• Title/Summary/Keyword: fracture morphology

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Fabrication and Characterization of Alumina/Silver Nanocomposites

  • Cheon, Seung-Ho;Han, In-Sub;Woo, Sang-Kuk
    • Journal of the Korean Ceramic Society
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    • v.44 no.7
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    • pp.343-348
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    • 2007
  • Alumina/silver nanocomposites were fabricated using a soaking method through a sol-gel route to construct an intra-type nanostructure. The pulse electric-current sintering (PECS) technique was used to sinter the nanocomposites. Several specimens were annealed after sintering. The microstructure, mechanical properties, critical frontal process zone (FPZ) size, and thermo-mechanical properties of the nanocomposites were estimated. The relative densities of the specimens sintered at 1350 and $1450^{\circ}C$ were 95% and 99%, respectively. The maximum value of the three-point bending strength was found to be 780 MPa for the $2{\times}2{\times}10 mm$ specimen sintered at $1350^{\circ}C$. The fracture toughness of the specimen sintered at $1350^{\circ}C$ was measured to be $3.60 MPa{\cdot}m^{1/2}$ using the single-edge V-notched beam (SEVNB) technique. The fracture mode of the nanocomposites was transgranular, in contrast to the intergranular mode of monolithic alumina. The fracture morphology suggested that dislocations were generated around the silver nanoparticles dispersed within the alumina matrix. The specimens sintered at $1350^{\circ}C$ were annealed at $800^{\circ}C$ for 5 min, following which the maximum fracture strength became 810 MPa and the fracture toughness improved to $4.21 MPam^{1/2}$. The critical FPZ size was the largest for the specimen annealed at $800^{\circ}C$ for 5 min. Thermal conductivity of the alumina/silver nanocomposites sintered at $1350^{\circ}C$ was 38 W/mK at room temperature, which was higher than the value obtained with the law of mixture.

Failure Behavior of Laser Cladding Layer used by Fe-based Bulk Metallic Glass (Fe계 벌크 비정질 합금을 이용한 레이저 용접층의 파손 거동)

  • Lim, Byung-Chul;Kim, Dae-Hwan;Park, Sang-Heup
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.9
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    • pp.5743-5747
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    • 2015
  • In this study, Fe-based bulk amorphous alloy powder manufactured using gas atomization fabrication was used for laser welding. the fracture behavior of welding layer were analyzed. Tensile test results show that the destruction occurred immediately after the elastic deformation, After plastic deformation of the substrate, the destruction occurred. The actual maximum tensile strength of the welding layer and the substrate are 959.9MPa and 220.4MPa. welding layer were each $485.5{\pm}21$ and $197.4{\pm}14$ to the substrate and the actual microhardness, The welding layer has very high hardness. The welding layer showed a very weak fine acicular structure. The base material was shown in the micro structure appear a coarse grain. SEM observations of the fracture after the tensile test. Fracture morphology of the base metal and the welding layer showed ductile fracture and brittle fracture, respectively.

A study on the Faigue Behavior and Mechanism of High Hardened Steel (고판도강재의 피로거동과 기구)

  • ;Song, Sam Hong
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.3 no.3
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    • pp.116-123
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    • 1979
  • On the basis of optical microscope and electro microscope observation for the fatigue fracture process of medium corbon martensitic structure produced by rapid heat treatment, mainly the abstracts of the studied results for the morphology of fatigue crack initiation process of high hardened steel are summarized as follows. Fatigue crack initiated from inclusion on the surface or subsurface. Above all the crack which initiated from inclusion exposed on the surface in as follows. (1) fatigue crack initiated from the boundary of the matrix and inclusion. (2) fatigue crack initiated at surrounding of small pit by drop out of inclusion.

Vacuum Casting of Mn-Zn Ferrite Powders Prepared by Alcoholic Dehydration Method (알콜탈수법에 의해 제조된 Mn-Zn Ferrite 미분체의 진공주입성형)

  • 이경직;이대희;김창현;이창섭;이석기;이병교
    • Journal of the Korean Ceramic Society
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    • v.34 no.11
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    • pp.1107-1112
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    • 1997
  • Mn-Zn ferrite powders prepared by an alcoholic dehydration method. Vacuum casting, a kind of wet forming process was examined with this powders. As binders, polyethylene glycol and polyvinyl alcohol were used. In order to estimate this conditions, fracture morphology, densities of green and sintered bodies and the microstructure were observed. High density and homogeneous microstructure in sintered bodies were obtained in the case of 0.1 wt% PEG or 0.5 wt% PVA.

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Failure Analysis of Circulating Water Pump Shaft in Power Plant (발전 계획에서 순환 물 펌프 고장 분석)

  • Lee, Jaehong;Jung, Nam-gun
    • KEPCO Journal on Electric Power and Energy
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    • v.7 no.1
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    • pp.125-128
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    • 2021
  • This paper presents the root cause failure analysis of the circulating water pump in the 560 MW thermal power plant. A fractured austenitic stainless-steel shaft operated for 24 years was examined. Fracture morphology was investigated by micro and macro-fractographic analysis. The metallurgical analyses including chemical analysis, metallography and hardness testing were performed. The analysis reveals that the pump shaft was fractured due to the reverse bending load with combination of rotating bending load. Corrective actions for plant operator was recommended based on the analysis.

Effect of morphology and diameter of implant fixture-abutment connection on mechanical failure of implants (임플랜트 고정체-지대주 연결부의 형태와 직경이 임플랜트의 기계적 실패에 미치는 영향)

  • Yun, Bo-Hyeok;Shin, Hyon-Mo;Yun, Mi-Jung;Huh, Jung-Bo;Jeong, Chang-Mo;Kang, Eun-Sook
    • The Journal of the Korean dental association
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    • v.53 no.9
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    • pp.644-655
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    • 2015
  • Purpose: This study was conducted to evaluate the effect of the fixture abutment connection type and diameter on the screw joint stability in external butt joint for 2nd surgery and internal cone connected type implant system for 1st and 2nd surgery using ultimate fracture strength. Materials and Methods: USII system, SSII system and GSII system of Osstem Implant were used. Each system used the fixture with two different diameters and cement-retained abutments, and tungsten carbide / carbon coated abutment screws were used. Disc shaped stainless steel metal tube was attached using resin-based temporary cement. The experimental group was divided into seven subgroups, including the platform switching shaped specimen that uses a regular abutment in the fixture with a wide diameter in USII system. A static load was increased to the metal tube at 5mm deviated point from the implant central axis until it reached the compression bending strength at a rate of 1mm/min. Then the deformations and patterns of fracture in threaded connection were compared. Results and Conclusion: 1. In the comparison between the Regular diameter, compression bending strength of SSII system was higher than USII system and GSII system. There was no significant difference between USII system and GSII system. 2. In the comparison between wide diameter, compression bending strength was increased in the order of GSII system, USII system, and SSII system. 3. In comparison between the implant diameter, compression bending strength of the wide diameter was greater than the regular diameter in any system(P<0.05). 4. There was no significant difference between the platform switching (III group) and the regular diameter (I group) in USII system. 5. In USII system, fracture of abutment screw and deformation of both fixture and abutment were observed in I, II and III subgroups. 6. Failure pattern of SSII system, which was the fracture of abutment screw and deformation of the abutment and fixture, was observed in both IV and V subgroups. Fracture of some fixtures was observed in subgroup V. 7. Failure pattern of GSII system, which was the fracture of the abutment screw and deformation of the fixture and the abutment, was observed in both VI and VII subgroups. Apart from other subgroups, subgroup VII demonstrated no bending neither the fracture at the top of the fixture. The compressive deformation of internal slope in the fixture was the only thing observed in subgroup VII.

Behavior of Eutectic Si and Mechanical Properties of Sr Modified Al-7Si-0.35Mg alloy with Solid Solution Treatment for Sand Casting (Sr 개량처리된 사형주조 Al-7Si-0.35Mg 합금의 열처리에 따른 공정 Si상 변화거동 및 특성평가)

  • Kim, Myoung-Gyun;Hwang, Seok-Min
    • Journal of Korea Foundry Society
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    • v.38 no.1
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    • pp.1-8
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    • 2018
  • In this study, we focused on the correlation between the solidification structure, heat treatment and mechanical properties of the A356 alloy according to the conditions of Sr modification. The microstructural evolution of the eutectic Si and ${\alpha}-Al$ phase in the A356 alloy castings depending on the amount of Sr were investigated during solid solution heat treatment using an optical microscope, a scanning electron microscope and an image analyzer. In addition, tensile tests on the heat treated materials examined the relationship between the microstructure and the fracture surface. The as-cast A356 alloys under 40 ppm Sr showed an undermodified microstructure, but that of the added 60-80 ppm Sr had well modified structure of fine fibrous silicon. After solid solution treatment, the microstructure of the undermodified A356 alloy exhibited a partially spheroidized morphology, but the remainder showed the fragmentation of fibrous shaped silicon. The spheroidization of the eutectic silicon in the modified A356 alloys was completed during heat treatment, which was very effective in increasing the elongation. This is supported by the fracture surface in the tensile test.

Mechanical Behaviour of Non-Oxide Boride Type Ceramics Formed on The AISI 1040 Plain Carbon Steel

  • Sen, Saduman;Usta, Metin;Bindal, Cuma;UciSik, A.Hikmet
    • The Korean Journal of Ceramics
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    • v.6 no.1
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    • pp.27-31
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    • 2000
  • A series experiments were performed to evaluate mechanical behavior of non-oxide boride type ceramics formed on the AISI 1040 plain carbon steel. Boronizing was performed in a slurry salt bath consisting of borax, boric acid, and ferro-silicon at $950^{\circ}C$ for 2-6h. The AISI 1040 steel used as substrate material was containing 0.4%C, 0.13%Si, 0.65%Mn, 0.02%P, 0.014%S. The presence of non-oxide boride type ceramics $Fe_2B $ and FeB formed on the surface of steel was confirmed by metallographic technique and X-ray diffraction (XRD) analysis. The hardness of borides measured via Vickers indenter with a load of 2N reached a microhardness of up to 1800 DPN. The hardness of unborided steel was 185 DPN. The fracture toughness of borides measured by means of Vickers indenter with a load of 10N was about 2.30 MPa.$m^{1/2}$. The thickness of boride layers ranged from 72$\mu\textrm{m}$ to 145$\mu\textrm{m}$. Boride layers have a columnar morphology.

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An Experimental Study on the Change of the Material Properties and the Fatigue Life of Natural Rubber due to Carbon Black (카본블랙에 의한 천연고무 물성치와 피로수명 변화에 대한 실험적 연구)

  • Kim, Jae-Hun;Kim, Yeong-Hak;Jeong, Hyeon-Yong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.11
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    • pp.1887-1894
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    • 2001
  • The effects of carbon black on the material properties and the fatigue life of the carbon-black filled natural rubbers were investigated. Different kinds of carbon blacks resulted in different fatigue lives, hysteresis, and critical J-values. It was noticed that the hysteresis was inversely proportional to the difference between DBPA and CTAB, and the critical J-value was almost the same regardless of the length of a precrack. In addition, different kinds of carbon blacks resulted in different fracture morphologies, and micro-scale and macro-scale roughnesses. The critical J-value was proportional to the micro-scale roughness. and it seemed relate to the size distribution of carbon black particles. By reviewing all the experimental data. it was finally noticed that the logarithmic value of the fatigue life could be linearly expressed by a multiplication of the critical J-value and the logarithmic value of the hysteresis.

Toughness Improvement of Tetrafunctional Epoxy Resin with Thermoplastic Polymer (열가소성 고분자를 이용한 사관능성 에폭시 수지의 강인성 향상에 관한 연구)

  • Shim, Jyong-Sup;Jung, Ho-Soon;Jang, Jyong-Sik
    • Applied Chemistry for Engineering
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    • v.1 no.2
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    • pp.124-132
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    • 1990
  • In order to improve the mechanical properties and fracture toughness of HPT 1071/DDS system, poly(aryl etherimide) (PEI) was incorporated in the resin system. In HPT 1071/DDS system, mechanical properties of cured epoxy resins were not strongly dependent on the concentration of DDS curing agent strongly. In the case of HPT 1071/DDS/PEI system, the fracture toughness and flexural properties of epoxy resins increased with increasing the concentration of PEI. SEM micrographs of cured epoxy resin indicated that the phase separation occured at the low concentration of PEI in this system. In addition, investigation of the relationship between mechanical properties and the morphology of modified epoxy resin was undertaken in HPT 1071/DDS/PEI system.

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