• Title/Summary/Keyword: fractional extraction

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Fractional Extraction of DHA and EPA by Supercritical Fluid (DHA와 EPA에 대한 초임계 유체의 분할추출)

  • Hur, Byung-Ki;Noh, Duck-Woo
    • KSBB Journal
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    • v.14 no.6
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    • pp.655-660
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    • 1999
  • Supercritical fractional extraction of DHA and EPA from the mixture of fatty acids composing the fish oil was performed. The compositions, extracted quantities, and cumulative extracted quantities of fatty acids in the extract and the raffinate were investigated according to the fractional steps. The temperature and pressure for the miximum concentration of DHA and EPA in the extract or the raffinate were 60$^{\circ}C$ and 101 bar respectively among the extraction conditions considered in this study. In this case, the weight percent of EPA in the extract was 50% and that of DHA in the raffinate was 40%. These values were two times higher than those in fish oil. THe same temperature and pressure were used to extract DHA and EPA from the mixture of fatty acids whose the initial weight percent of DHA was 34%. The weight percent of DHA in the raffinate after the fourth fractionation was 7-%. And the remaining weight of DHA in the raffinate was 80% of DHA initially loaded in the extraction vessel.

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Optimization of Beverage Preparation from Schizandra chinensis Baillon by Response Surface Methodlogy (반응표면 방법에 의한 오미자 음료 제조의 최적화)

  • Kang, Kyoo-Chan;Park, Jae-Han;Baek, Sang-Bong;Jhin, Hong-Seung;Rhee, Kyu-Soon
    • Korean Journal of Food Science and Technology
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    • v.24 no.1
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    • pp.74-81
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    • 1992
  • To develop the beverage from Schizandra chinensis Baillon, extraction condition was optimized, using the fractional factorial design with 3 variables and 3 levels, by a RSM computer program. The optimum extraction time, extraction temperature and alcohol concentration levels were 3 hrs, $80{\sim}85^{\circ}C$ and 0%(water) for a desired yield, color and non-volatile organic acid. And to obtain the optimum recipe, amounts of extract, sugar and citric acid were optimized, using the fractional factorial design with 3 variables and 3 levels, by a RSM program. The optimum extract, sugar and citric acid levels were 4%, 9.6%n and 0.06%, respectively, for a disired flavor and overall acceptance.

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Optimization of Aqueous Methanol Extraction Condition of Total Polyphenol from Spent $Lycium$ $chinense$ Miller to Develop Feed Additives for Pig (양돈용 사료 첨가제 개발을 위하여 구기자 부산물로부터 메탄올수용액을 이용한 총 폴리페놀 추출조건 최적화)

  • Shim, Kwan-Seob;Na, Chong-Sam;Oh, Sung-Jin;Choi, Nag-Jin
    • Korean Journal of Organic Agriculture
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    • v.20 no.1
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    • pp.91-99
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    • 2012
  • This study was conducted to develop a functional feed additive for pig with spent $Lycium$ $chinense$ Mill fruit. We investigated the optimum conditions for the extraction of polyphenol from spent $Lycium$ $chinense$ Mill using methanol. Methanol concentration as a solvent for extraction, extraction time and the volume of solvent per a gram of solid (ground spent Lyceum chinense Mill) were selected as parameters. Three levels of parameters were configured according to Box Behnken experiment design, a fractional factorial design, and total 15 trials were employed. Total polyphenol concentration from each trial was used as response from experiment system and effects of parameters on total polyphenol extraction efficiency were determined using response surface model. As a result, all terms in analysis of variance, regression ($p$ = 0.001), linear ($p$ = 0.002), square ($p$ = 0.017) and interaction ($p$ = 0.047) was significant and adjusted determination coefficient ($R^2$) was 94.7%. Total polyphenol extraction efficiency was elevated along increased methanol content and decreased solvent to solid ratio. However extraction time did not affect the efficiency. This study provides a primary information for the optimum extraction conditions to maximize total polyphenol recovery from spent Lycium chinens Mill fruit and this result could be applied to re-use of argo-industrial by-products and to develop of functional feed additives in organic farming.

Optimization of Saponin Extraction Conditions in Ginseng Milk using Response Surface Methodology (반응표면분석 법을 이용한 인삼우유 중 사포닌 추출조건의 최적화)

  • 이승수;박종면
    • Journal of Ginseng Research
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    • v.18 no.1
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    • pp.53-59
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    • 1994
  • To develop the methodology of the quantitative analysis of saponin in ginseng milk, conditions of the saponin extraction were optimized using the fractional factorial design with 3 variables and 3 levels by a RSM computer program. The extraction of saponin increased with an increase in extraction temperature up to $90^{\circ}C$ and then decreased significantly at $100^{\circ}C$. Extraction time affected the saponin yield in a similar trend. On the other hand, decreasing cooling temperature increased the amount of the saponin extracted. Recovery yield of the saponin from ginseng milk varied from 70.0% to 92.9%. The optimum extraction temperature, time and cooling temperature determined by partial differentiation of the model equation were $86^{\circ}C$, 2.83 hrs and $4^{\circ}C$, respectively. Key words Ginseng milk, saponin, response surface methodology.

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Studies on the Extracting Methods of Ginseng Extract and Saponins in Panax Ginseng (유출조건에 따른 인삼중의 Ginseng Extract와 Saponin 합량변화에 관한 연구)

  • 주현규;조규성
    • Journal of Ginseng Research
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    • v.3 no.1
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    • pp.40-53
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    • 1979
  • In order to investigate the optimal conditions which affects to extraction of ginseng extract and saponin in ginseng extract, experiment was carried out varing with ethanol percentage, extraction time, temperature, sol$.$vent and Plant Parts. The results art as follows: 1. The amounts of ginseng saponin was increased according to increanation of ethanol Percentage while the amounts of ginseng extract was decreased. 2. The amounts of ginseng extract was increased as the prolongation of extraction time, on the ether hand, ginseng saponin contents increased lentil 40hr. and decreased after that. 3. By the raise of extract temperature, both of the amounts of ginseng saponin and ginseng extract was increased two times and four times. respectively. 4. The total amounts ginseng extract was obtained 22.86u when the water used as the extraction solvent, 11.28% on ethanol and 11.04U on methanol, in the order. and the saponin contents gained when the extraction solvents of water, methanol and ethanol 7.47%, 12.36% and 12.77%, respectively. 5. It showed 9.23% of ginseng extract in epidermis and 8.4% of ginseng saponin in tail Part of raw ginseng and in the case of dried ginseng, ginseng extract and saponin showed the most amounts in epidermis of 18.28% and 19.35%, respectively. 6. The ratio of panaxadiol and panaxatriol contents of ginseng saponin was almost same when it was extracted varing with ethanol percentage and extraction time (duration), and the more alcohol percentage and the longer extraction time increased, the more fractional content of ginseng saponin was extracted.

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Multi-aspect Based Active Sonar Target Classification (다중 자세각 기반의 능동소나 표적 식별)

  • Seok, Jongwon
    • Journal of Korea Multimedia Society
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    • v.19 no.10
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    • pp.1775-1781
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    • 2016
  • Generally, in the underwater target recognition, feature vectors are extracted from the target signal utilizing spatial information according to target shape/material characteristics. In addition, various signal processing techniques have been studied to extract feature vectors which are less sensitive to the location of the receiver. In this paper, we synthesized active echo signals using 3-dimensional highlight distribution. Then, Fractional Fourier transform was applied to echo signals to extract signal features. For the performance verification, classification experiments were performed using backpropagation and probabilistic neural network classifiers based on single aspect and multi-aspect method. As a result, we obtained a better recognition result using proposed feature extraction and multi-aspect based method.

Signal Synthesis and Feature Extraction for Active Sonar Target Classification (능동소나 표적 인식을 위한 신호합성 및 특징추출)

  • Uh, Y.;Seok, J.W.
    • Journal of Korea Multimedia Society
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    • v.18 no.1
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    • pp.9-16
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    • 2015
  • Various approaches to process active sonar signals are under study, but there are many problems to be considered. The sonar signals are distorted by the underwater environment, and the spatio-temporal and spectral characteristics of active sonar signals change in accordance with the aspect of the target even though they come from the same one. And it has difficulties in collecting actual underwater data. In this paper, we synthesized active target echoes based on ray tracing algorithm using target model having 3-dimensional highlight distribution. Then, Fractional Fourier transform was applied to synthesized target echoes to extract feature vector. Recognition experiment was performed using probabilistic neural network classifier.

Optimal Conditions for Extraction of Anthocyan from Celosia cristata L., Brassica juncea czerniak et coss, Beta vulgaris L. for manufacture of Color Dongchimi (컬러동치미 제조를 위한 홍갓, 맨드라미, 비트에 함유된 안토사이안 색소의 최적 추출 조건)

  • Kim, Mi-Hye
    • Journal of the Korean Society of Food Culture
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    • v.27 no.6
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    • pp.686-694
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    • 2012
  • This study was conducted to develop a method to change the color of traditional Dongchimi using natural dyes to meet changing consumer demands. It was intended to improve the manufacturing process ability for color Dongchimi, and the best optimum extraction solvent and method from the natural dyes were proven to be confirmed and valid. The extraction process was evaluated using different solvents including distilled water, 20% ethyl alcohol, and 1% citric acid, and the quantity of the extracted anthocyanin was then measured based on the absorbance. The greatest absorbance was observed when 1% citric acid was used. Based on these findings, it would be most efficient to allow the traditional Dongchimi to produce citric acid naturally instead of using artificial additives during its production. Celosia cristata L. was extracted in its largest quantity when reacted with 20% ethyl alcohol. Therefore, instead of applying Celosia cristata L. to Dongchimi as the sub-ingredient during the preparatory stage, it will be more efficient to use Celosia cristata L. as the fractional ingredient in order to first extraction.

Optimization of Extraction Conditions for Hot Water Extracts from Chrysanthemum indicum L. by Response Surface Methodology (반응표면분석법을 이용한 감국(甘菊) 열수 추출물의 추출조건 최적화)

  • Yun, Ok-Hui;Jo, Jeong-Sun
    • Korean journal of food and cookery science
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    • v.23 no.1 s.97
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    • pp.1-8
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    • 2007
  • Extraction conditions were optimized using response surface methodology for preparing high-quality, hot water extracts from cultivated Chrysanthemum indicum L. petals. A fractional factorial design was applied to investigate the effects of added sample ratio ($X_1$), extraction temperature ($X_2$) and extraction time ($X_3$) variables on extract properties, such as, soluble solid contents ($Y_1$), sugar content ($Y_2$), ?E ($Y_3$), turbidity ($Y_4$), total phenol ($Y_5$) and DPPH ($Y_6$). Second-order models were employed to generate a 3-dimensional response surface for dependent variables and their coefficients of determination ($R^2$) ranged from 0.8408${\sim}$0.9914. The range of optimum conditions at $80^{\circ}C$ extraction for maximize characteristics of hot water extracts was 2.3${\sim}$2.7 g and 9.2${\sim}$11.2 hr.

Studies on the Manufacturing and Analysis of Wax for Thermostat for use in Cooling System of Automobile (자동차 냉각 시스템에 사용되는 thermostat용 wax의 제조 및 분석에 관한 연구)

  • Park, Kyoung-Suk;Choung, Suk-Jin
    • Applied Chemistry for Engineering
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    • v.7 no.1
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    • pp.1-8
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    • 1996
  • The component analysis of wax for detecting temperature in automobile thermostat of the automotive engine and manufacture of it with distillation and solvent extraction were progressed. From the lift test results of prepared samples, it was found that the solvent extracted samples were in the proper range for use as an automobile thermostat of the automotive engine. And more accurate wax could be manufactured by high vacuum fractional distillation and acid treatment after solvent extraction from crude oil pitch.

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