method of mineral quantification. In addition, samples containing amorphous minerals were quantitatively analyzed by the Rietveld method and the efficiency was reviewed. As a result of the study, the optimal random orientation could be reached by the side mounting method. The Rietveld method using the full pattern of X-ray diffraction was more suitable for mineral quantitative analysis, rather than the RIR method using a specific peak. However, either method could depend on the analyst's experience in addition to analytical technique. Moreover, amorphous minerals can be quantitatively analyzed by the Rietveld method, and the analysis results make the geological analysis possible.

Predicting standardized ileal digestibility of lysine in full-fat soybeans using chemical composition and physical characteristics

  • Chanwit Kaewtapee;Rainer Mosenthin
    • Animal Bioscience
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    • v.37 no.6
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    • pp.1077-1084
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    • 2024
  • Objective: The present work was conducted to evaluate suitable variables and develop prediction equations using chemical composition and physical characteristics for estimating standardized ileal digestibility (SID) of lysine (Lys) in full-fat soybeans (FFSB). Methods: The chemical composition and physical characteristics were determined including trypsin inhibitor activity (TIA), urease activity (UA), protein solubility in 0.2% potassium hydroxide (KOH), protein dispersibility index (PDI), lysine to crude protein ratio (Lys:CP), reactive Lys:CP ratio, neutral detergent fiber, neutral detergent insoluble nitrogen (NDIN), acid detergent insoluble nitrogen (ADIN), acid detergent fiber, L* (lightness), and a* (redness). Pearson's correlation (r) was computed, and the relationship between variables was determined by linear or quadratic regression. Stepwise multiple regression was performed to develop prediction equations for SID of Lys. Results: Negative correlations (p<0.01) between SID of Lys and protein quality indicators were observed for TIA (r = -0.80), PDI (r = -0.80), and UA (r = -0.76). The SID of Lys also showed a quadratic response (p<0.01) to UA, NDIN, TIA, L*, KOH, a* and Lys:CP. The best-fit model for predicting SID of Lys in FFSB included TIA, UA, NDIN, and ADIN, resulting in the highest coefficient of determination (R2 = 0.94). Conclusion: Quadratic regression with one variable indicated the high accuracy for UA, NDIN, TIA, and PDI. The multiple linear regression including TIA, UA, NDIN, and ADIN is an alternative model used to predict SID of Lys in FFSB to improve the accuracy. Therefore, multiple indicators are warranted to assess either insufficient or excessive heat treatment accurately, which can be employed by the feed industry as measures for quality control purposes to predict SID of Lys in FFSB.

Experimental Analysis of Load Distribution in Pile Foundations Using a Smart Preloading System for Vertical Extension Remodeling (수직증축 리모델링시 스마트 선재하시스템 적용을 위한 말뚝기초의 하중분담 실험적 연구)

  • Won, Jinoh;Kim, Junsung;Song, Hyoungmin;Lee, Kiho;Son, Sewook;Cho, Chunwhan
    • Journal of the Korean Geotechnical Society
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    • v.40 no.5
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    • pp.131-142
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    • 2024
  • To analyze the preloading effects and the load distribution ratio between existing piles and reinforcing piles during vertical extension remodeling, pilot tests were conducted. Previous studies on load distribution typically involved small-scale experiments or numerical simulations. The stiffness of piles used in load distribution designs is often estimated using empirical formulas, which exhibit significant variability. In this study, steel reinforcing piles were installed adjacent to existing PHC piles at an apartment construction site. The actual stiffness of the individual piles was determined through static load tests and compared with empirical formula predictions. The pilot tests (full-scale load-distribution tests), applying column loads simultaneously to the existing and reinforcing piles, demonstrated that column loads are distributed based on the stiffness ratio of each pile. The pilot test outcomes were further compared with long-term measurement data. A smart preloading system was developed in this study to address the preloading loss observed in previous systems, and its applicability was validated through full-scale tests.

Evaluation of TOF MR Angiography and Imaging for the Half Scan Factor of Cerebral Artery (유속신호증강효과의 자기공명혈관조영술을 이용한 뇌혈관검사에서 Half Scan Factor 적용한 영상 평가)

  • Choi, Young Jae;Kweon, Dae Cheol
    • Journal of the Korean Magnetics Society
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    • v.26 no.3
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    • pp.92-98
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    • 2016
  • To aim of this study was to assess the full scan and half scan of imaging with half scan factor. Patients without a cerebral vascular disease (n = 30) and were subject to the full scan half scan, and set a region of interest in the cerebral artery from the three regions (C1, C2, C3) in the range of 7 to 8 mm. MIP (maximum intensity projection) to reconstruct the images in signal strength SNR (signal to noise ration), PSNR (peak signal noise to ratio), RMSE (root mean square error), MAE (mean absolute error) and calculated by paired t-test for use by statistics were analyzed. Scan time was half scan (4 minutes 53 seconds), the full scan (6 minutes 04 seconds). The mean measurement range (7.21 mm) of all the ROI in the brain blood vessel, was the SNR of the first C1 is completely scanned (58.66 dB), half-scan (62.10 dB), a positive correlation ($r^2=0.503$), for the second C2 SNR is completely scanned (70.30 dB), half-scan (74.67 dB) the amount of correlation ($r^2=0.575$), third C3 of a complete scan SNR (70.33 dB), half scan SNR (74.64 dB) in the amount of correlation between the It was analyzed with ($r^2=0.523$). Comparative full scan with half of SNR ($4.75{\pm}0.26dB$), PSNR ($21.87{\pm}0.28dB$), RMSE ($48.88{\pm}1.61$), was calculated as MAE ($25.56{\pm}2.2$). SNR is also applied to examine the half-scans are not many differences in the quality of the two scan methods were not statistically significant in the scan (p-value > .05) image takes less time than a full scan was used.

Measurement of shoulder motion fraction and motion ratio (견관절 운동 분율의 측정)

  • Kang, Yeong-Han
    • Journal of radiological science and technology
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    • v.29 no.2
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    • pp.57-62
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    • 2006
  • Purpose : This study was to understand about the measurement of shoulder motion fraction and motion ratio. We proposed the radiological criterior of glenohumeral and scapulothoracic movement ratio. Materials and Methods : We measured the motion fraction of the glenohumeral and scapulothoracic movement using CR(computed radiological system) of arm elevation at neutral, 90 degree, full elevation. Central ray was $15^{\circ},\;19^{\circ},\;22^{\circ}$ to the cephald for the parallel scapular spine, and the tilting of torso was external oblique $40^{\circ},\;36^{\circ},\;22^{\circ}$ for perpendicular to glenohumeral surface. Healthful donor of 100 was divided 5 groups by age(20, 30, 40, 50, 60). The angle of glenohumeral motion and scapulothoracic motion could be taken from gross arm angle and radiological arm angle. We acquired 3 images at neutral, $90^{\circ}$ and full elevation position and measured radiographic angle of glenoheumeral, scapulothoracic movement respectively. Results : While the arm elevation was $90^{\circ}$, the shoulder motion fraction was 1.22(M), 1.70(W) in right arm and 1.31, 1.54 in left. In full elevation, Right arm fraction was 1.63, 1.84, and left was 1.57, 1.32. In right dominant arm(78%), $90^{\circ} and Full motion fraction was 1.58, 1.43, in left(22%) 1.82, 1.94. In generation 20, $90^{\circ} and Full motion fraction was 1.56, 1.52, 30' was 1.82, 1.43, 40' was 1.23, 1.16, 50' was 1.80, 1.28, 60' was 1.24, 1.75. There was not significantly by gender, dominant arm and age. Conclusion : The criterior of motion fraction was useful reference for clinical dignosis the shoulder instability.

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Seismic Performance Evaluation of RC Bridge Piers with Limited Ductility by the Pseudo-Dynamic Test (한정연성 철근콘크리트 교각의 유사동적 실험에 의한 내진 성능 평가)

  • Chung, Young-Soo;Park, Chang-Kyu;Park, Jin-Young
    • Journal of the Korea Concrete Institute
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    • v.15 no.5
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    • pp.705-714
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    • 2003
  • Even though Korean peninsula is located in regions of moderate seismic risks, current seismic design provisions of the roadway bridge design code have adopted the AASHTO code which is based on the requirements for high seismic regions. The objective of this research is to investigate the seismic performance of circular reinforced concrete (RC) bridge piers with limited ductility, which may be desirable in low or moderate seismic regions, such as in Korea. Four test specimens were designed and constructed. The reference specimen was designed with longitudinal steel ratio as 1.01% and the confinement reinforcement ratio as 0.13% without considering earthquake, and three other test specimens were designed in accordance with a limited-ductility concept as 0.3% for the confinement steel ratio. This confinement ratio is 0.32 times of minimum lateral reinforcement specified in current seismic design provisions, and 2.3 times of lateral reinforcement required in nonseismic design provisions. The pseudo-dynamic test was carried out to evaluate the seismic performance of full-scale specimens in size of 1.2m diameter and 4.8m height. Judging from the experiment, the reference specimen was not satisfactory for the demand displacement ductility ${\mu}$=5.0, but three limited-ductility specimens appeared to have the displacement ductility of more than 5.

Ultimate capacity of welded box section columns with slender plate elements

  • Shen, Hong-Xia
    • Steel and Composite Structures
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    • v.13 no.1
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    • pp.15-33
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    • 2012
  • For an axially loaded box-shaped member, the width-to-thickness ratio of the plate elements preferably should not be greater than 40 for Q235 steel grades in accordance with the Chinese code GB50017-2003. However, in practical engineering the plate width-to-thickness ratio is up to 120, much more than the limiting value. In this paper, a 3D nonlinear finite element model is developed that accounts for both geometrical imperfections and residual stresses and the ultimate capacity of welded built-up box columns, with larger width-to-thickness ratios of 60, 70, 80, and 100, is simulated. At the same time, the interaction buckling strength of these members is determined using the effective width method recommended in the Chinese code GB50018-2002, Eurocode 3 EN1993-1 and American standard ANSI/AISC 360-10 and the direct strength method developed in recent years. The studies show that the finite element model proposed can simulate the behavior of nonlinear buckling of axially loaded box-shaped members very well. The width-to-thickness ratio of the plate elements in welded box section columns can be enlarged up to 100 for Q235 steel grades. Good agreements are observed between the results obtained from the FEM and direct strength method. The modified direct strength method provides a better estimation of the column strength compared to the direct strength method over the full range of plate width-to-thickness ratio. The Chinese code and Eurocode 3 are overly conservative prediction of column capacity while the American standard provides a better prediction and is slightly conservative for b/t = 60. Therefore, it is suggested that the modified direct strength method should be adopted when revising the Chinese code.

New three-layer-type hysteretic damper system and its damping capacity

  • Kim, Hyeong Gook;Yoshitomi, Shinta;Tsuji, Masaaki;Takewaki, Izuru
    • Earthquakes and Structures
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    • v.3 no.6
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    • pp.821-838
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    • 2012
  • This paper proposes a new three-layer pillar-type hysteretic damper system for residential houses. The proposed vibration control system has braces, upper and lower frames and a damper unit including hysteretic dampers. The proposed vibration control system supplements the weaknesses of the previously proposed post-tensioning vibration control system in the damping efficiency and cumbersomeness of introducing a post-tension. The structural variables employed in the damper design are the stiffness ratio ${\kappa}$, the ductility ratio ${\mu}_a$, and the ratio ${\beta}$ of the damper's shear force to the maximum resistance. The hysteretic dampers are designed so that they exhibit the targeted damping capacity at a specified response amplitude. Element tests of hysteretic dampers are carried out to examine the mechanical property and to compare its restoring-force characteristic with that of the analytical model. Analytical studies using an equivalent linearization method and time-history response analysis are performed to investigate the damping performance of the proposed vibration control system. Free vibration tests using a full-scale model are conducted in order to verify the damping capacity and reliability of the proposed vibration control system. In this paper, the damping capacity of the proposed system is estimated by the logarithmic decrement method for the response amplitudes. The accuracy of the analytical models is evaluated through the comparison of the test results with those of analytical studies.

Effect of plate properties on shear strength of bolt group in single plate connection

  • Ashakul, Aphinat;Khampa, Kriangkrai
    • Steel and Composite Structures
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    • v.16 no.6
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    • pp.611-637
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    • 2014
  • A single plate shear connection, or shear tab, is a very popular shear connection due to its merit in ease of construction and material economy. However, problems in understanding the connection behavior, both in terms of strength and ductility, have been well-documented. Suggestions or design model for single plate connections in AISC Design Manual have been altered several times, with the latest edition settling down to giving designers pre-calculated design strength tables if the connection details agree with given configurations. Results from many full-scale tests and finite element models in the past suggest that shear strength of a bolt group in single plate shear connections might be affected by yield strength of plate material; therefore, this research was aimed to investigate and clarify effects of plate yield strength and thickness on shear strength of the bolt group in the connections, including the validity of using a plate thickness/bolt diameter ratio ($t_p/d_b$) in design, by using finite element models. More than 20 models have been created by using ABAQUS program with 19.0- and 22.2-mm A325N bolts and A36 and Gr.50 plates with various thicknesses. Results demonstrated that increase of plate thickness or plate yield strength, with the $t_p/d_b$ ratio remained intact, could significantly reduce shear strength of the bolt group in the connection as much as 15 percent. Results also confirmed that the $t_p/d_b$ ratio is a valid indicator to be used for guaranteeing strength sufficiency. Because the actual ratio recommended by AISC Design Manual is $t_p/d_b$ + 1.6 (mm) for connections with a number of bolts less than six and plate yield strength in construction is normally higher than the nominal value used in design, it is proposed that shear strength of a bolt group in single plate connections with a number of bolts equal or greater than seven be reduced by 15 percent and the $t_p/d_b$ ratio be limited to 0.500.

Flexural behaviour of reinforced low-strength concrete beams strengthened with CFRP plates

  • Boukhezar, Mohcene;Samai, Mohamed Laid;Mesbah, Habib Abdelhak;Houari, Hacene
    • Structural Engineering and Mechanics
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    • v.47 no.6
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    • pp.819-838
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    • 2013
  • This paper summarises the results of an experimental study to investigate the flexural behaviour of reinforced concrete beams strengthened using carbon-fibre reinforced polymer (CFRP) laminate in four-point bending. The experimental parameters included are the reinforcing bar ratio ${\rho}_s$ and preload level. Four bar ratios were selected (${\rho}_s=0.13$ to 0.86%), representing the section of two longitudinal tensile reinforcements, with diameters of 8, 14, 16, and 20 mm in order to reveal the effect of bar ratio on failure load and failure mode. Eight beams that could be considered "full-scale" in size, measuring 200 mm in width, 400 mm in total height and 2300 mm in length, were tested. Three beams were selected with different bar ratios (${\rho}_1$, ${\rho}_2$, ${\rho}_3$), and considered as control specimens (without ), while three other beams identical to the control beams with the same CFRP laminates ratio and a seventh beam with ${\rho}_{min}$ (the lowest bar ratio) were also used. In the second part of the study, two beams with the bar ratio ${\rho}_2$ were preloaded at two levels, 50 and 100% of their ultimate loads, and then repaired. This experimental investigation was consolidated using an analytical model. The experimental and analytical results indicate that the flexional capacity and stiffness of strengthened and repaired beams using CFRP laminate were increased compared to those of control beams, and the behaviour of repaired beams was nearly similar to the undamaged and strengthened beams; unlike the ductility of strengthened beams, which was greatly reduced compared to the control.