• Title/Summary/Keyword: forensic science

Search Result 459, Processing Time 0.045 seconds

Washing effect of fingermark contaminated with flammable liquids (인화성액체에 오염된 지문의 세척 효과)

  • Ho-Won, Jang;Ji-Yun, Kwon;Hyo-Mi, Kim;Seung-Ju, Yoo;Sungwook, Hong
    • Analytical Science and Technology
    • /
    • v.35 no.6
    • /
    • pp.237-241
    • /
    • 2022
  • The effect of washing fingerprints deposited on glass that were contaminated with a flammable liquid (gasoline, kerosene, diesel, and thinner) was studied by washing with hexane or heptane. The fingerprints were visualized using fuming cyanoacrylate, followed by basic yellow 40 staining. After comparing the washing effect, by dividing one fingerprint into four sections, it was confirmed that the ridge detail was damaged by dissolving the fingerprints in flammable liquid. As a result of washing fingerprints contaminated with flammable liquids using hexane or heptane, fingerprints contaminated with gasoline, kerosene, and thinner did not show a washing effect because the ridge detail was damaged at the time of contamination, and only fingerprints contaminated with diesel exhibited improved ridge detail quality. Because hexane and heptane washing damage the ridge detail, it was found that fingerprints contaminated with gasoline, kerosene, and thinner were better enhanced directly without the washing process. In addition, it was found that the amount of the washing solvent and contact time should be minimized when washing fingerprints contaminated with diesel.

Effect of ethylenediamine on luminol (or Bluestar) - bleach reaction (Ethylenediamine이 luminol (or Bluestar) - 표백제 반응에 미치는 영향)

  • Seulgi, Jang;Minkyoung, Kim;Heejin, Kim;Munhee, Lee;Sungwook, Hong
    • Analytical Science and Technology
    • /
    • v.35 no.6
    • /
    • pp.242-248
    • /
    • 2022
  • The effect of ethylenediamine (EDA) on the reaction of luminol or Bluestar with blood and bleaches was studied. For this purpose, blood, chlorine bleach, and oxygen bleach were applied to filter paper, treated with EDA-containing luminol or Bluestar, and the changes in chemiluminescence intensity were observed. It was found that the chemiluminescence intensity of the luminol (or Bluestar)-blood reaction did not change with the increasing concentration of EDA. However, the chemiluminescence intensity of the luminol (or Bluestar)-chlorine bleach reaction decreased and the chemiluminescence intensity of the luminol (or Bluestar)-oxygen bleach reaction increased, with increasing EDA concentration. Thus, it was found that when EDA was added to luminol (or Bluestar), which is a blood-sensitive reagent, EDA suppressed the false-positive reaction induced by chlorine bleach and induced a false-positive reaction with oxygen bleach. Consequently, the addition of EDA is not recommended for enhancing bloodstains with luminol or Bluestar.

A case study on the fire victim in the vehicle by GC/MS through derivatization of cyanide with pentafluorobenzyl bromide (PFBBr) (시안화이온의 pentafluorobenzyl bromide (PFBBr)에 의한 유도체화 후 GC/MS 분석에 의한 차량화재 변사체 사인규명에 관한 사례연구)

  • Lee, Joon-Bae;Shon, Sung Kun;Woo, Sang Hee;Park, Se Yeon;Hwang, Jung Ho;Kwon, O-Seong;Kim, Nam Yi;Paeng, Ki Jung
    • Analytical Science and Technology
    • /
    • v.29 no.2
    • /
    • pp.73-78
    • /
    • 2016
  • Hydrogen cyanide (HCN) is an extremely toxic gas frequently produced during the incineration of plastics, such as acrylonitrile-butadiene-styrene (ABS). A victim of a fire who has inhaled smoke could have cyanide in the blood. Therefore, cyanide could be a good marker for a post-mortem examination of a fire as well as carboxyhemoglobine (COHb) test of blood samples. For a particular fire case, a burned body with a suicide note was found inside a burned vehicle. Even though the COHb value is conclusive evidence, measuring the COHb for denatured blood might be difficult due to severe thermal denaturation or the formation of methemoglobin (MetHb). To overcome this difficulty, cyanide could be used as an indicator when investigating the death of a fire victim. In this study, gas chromatography/mass spectrometry (GC/MS) was adopted to measure the levels of cyanide in the blood through derivatization with pentafluorobenzyl bromide (PFBBr) under cation surfactant by scan and SIM mode. The concentration of cyanide in the blood of heart blood and brain of the victim was found to be 0.36 µg/mL and 1.20 µg/mL respectively, which was higher than the average value (0.041 µg/mL) found in the blood of 14 people who smoked.

Smart Phone Copyright Violation and Forensic Apply Method (Smart Phone 저작권 위반과 포렌식 적용 방안)

  • Yi, Jeong-Hoon;Park, Dea-Woo
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
    • /
    • 2010.10a
    • /
    • pp.215-218
    • /
    • 2010
  • Smart Phone with domestic demand increasing rapidly, the utilization of multimedia services have become diverse. Accordingly, Smart Phone users to hack their Jail Breaking and Rooting and illegal use of the multimedia content is copyrighted. Also relevant to mobile communication terminal as a high crime, create, and the digital evidence increases the utilization of the mobile forensic evidence is required to study. In this paper, Smart Phone Copyright Violation and Forensic Apply Method research. Smart Phone Status and related violations of copyright infringement, broadcasting, film, music, e-book, etc. for each survey item, and how to apply for forensics were studied. This study investigated the development and forensic science will be able to contribute to the development.

  • PDF

Development of the Forensic Nursing Competency Scale for Nurses (간호사의 법의간호 역량 측정도구 개발)

  • Jo, Na Young;Kim, Min Hye;Lee, Yun Mi
    • Journal of Korean Critical Care Nursing
    • /
    • v.13 no.3
    • /
    • pp.24-40
    • /
    • 2020
  • Purpose : This study aims to develop the Forensic Nursing Competency Scale suitable to South Korea. Methods : The initial items were generated through literature review and interviews. Items were evaluated by experts for content and face validity. By conducting a pilot test, 74 measurement items were developed. In total, 333 copies of the questionnaire were analyzed regarding the validity and reliability of the study. Data were analyzed using SPSS 23.0 program and AMOS 18.0 program. Results : The study selected 53 questions after testing the content, face, and construct validity of the scale. The final 53 questions were composed of 15 sub-components in eight domains. These eight domains encompassed nursing practice, communication, critical thinking, human caring and relationships, evidence management, active information collection, professional development, and knowledge integration. Conclusions : In order to verify the effectiveness of the scale, future studies need to compare the forensic nursing competency in two groups to assess differences in these competency. Moreover, it is necessary to develop a forensic nursing educational program and validate its effectiveness by using this scale.

Development of dry-origin latent footwear impression on non-porous and semi-porous surfaces using a 5-methylthioninhydrin and L-alanine complex

  • Hong, Sungwook;Kim, Yeounjeung;Park, Jihye;Lee, Hoseon
    • Analytical Science and Technology
    • /
    • v.30 no.2
    • /
    • pp.75-81
    • /
    • 2017
  • 5-methylthioninhydrin (5-MTN) is an amino acid sensitive reagent used for the development of latent fingermarks deposited on porous surfaces such as paper and wood. The present study demonstrates that the 5-MTN can be used as a latent footwear impression enhancement reagent, by reacting with trace multivalent metal ions, which are the main components of the latent footwear impression. 5-MTN and L-alanine complex (MTN-ALA) used for the latent footwear impression development was prepared, by mixing $4.5{\times}10^{-3}M$ 5-MTN (in methanol) and $4.5{\times}10^{-3}M$ L-alanine (in methanol) in 1:1 ratio, and keeping undisturbed at room temperature for 24 h. The latent footwear impressions were deposited on white and black non-porous surfaces (glass plate, polyethylene panel, polypropylene panel, acryl panel, polyvinyl chloride (PVC) panel, poly(methyl methacrylate) (PMMA) panel, acrylonitrile-butadiene-styrene (ABS) panel, tile), and a semi-porous surfaces (painted wood). The latent footwear impressions on these surfaces were treated with MTN-ALA complex by spraying. The fluorescence of footwear impressions (occurred due to the reaction between MTN-ALA and metal complexes) was observed under a 505 nm forensic light source and an orange barrier filter. The enhancement of latent footwear impression was achieved from black surfaces without any blurring. However, the fluorescence (enhancement) of footwear impression was not observed on the white PVC, PMMA, and ABS surfaces, because the incident light interfered and reflected on the surface. The sensitivity of MTN-ALA was superior to 2,2'-dipyridil, which is a representative non-fluorescing footwear impression enhancement reagent, and similar to 8-hydroxyquinoline, which is a representative fluorescing footwear impression enhancement reagent.

Effect of silver (Ag) deposition before physical developer to develop latent fingerprints on wet paper (젖은 종이류에서 잠재지문을 현출하기 위한 physical developer 전 은 (Ag) 증착의 효과)

  • Wonyoung Lee;Min-Jeong Kang;Yoo-Jung Lee;Je-seol Yu
    • Analytical Science and Technology
    • /
    • v.36 no.6
    • /
    • pp.324-331
    • /
    • 2023
  • Latent fingerprints on wet paper cannot be developed using amino acid reaction reagents. Therefore, physical developer (PD) or lipid staining reagents like oil red O (ORO) should be utilized. However, ORO is not very effective in developing fingerprints that are older than approximately 4 weeks. On the other hand, PD performs well in developing older fingerprints, but it cannot do so for relatively fresh fingerprints. Additionally, PD has the disadvantage of taking a long time to develop fingerprints. In this study, in order to overcome the limitations of PD, we attempted to increase its reactivity by applying Ag-PD, which involves depositing silver onto paper using vacuum metal deposition (VMD), and compared this with fingerprints developed using ORO and PD. As a result, Ag-PD showed superior fingerprint development compared to ORO and PD on wet paper stored for 2~8 weeks, and the fingerprint development time for PD was significantly reduced to 90~150 seconds.

The Classification and Age Determination of Ballpoint Pen Inks in Questioned Documents

  • Kim, Nam Yee;Park, Sung Woo;Doble, Philip;Roux, Claude
    • Analytical Science and Technology
    • /
    • v.17 no.3
    • /
    • pp.271-277
    • /
    • 2004
  • The aim of this study was to investigate questioned documents written with blue or black ballpoint pen on paper by nondestructive technique. In this work, 21 blue and 22 black ballpoint pen inks which were purchased on different brands were analyzed by using Microspectrophotometry (MSP). The reflectance spectra were obtained from these ink samples and their shapes and the wavelength of the maximum intensity were compared. In the blue and black ballpoint pen inks, the discriminating powers (DP) were 0.85 and 0.61, respectively. The changes of the reflectance intensity at their wavelength of maximum intensity and their shapes appeared according to the exposure time to sunshine in a laboratory, especially in the blue ballpoint pen inks. Therefore it is possible to distinguish ink entries on the same paper with the relative age in case of questioned letters written with blue ballpoint pen.

The classification of ballpoint pen inks in Questioned Documents by using VSC and SERRS

  • Kim, Nam Yee;Park, Sung Woo;Doble, Philip;Roux, Claude
    • Analytical Science and Technology
    • /
    • v.17 no.4
    • /
    • pp.315-321
    • /
    • 2004
  • The aim of this study was to investigate the evidential value of blue and black ballpoint pens on paper by nondestructive techniques. In this work, 21 blue and 22 black ballpoint pens which were purchased on different brands were analyzed by Raman Spectroscopy and Video Spectral Comparator (VSC). Surface-Enhanced Resonance Raman Spectroscopy (SERRS) with excitation at 685 nm and VSC with several spot light filters were used for the discrimination of ballpoint pen inks. In the SERR spectra, the ballpoint pen inks on paper could be shown sharp spectral bands and distinguished by their band shapes and relative intensities. In the blue and black ballpoint pen inks, the discriminating powers (DP) by SERRS were 0.85 and 0.67 and the DP by VSC were 0.88 and 0.90, respectively. The DP by combined sequence of techniques was all 0.97 in both black and blue ballpoint pen inks.

Acute cocaine intoxication in a body packer

  • Park, Mee-Jung;Lim, Mi-Ae;Chung, Hee-Sun
    • Analytical Science and Technology
    • /
    • v.19 no.1
    • /
    • pp.103-106
    • /
    • 2006
  • A 35-year-old Perubian who suffered from grand mal seizures died in the aircraft on his way from the United States to Hongkong via Incheon international airport of Korea. While performing the autopsy, 115 packs made with double layer of transparent film and black plastic bag containing cocaine were found in the ileum and large intestine. Among of them, 3 packs were ruptured. To determine the concentration of cocaine and its metabolites, blood, urine, bile, liver, spleen, heart, kidney, brain and gastric contents were taken and toxicological analysis was performed. Gas chromatography/mass spectrometry (GC/MS) following liquid-phase extraction using chloroform:isopropanol (=9:1) and derivatization with bis(trimethylsilyl)-trifluoroacetamide (contains 1% trimethylchlorosilane) was performed. High levels of cocaine, benzoylecgonine (BE) and ecgonine methylester (EME) were found in the postmortem blood (0.96, 3.09 and $5.59{\mu}g/mL$) and urine (32.85, 145.35 and $53.17{\mu}g/mL$), respectively. Cocaine and its metabolites were also detected in all other biological specimen.