• Title/Summary/Keyword: free abrasive

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The Endotoxin Assay of Contaminated Titanium Implants following Various Techniques of Detoxification (오염된 임프란트 표면의 해독 방법에 따른 내독소 제거 효과에 관한 연구)

  • Park, Joong-Hee;Lim, Sung-Bin
    • Journal of Periodontal and Implant Science
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    • v.34 no.1
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    • pp.71-81
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    • 2004
  • Peri-implantitis could be the result of biomechanical and occlusal overload as well as microbiologic invasion. The dental implant may be more susceptible to dental plaque than the natural tooth, as the predictability of a stable soft tissue attachment complex has not yet been confirmed. With the development of peri-implantitis, the implant surface would be exposed to the oral environment and becomes coated with bacteria. The objective of therapy for this condition is to regain integration of the implant with bone. Since fibroblast adherence to surfaces is impeded by endotoxin, it would seem that decontamination would be desirable to obtain maximum osseointegration. The purpose of this study was to determine whether various chemotherapeutic and mechanical treatments(distilled water, air-powder abrasive, hypersaturated citric acid, tetracycline) can detoxify contaminated titanium implant surface by means of kinetic LAL test. Experimental rough surface titanium disks were fabricated. All of them were divided into two groups(A.a group and P.g group) and each contaminated by A. actinomycetemcomitans and P. gingivalis suspension. Contaminated disks were treated with distilled water, air-powder abrasive, citric acid and tetracycline, and then all disks were placed into LPS-free water for elution. The results were as follows : 1. In A.a group, LPS elute level of all test groups were significantly lower than control group(p<0.05). 2. In A.a group, LPS elute level of test 2, test 3 and test4 groups were significantly lower than that of control group(p<0.05). But, among the test 2, test 3, test4 groups, the significant differences were not detected. 3. In P.g group, LPS elute level of test 2, test 3 and test 4 groups were lower than that of control group(p<0.05). But, among the test groups, the significant differences were not detected. From the result of this study, it would be concluded that air-powder abrasive, hypersaturated citric acid and tetracycline treatments may be effective at reducing endotoxin level on rough titanium implant surfaces, and can be clinically used. But the treatments in peri-implantitis differentially impact osseointegration making one method clinically superior. To gain this knowledges, further molecular biologic and histopathologic studies should be developed.

A Study of Toothpaste Containing Pyrophosphates and Cellulose on the Abrasivity and Cleaning Power (피로인산염과 셀룰로오스 배합 세치제의 마모력과 세정력에 관한 연구)

  • Kim, Byung-Jun;Kim, Ji-Hye;Ha, Won-Ho;Ahn, Jae-Hyun
    • Journal of dental hygiene science
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    • v.13 no.1
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    • pp.83-90
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    • 2013
  • The aim of this study was to evaluate the abrasive effect and cleaning power of toothpaste containing tetrasodium pyrophosphate and cellulose. The relative dentin abrasivity, cleaning power by modified Stookey method, dentin abrasivity of brushing after Cola treatment and consumer survey were investigated with control toothpaste containing dental type silica as an abrasive. The results obtained were as follows: 1. Experimental toothpaste hardly influenced dentin abrasivity, but control toothpaste had an effect on dentin abrasivity significantly (p<0.05). 2. There was no significant difference in cleaning power between experimental and control toothpaste (p>0.05). 3. Experimental toothpaste hardly influenced dentin abrasivity, despite 100 or 1,000 times of brushing after Cola treatment, but control toothpaste showed a big increase in dentin abrasivity as the number of brushing has been increased (p<0.05). 4. According to the consumer survey results, there was no difference between control and experimental toothpaste in the satisfaction rate of refreshing sensation, the satisfaction rate of the lasting effect of refreshing sensation and the overall satisfaction rate of the toothpaste (p>0.05). These results showed a possibility to make abrasive free toothpaste having cleaning power without dentin abrasivity.

A Study on Coating Performance Design for Ice Belt Zone of the Arctic Vessels (극지 운항 선박 Ice Belt Zone의 도장 사양 설계 연구)

  • Baek, Yun-Ho;Park, Chung-Seo;So, Yong-Shin
    • Special Issue of the Society of Naval Architects of Korea
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    • 2013.12a
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    • pp.66-72
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    • 2013
  • The demand for an ice class ship is rising expected to rise according to the increase of energy consumption and the opening of arctic sea routes. Ice class ship should be designed to cope with the severe environmental conditions of arctic sea such as a high mechanical impact and abrasion damage, caused by pack ice, ice bergs and low temperature. The ice class ship hulls are coated with an anti-abrasion and low friction coating such as a solvent free epoxy or high solid-volume epoxy. These coatings require two-component heating pump and a high grade surface preparation. In this study, the coating performances for the arctic vessels, such as puncture absorbed energy, abrasive wear loss, friction coefficients and impact absorbed energy were evaluated. Based on this study, a proper coating performance specification for the arctic vessels was proposed and coating selection guideline in terms of coating performance and workability was also established.

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Surface Characterization of Cu as Electrolyte in ECMP (ECMP 공정에서 전해질에 따른 Cu 표면 특성 평가)

  • Kwon, Tae-Young;Kim, In-Kwon;Cho, Byung-Gwun;Park, Jin-Goo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.528-528
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    • 2007
  • Cu CMP widely has been using for the formation of multilevel metal interconnects by the Cu damascene process. And lower dielectric constant materials are required for the below 45nm technology node. As the dielectric constant of dielectric materials are smaller, the strength of dielectric materials become weaker. Therefore these materials are easily damaged by high down pressure during conventional CMP. Also, technical problems such as surface scratches, delamination, dishing and erosion are also occurred. In order to overcome these problems in CMP, the ECMP (electro-chemical mechanical planarization) has been introduced. In this process, abrasive free electrolyte, soft pad and low down force were used. The electrolyte is one of important factor to solve these problems. Also, additives are required to improve the removal rate, uniformity, surface roughness, defects, and so on. In this study, KOH and $NaNO_3$ based electrolytes were used for Cu ECMP and the electrochemical behavior was evaluated by the potentiostat. Also, the Cu surface was observed by SEM as a function of applied voltage and chemical concentration.

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Apple Virus Diagnosis Using Simplified RNA Extraction Method (사과바이러스 간편 진단을 위한 RNA추출법 개선)

  • Shin, Dong-Il;Park, Hee-Sung
    • Journal of agriculture & life science
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    • v.43 no.6
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    • pp.105-109
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    • 2009
  • Kyungsan nursery complex which has a vast area for the production of various species of fruit tree stocks is in a high demand of virus-free saplings. Apple tree stocks, the most important products, urgently need more rapid and reliable viral diagnosis. In this study, a bead beater was tested because of convenience in dealing with large number of samples. Also, industrial glass bead abrasive (0.4 mm in diameter) at very low cost was used in a disposable way. For bead beater-aided RNA extraction from apple stem tissues, the guanidine thiocyanate method was confirmed to be very reliable. Silca membrane filter tube in connection to vacuum filtering device was strongly suggested for simplifying RNA capture and washing steps. Apple virus detection was confirmed by RT-PCR.

Effects of Electron Beam Irradiation on Tribological and Physico-chemical Properties of Polyoxymethylene (POM-C) copolymer

  • Rahman, Md. Shahinur;Yang, Jong-Keun;Shaislamov, Ulugbek;Lyakhov, Konstantin;Kim, Min-Seok;Lee, Heon-Ju
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.153-153
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    • 2016
  • Polyoxymethylene copolymer (POM-C) is an attractive and widely used engineering thermoplastic across many industrial sectors owing to outstanding physical, mechanical, self-lubricating and chemical properties. In this research work, the POM-C blocks were irradiated with 1 MeV electron beam energy in five doses (100, 200, 300, 500 and 700 KGy) in vacuum condition at room temperature. The tribological and physico-chemical properties of electron beam irradiated POM-C blocks have been analyzed using Pin on disk tribometer, Raman spectroscopy, SEM-EDS, Optical microscopy, 3D Nano surface profiler system and Contact angle analyzer. Electron beam irradiation at a dose of 100 kGy resulted in a decrease of the friction coefficient and wear loss of POM-C block due to well suited cross-linking, carbonization, free radicals formation and energetic electrons-atoms collisions (physical interaction). It also shows lowest surface roughness and highest water contact angle among all unirradiated and irradiated POM-C blocks. The irradiation doses at 200, 300, 500 and 700 kGy resulted in increase of the friction coefficient as compared to unirradiated POM-C block due to severe chain scission, chemical and physical structural degradation. The electron beam irradiation transferred the wear of unirradiated POM-C block from the abrasive wear, adhesive wear and scraping to mild scraping for the 1 MeV, 100 kGy irradiated POM-C block which is concluded from SEM-EDS and Optical microscopic observations. The degree of improvement for tribological attribute relies on the electron beam irradiation condition (energy and dose rate).

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A Study on Fabrication Conditions of Al-SiCp Composites by Squeeze Casting (Squeeze Casting에 의한 Al-SiCp 복합재료의 제조 조건에 관한 연구)

  • Kim, Sug-Won;Woo, Kee-Do;Han, Sang-Won
    • Journal of Korea Foundry Society
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    • v.14 no.5
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    • pp.471-479
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    • 1994
  • Al-2%Si-2%Mg alloy containing SiC particle in 20, $70{\mu}m$ were prepared by mean of squeeze casting with various pressure 50, 100, 150 and 220MPa respectively. The specimens were made by casting into $50{\Phi}{\times}100{\ell}$ mold under various squeeze conditions(pressures, pressurizing temperature, particle sizes). Mechanical properties(hardness, tensile strength, elongation and wear characteristics) were evaluated at room temperature with those various fabrication factors. It became feasible to make favorable Al-SiCp composite free from casting defects by the injection of Ar gas during melting and 100MPa pressure squeeze casting. However, pressure of 50MPa was not sufficient to avoid completely porosity formation as a result of precessing and shrinkage during solidification. As the particle size is smaller and the squeeze pressure is higher, the hardness and tensile strength at room temperature are higher. Cell size became smaller gradually with increase of squeeze pressure. With increase of squeeze pressure(MPa), wear behaviors of those composites were changed from adhesive into abrasive wear, and the tendency of above behavior became outstanding with increasing sliding speed. The chemical reaction(4Al+3SiC${\rightarrow}$$Al_4C_3+3Si$) is more accelerated at interface between SiCp and matrix with increase of squeeze pressure. Therefore $Al_4C_3$ intercompound and Si peak intensity is increased at interface.

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Preparation of Cross-sectional Specimen for High Resolution Observation of Coating Structure and Visualization of Styrene/butadiene Latex Binder (고배율 도공층 구조 및 S/B latex 분포 분석을 위한 도공층 횡단면 제작)

  • Kim, Chae-Hoon;Youn, Hye-Jung;Lee, Hak-Lae
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.44 no.4
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    • pp.16-24
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    • 2012
  • To characterize the coating structure, diverse methods such as mercury intrusion, nitrogen adsorption and oil absorption methods have been developed and widely employed. These indirect techniques, however, have some limitation to explain the actual coating structure. Recently microscopic observation methods have been tried for analyzing structural characteristics of coating layers. Preparation of the undamaged cross section of a coating layer is essential for obtaining high quality image for analysis. In this study, distortion-free cross-section of the coating layer was prepared using a grinding and polishing technique. The coated paper was embedded in epoxy resin and cured. After curing the resin block it was ground with abrasive papers and then polished with diamond particle suspension and nylon cloth. Polished coating layer was sufficient enough to obtain undamaged cross sectional images with scanning electron microscope under backscattered electron image mode. In addition, the SEM images allowed distinction of the coating layer components. Also S/B latex film formed between pigment particles was visualized by osmium tetroxide staining. Pore size distribution and pore orientation were evaluated by image analysis from SEM cross-sectional images.

A study on material removal characteristics of MR fluid jet polishing system through flow analysis (유동해석을 통한 MR fluid jet polishing 시스템의 재료제거 특성 분석)

  • Sin, Bong-Cheol;Lim, Dong-Wook;Lee, Jung-Won
    • Design & Manufacturing
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    • v.13 no.3
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    • pp.12-18
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    • 2019
  • Fluid jet polishing is a method of jetting a fluid to polish a concave or free-form surface. However, the fluid jet method is difficult to form a stable polishing spot because of the lack of concentration. In order to solve this problem, MR fluid jet polishing system using an abrasive mixed with an MR fluid whose viscosity changes according to the intensity of a magnetic field is under study. MR fluid jet polishing is not easy to formulate for precise optimal conditions and material removal due to numerous fluid compositions and process conditions. Therefore, in this paper, quantitative data on the factors that have significant influence on the machining conditions are presented using various simulations and the correlation studies are conducted. In order to verify applicability of the fabricated MR fluid jet polishing system by nozzle diameter, the flow pattern and velocity distribution of MR fluid and polishing slurry of MR fluid jet polishing were analyzed by flow analysis and shear stress due to magnetic field changes was analyzed. The MR fluid of the MR fluid jet polishing and the flow pattern and velocity distribution of the polishing slurry were analyzed according to the nozzle diameter and the effects of nozzle diameter on the polishing effect were discussed. The analysis showed that the maximum shear stress was 0.45 mm at the diameter of 0.5 mm, 0.73 mm at 1.0 mm, and 1.24 mm at 1.5 mm. The cross-sectional shape is symmetrical and smooth W-shape is generated, which is consistent with typical fluid spray polishing result. Therefore, it was confirmed that the high-quality surface polishing process can be stably performed using the developed system.

Effects of Increasing Ambient Temperatures on the Static Load Performance and Surface Coating of a Gas Foil Thrust Bearing (외기 온도 증가가 가스 포일 스러스트 베어링의 하중지지 성능과 표면 코팅에 미치는 영향)

  • Hyunwoo Cho;Youngwoo Kim;Yongbum Kwon;Tae Ho Kim
    • Tribology and Lubricants
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    • v.40 no.3
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    • pp.103-110
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    • 2024
  • Gas foil thrust bearings (GFTBs) are oil-free self-acting hydrodynamic bearings that support axial loads with a low friction during airborne operation. They need solid lubricants to reduce dry-friction between the runner and top foil and minimize local wears on their surfaces during start-up and shutdown processes. In this study, we evaluate the lift-off speeds and load capacity performance of a GFTB with Polytetrafluoroethylene (PTFE) surface coating by measuring drag torques during a series of experimental tests at increasing ambient temperatures of 25, 75 and 110℃. An electric heat gun provides hot air to the test GFTB operating in the closed booth to increase the ambient temperature. Test results show that the increasing ambient temperature delays the lift-off speed and decreases the load capacity of the test GFTB. An early developed prediction tool well predicts the measured drag torques at 60 krpm. After all tests, post inspections of the surface coating of the top foil are conducted. Scanning electron microscope (SEM) images imply that abrasive wear and oxidation wear are dominant during the tests at 25℃ and 110℃, respectively. A quantitative energy dispersive spectroscopy (EDS) microanalysis reveals that the weight percentages of carbon, oxygen, and nitrogen decrease, while that of fluorine increases significantly during the highest-temperature tests. The study demonstrates that the increasing ambient temperature noticeably deteriorates the static performances and degrades the surface coating of the test GFTB.