• 자원환경지질
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• 제49권5호
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• pp.389-410
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• 2016

옥천대 남서부인 전주-김제-정읍일대 쥬라기 화강암질 저반체로부터 구한 FT 연대는 넓은 범위에 걸쳐 나타난다: 스핀=158~70 Ma; 저콘=127~71 Ma; 인회석=72~46 Ma. 교란되지 않은 일차냉각 및 리셋 또는 부분감소된 FT 연대, 그리고 일부 트랙 길이 측정자료에 기반한 열연대학적 해석을 통해 화강암체가 겪은 복잡한 지열사를 규명하였다. 이 화강암체의 전체 냉각사는 정출 후 $300^{\circ}C$ 등온선까지의 비교적 빠른 전기 냉각(${\sim}20^{\circ}C/Ma$)과 $300^{\circ}C-200^{\circ}C-100^{\circ}C$ 등온선을 거쳐 현재 지표온도에 이르기까지의 매우 느린 후기 냉각($2.0{\sim}1.5^{\circ}C/Ma$)으로 특징지어진다. 이 쥬라기 화강암체의 많은 부분은 일련의 후기 백악기 화성활동에 의해 적어도 $170^{\circ}C$ 이상(최고 >$330^{\circ}C$)의 다양한 수준에 달하는 지열상승을 겪은 것으로 확인되었다. 다양한 후기 화성암체들의 두 지점으로부터 중복측정된 FT 저콘 연대의 일치된 결과는 그들의 생성시기를 잘 정의한다: 석영반암=$73{\pm}3Ma$; 섬록암=$73{\pm}2Ma$; 유문암=$72{\pm}3Ma$; 장석반암=$78{\pm}4Ma$ (전체 가중평균=$73{\pm}3Ma$). 이들 후기 화성암체와 페그마타이트 암맥군의 관입은 온천개발지역(화심, 죽림, 목욕리, 회봉 등)을 위시한 연구지역 내에서의 후기 지열상승에 주요 역할을 하였던 것으로 해석된다. 이 화강암 저반체의 후기냉각이 지표면의 침식-삭박에 따른 상대적 융기에 의해 근본적으로 규제되었다고 가정하면, 전기 백악기 이후의 융기는 연간 평균 약 0.05 mm (즉 백만 년에 약 50 m)의 매우 느린 속도로 진행되었다. 100 Ma, 70 Ma, 40 Ma를 기준으로 현재까지의 총융기량은 각각 5 km, 3.5 km, 2 km 정도로 추정된다. 여러 지점의 일정한 융기량은 암체 전체가 광역적으로 고르게 융기하였음을 지시한다.

• 한국의류학회지
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• 제43권2호
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• pp.288-296
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• 2019

This study examined the proper dyeing conditions, color fastness and functionality for wool fabrics dyed with Chamaecyparis obtusa leaf extract. FT-IR and UV-Vis spectrum analysis showed that tannin and flavonoids were contained in the extracted colorant. The dyeing of wool fabrics using Chamaecyparis obtusa leaf was good without pretreatment or mordant treatment. Optimal dyeing conditions for wool fabrics were a colorant concentration of 70%(v/v), dyeing temperature of $100^{\circ}C$, dyeing time of 100 minutes and dyebath pH of 5.8. Color fastness of dyed wool fabrics to washing, rubbing, perspiration was good, whereas light was grade 3. The UV protection rate and deodorization rate of wool fabrics dyed with Chamaecyparis obtusa leaf improved. Reduction rate of Staphylococcus aureus/Klebsiella pneumoniae were excellent at 99.9%. Therefore, it was confirmed that Chamaecyparis obtusa leaf can be used as environ-mentally friendly natural dye.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2012년도 제43회 하계 정기 학술대회 초록집
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• pp.249-249
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• 2012

최근 주목받고 있는 Flexible Organic Light Emitting Diode (OLED) display에서는 Flexible 특성이 요구된다. 이는 현재 쓰이는 유리기판 대신 플라스틱기판으로 만들어야 가능하다. 하지만 플라스틱기판은 구성물질로 유기물을 사용하므로 수분과 산소의 투과에 매우 취약하다. 이는 장시간 사용 시 기판 위에 제작된 소자성능저하를 야기하는 등의 소자 신뢰도에 치명적 결함을 갖게 하는 원인이 된다. 따라서 기판 위의 소자를 보호할 수 있는 봉지기술 개발이 필요한데 가장 잘 알려진 플라스틱 기판에 적합한 Barrier기술로 유기물과 무기물을 교대로 적층하는 기술[1] 등이 있다. 본 연구에서는 PE-CVD 공정기술을 이용한 Flowable Oxide 박막과 ALD 공정기술을 이용한 Al2O3 무기물 박막을 적층하여 봉지박막을 구성하려 한다. Flowable Oxide는 저온공정이 가능하며 높은 증착속도와 뛰어난 Gap fill 특성을 가지고 있는데 이는 플라스틱기판의 엉성한 분자구조를 치밀하게 만들 것으로 예상되며 표면의 Pin-hole 또한 쉽게 채우는 특성이 있다. 실험은 Polyethylene Naphthalate (PEN) film 위에 PE-CVD 공정을 이용하여 Flowable Oxide를 증착하고, 그 후에 ALD 공정을 이용하여 Al2O3을 적층한 것을 하나의 샘플로 하였다. 샘플의 분석은 Ca test를 이용한 Water Vapor Transmission rate(WVTR)과 FT-IR, FE-SEM을 이용하여 분석하였다. FT-IR로 박막의 구성요소를 확인 하고 FE-SEM으로 박막의 Cross section image를 얻을 수 있었으며 또한 $4.85{\times}10^{-5}g/m^2$ day의 초기 WVTR 값을 얻을 수 있었다.

• 한국수소및신에너지학회논문집
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• 제31권1호
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• pp.73-81
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• 2020

For the fault tree analysis (FTA) analysis of the packaged hydrogen filling station, the composition of the charging station was analyzed and the fault tree (FT) diagram was prepared. FT diagrams were created by dividing the causes of events into external factors and internal factors with the hydrogen event as the top event. The external factors include the effects of major disasters caused by natural disasters and external factors as OR gates. Internal factors are divided into tube tailer, compressor & storage tank, and dispenser, which are composed of mistakes in operation process and causes of accidents caused by parts leakage. In this study, the purpose was to improve the hydrogen station. The subjects of this study were domestic packaged hydrogen stations and FTA study was conducted based on the previous studies, failure mode & effect analysis (FMEA) and hazard & operability study (HAZOP). Top event as a hydrogen leaking event and constructed the flow of events based on the previous study. Refer to "Off shore and onshore reliability data 6th edition", "European Industry Reliability Data Bank", technique for human error rate prediction (THERP) for reliability data. We hope that this study will help to improve the safety and activation of the hydrogen station.

• 대한기계학회논문집A
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• 제21권8호
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• pp.1259-1269
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• 1997

The procedure for the determination of the residual life of the pressurizer surge line nozzle in the nuclear plant is developed. The design fatigue life for the 1800 $ft^3$ pressurizer surge line nozzle in cast head design is compared with that of Westinghouse stress report, and the percentage difference between two results is less than 9%. The design fatigue life evaluation of the 1000 $ft^3$ pressurizer surge line nozzle in fabricated head design is carried out, and the consuming rate and residual life are estimated using the operating data.

• 한국세라믹학회지
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• 제30권3호
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• pp.222-228
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• 1993

In order to obtian TiO2 fine powder of high purity, the new method which is different from the sulfate process and the chloride one was employed. TiO2 was syntehsized by the reaction between elemental titanium particles and H2O2 solutiosn at 30~7$0^{\circ}C$, and then TiO2 powder was characterized using XRD, SEM, TEM, DTA and FT-IR. It was found that the initial reaction rate was fast at a high temperature due to the high generation of activated oxygen associated with thedecomposition of H2O2. However, the reaction was slowly proceeded at a low temperature due to slow decomposition of H2O2. In this experimental range, the optimum temeprature was ocnsidered to be about 5$0^{\circ}C$. The primary particles of the hydrous titanium dioxide (TiO2 gel) before aging were spherical, and their mean sizes were about 50nm. The similar shapes and sizes were observed with calcinatin at 40$0^{\circ}C$. The FT-IR spectrum of Ti-OH in the TiO2 gel powder appeared at around 3380cm-1, 1630cm-1 and 530cm-1. This gel powder was crystallized into the anatase type TiO2 at 300~40$0^{\circ}C$.

• 한국인쇄학회지
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• 제13권2호
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• pp.47-53
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• 1995

Photosensitive resin of azide type is good for resolution and inner solvent, but it is really problem to development of practical use because fanctional groups of polymer has many hydrophilic radicals. By careful attention to this point, this study was investigated synthesis term, photo property and development property of composed photosensitive resin of azida type, it is to this effect. 1) H-NMR spectrum of compared DABCI showed amion redical by $\delta$6.0~6.1ppm to substitude for azide radical by amino radical by $\delta$8.9~9.45ppm, and FT-IR absorption spectra showed the absorption bends at 2100cm. 2)FT-IR absorption spectra of PHS1-DAB, PHS2-DAB, CMM-DAB and CHM-DAB showed azida radical pick to be lost at after irradiation by UV light. 3) According to exposuer change of PHS1-DAB, PHS2-DAB, CMM-DAB and CHM-DAB, absorption maximum value of UV spectrum change was 280nm. 4) to compared relative sensitivity of compared photosensitive resin, PHS2-DAB was the best and to compared insolubility rate of compared photosensitive resin, CMM-DAB was the lower. 5)Solubility if NaOH was the best by 1.0mol/$\ell$ and solubility of developing solution of ethanol to water was it in the ratio of 4 to 1.

• 통합자연과학논문집
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• 제3권3호
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• pp.153-156
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• 2010

Oxidation behaviors of porous silicon were investigated by the measurement of area of $SiO_2$ vibrational peaks in FT-IR spectra during thermal oxidation of porous silicon at corresponding temperatures. Visible photoluminescent porous silicon samples were obtained from an electrochemical etch of n-type silicon of resistivity between 1-10 ${\Omega}/cm$. The etching solution was prepared by adding an equal volume of pure ethanol to an aqueous solution of HF. The porous silicon was illuminated with a 300 W tungsten lamp for the duration of etch. Etching was carried out as a two-electrode galvanostatic procedure at applied current density of 200 $mA/cm^2$ for 5 min. The porosity of samples prepared was about 80%. After formation of porous silicon, the samples were thermally oxidized at $100^{\circ}C$, $200^{\circ}C$, $300^{\circ}C$, and $400^{\circ}C$, respectively. The growth rate of $SiO_2$ layer of porous silicon was investigated by using FT-IR spectroscopy. The effect of oxidation of porous silicon was presented.

• 대한설비공학회:학술대회논문집
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• 대한설비공학회 2009년도 하계학술발표대회 논문집
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• pp.1288-1293
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• 2009

The TES (Thermal Energy Storage) cooling system utilizing cheaper off-peak electricity has been applied just for building air-conditioning currently and causes limitation of usage rate and inefficiency of national resources utilization. In this regard, more says the necessity to apply TES system in industrial cooling system which is longer using period and wider usage. In this study, we will approve the technical and economical improvement in efficiency of industrial cooling system applied TES system by utilizing cheaper off-peak electricity and it will attribute the promotion of TES system and stabilization of supply and demand of electric power by proving the necessity to develop more efficient industrial cooling system by combining TES system.

• 폴리머
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• 제27권6호
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• pp.603-608
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• 2003

신디오탁틱 폴리스티렌 (5-PS)는 시료의 처리 조건에 따라 여러 구조를 가지며 열처리에 따른 고체상의 구조 전이현상을 보여준다 서로 다른 s-PS 사슬 및 결정 구조를 가지는 시료들을 상온에서 220 $^{\circ}C$까지 온도를 올려가며 열처리하여 준비한 후 FTIR과 FT-Raman 분광계를 이용하여 구조의 변화를 조사하였다. 빠른 결정화 속도 때문에 DSC 실험으로 측정하기 힘든 x-PS 시료의 열처리 시간에 따른 결정화도 변화를 결정 부분과 비결정 부분 infrared특성피크 세기에 따라 측정한 후 Beer-Lambert 법칙에 적용하여 조사할 수 있었다.