• 대한기계학회논문집A
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• 제23권6호
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• pp.1026-1038
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• 1999

Interlaminar fracture toughness of carbon/epoxy composite materials has been studied under tensile and flexural loading by the use of width tapered double cantilever beam(WTDCB) and end notched flexure(ENF) specimens. This study has significantly examined the effect of various interfacial ply orientation, ${\alpha}(0^{\circ},\;45^{\circ}\;and\;90^{\circ})$ and crack propagation direction, ${\theta}(0^{\circ},\;15^{\circ},\;30^{\circ}\;and\;45^{\circ})$ in terms of critical strain energy release rate through experiments. Twelve differently layered laminates were investigated. The data reduction for evaluating the fracture energy is based on compliance method and beam theory. Beam theory is used to analyze the effect of crack propagation direction. The geometry and lay-up sequence of specimens are considered various conditions such as skewness parameter, beam volume, and so on. The results show that the fiber bridging occurred due to the non-midplane crack propagation and causes the difference of fracture energy evaluated by both methods. For safer and more reliable composite structures, we obtain the optimal stacking sequence from initial fracture energy in each mode.

• Computers and Concrete
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• 제22권5호
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• pp.481-492
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• 2018

In this paper, a new hybrid fiber system (NHFS) is investigated for the application of slab. The steel fiber, polyvinyl alcohol (PVA) fiber and calcium carbonate ($CaCO_3$) whisker is added to form NHFS. The four-point bending test is carried out on the flexural properties of slab with plain, steel fiber, traditional hybrid fiber system (THFS) and NHFS reinforced cementitious composites. The flexural behavior is evaluated by ASTM C1018-97, JCI-SF4 and post-crack strength (PCS) technique. The evaluation parameters of flexural toughness such as toughness index (TI), equivalent flexural strength (EFS) and PCS are determined. The size of slab specimens is $15mm(thickness){\times}50mm(width){\times}200mm(length)$. The results show that adding $CaCO_3$ whisker to THFS can significantly improve the flexural strength, TI, EFS, PCS of the slab. The empirical relation between reinforcing index ($RI_v$) and flexural parameters show that flexural parameters of slabs increase first and then decrease; which indicates that optimum $RI_v$ values can be helpful in the considering the mix design of steel-PVA fibers-$CaCO_3$ whisker composites for achieving the desired flexural-related properties. The scanning electron microscopy is performed to observe the micro-morphological characteristics of the fracture surface, which proved the positive hybrid effect among the different fibers in cementitious composites. The NHFS can arrest the generation and propagation of the crack from micro to macro level.

• 콘크리트학회지
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• 제6권6호
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• pp.151-158
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• 1994

본 연구에서는 수경성 시멘트 경화체의 구조적 결함인 휨강도를 향상시키시 위해 보통 포틀랜드 시멘트비를 0.1로 하여 혼합수량을 줄이고 수용성 고분자 물질인 Hydroxy Propy Methyl Cellulose(HPMC)를 첨가하여 시멘트입자의 윤활작용에 따른 균일한 분산효과와 결합효과를 얻도록 하였으며, twin roll mill로 혼련 성형하여 치밀하고 균일한 경화제 시편을 제조하였다. 이러한 고강도 시멘트 경화체의 휨강도는 약 96MPa, 탄성계수는 60GPa로 우수한 특성을 나타내었다. 고강도 시멘트의 고강도화 기구는 100${\mu}m$ 이상의 큰 기공제거 및 균열성장경로인 모세관 기공의 감소, 미수화 시멘트의 증가로 인한 탄성계수의 증가와 crack toughening(입자 가교, 고분자 섬유 가교, frictional interlocking)에 의한 파괴 인성의 향상 때문인 것으로 판단된다.

• Restorative Dentistry and Endodontics
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• 제40권4호
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• pp.262-269
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• 2015

Objectives: The aim of this study was to evaluate the mechanical and physical properties of a newly developed fiber reinforced dental composite. Materials and Methods: Fiber reinforced composite EverX Posterior (EXP, GC EUROPE), and other commercially available bulk fill composites, including Filtek Bulk Fill (FB, 3M ESPE), SonicFill (SF, Kerr Corp.), SureFil (SDR, Dentsply), Venus Bulk Fill (VB, HerausKultzer), Tetric evoceram bulk fill (TECB, Ivoclar Vivadent), and Xtra Base (XB, Voco) were characterized. Composite samples light-cured with a LED device were evaluated in terms of flexural strength, flexural modulus (ISO 4049, n = 6), fracture toughness (n = 6), and Vickers hardness (0, 2, and 4 mm in depth at 24 hr, n = 5). The EXP samples and the fracture surface were observed under a scanning electron microscopy. Data were statistically analyzed using one-way ANOVA and unpaired t-test. Results: EXP, FB, and VB had significantly higher fracture toughness value compared to all the other bulk composite types. SF, EXP, and XB were not statistically different, and had significantly higher flexural strength values compared to other tested composite materials. EXP had the highest flexural modulus, VB had the lowest values. Vickers hardness values revealed SF, EXP, TECB, and XB were not statistically different, and had significantly higher values compared to other tested composite materials. SEM observations show well dispersed fibers working as a reinforcing phase. Conclusions: The addition of fibers to methacrylate-based matrix results in composites with either comparable or superior mechanical properties compared to the other bulk fill materials tested.

• 대한치과보철학회지
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• 제43권1호
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• pp.52-60
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• 2005

Purpose. The intent of this study was to evaluate the effects of curing conditions on self-curing denture base resins to find out proper condition in self-curing resin polymerization. Materials and methods, In this study, 3 commercial self-curing denture base resins are used Vertex SC, Tokuso Rebase and Jet Denture Repair Acrylic. After mixing the self curing resin, it was placed in a stainless steel mold(3$\times$6$\times$60mm). The mold containing the resin was placed under the following conditions: in air at 23$^{\circ}C$; or in water at 23$^{\circ}C$; or in water at 23$^{\circ}C$ under pressure(20psi); or in water at 37$^{\circ}C$ under pressure(20psi) or in water at 50$^{\circ}C$ under pressure(20psi) , or in water at 65$^{\circ}C$ under pressure(20psi), respectively. Also heat-curing denture base resin is polymerized according to manufactures' instructions as control. Fracture toughness was measured by a single edge notched beam(SENB) method. Notch about 3mm deep was carved at the center of the long axis of the specimen using a dental diamond disk driven by a dental micro engine. The flexural test was carried out at a crosshead speed 0.5mm/min and fracture surface were observed under measuring microscope. Results and conclusion . The results obtained were summarized as follows : 1. The fracture toughness value of self-curing denture base resins were relatively lower than that of heat-curing denture base resin. 2. In Vertex SC and Jet Denture Repair Acrylic, higher fracture toughness value was observed in the curing environment with pressure but in Tokuso Rebase, low fracture toughness value was observed but there was no statistical difference. 3. Higher fracture toughness value was observed in the curing environment with water than air but there was no statistical difference. 4. Raising the temperature in water showed the increase of fracture toughness.

• 구강회복응용과학지
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• 제17권3호
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• pp.199-204
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• 2001

This study was to investigate the reused possibility of zirconia reinforced glass-ceramic(IPS Empress Cosmo ceramic) with sprue button in the flexure strength and fracture toughness. 40 disk-shaped ceramic specimens (20 specimens: as-pressed material; 20 specimens: reused material) with approximately 1.7 mm thickness and 15 mm diameter were prepared by "lost wax" technique. The remnants(sprue buttons) were used for repressing. The surface treatments for the discs were gradually abraded with 320, 800, 1200, and 2000 grit SiC sandpaper. The specimens were evaluated their flexure strength with the biaxial flexure jig(ball-on-three balls) and their fracture toughness with Vickers Indentation-microfracture test. The Weibull moduli were calculated for biaxial flexural strength. The mean flexure strength and fracture toughness of each group were $122.2{\pm}18.3MPa$, $1.00{\pm}0.09MPa{\cdot}m^{0.5}$ (as-pressed ceramics), and $122.2{\pm}20.3MPa$, $1.01{\pm}0.10MPa{\cdot}m^{0.5}$ (reused ceramics). There were no significant differences in the strength and the fracture toughness between the as-pressed and the reused IPS Empress Cosmo ceramic (P>0.05). This implied zirconia reinforced glass-ceramic(IPS Empress Cosmo ceramic) could be used one more time by reusing of sprue button in the flexure strength and fracture toughness.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2004년도 추계학술발표대회 논문집
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• pp.189-192
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• 2004

In this study, mode II interlaminar fracture phenomena of carbon fabric/epoxy composite for tilting train were investigated. The end notched flexural specimen containing an artificial crack with the thickness of 12.5fl11l was used. The mode II interlaminar fracture toughness was evaluated through a three point bending test and the fractured surfaces were examined through a scanning electron microscope. The experimental results obtained in this study would be applicable in the design and structural analysis of the composite structures.

• Computers and Concrete
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• 제24권4호
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• pp.283-293
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• 2019

The limited availability of raw materials and increasing service demands for pavements pose a unique challenge in terms of pavement design and concrete material selection. The self-compacting rubberized concrete (SCRC) can be used in pavement design. The SCRC pavement slab has advantages of excellent toughness, anti-fatigue and convenient construction. On the premise of satisfying the strength, the SCRC can increase the ductility of pavement slab. The aim of this investigation is proposing a new method to predict the crack growth and flexural capacity of large-scale SCRC slabs. The mechanical properties of SCRC are obtained from experiments on small-scale SCRC specimens. With the increasing of the specimen depth, the bearing capacity of SCRC beams decreases at the same initial crack-depth ratio. By constructing extended finite element method (XFEM) models, crack growth and flexural capacity of large-scale SCRC slabs with different fracture types and force conditions can be predicted. Considering the diversity of fracture types and force conditions of the concrete pavement slab, the corresponding test was used to verify the reliability of the prediction model. The crack growth and flexural capacity of SCRC slabs can be obtained from XFEM models. It is convenient to conduct the experiment and can save cost.

• Journal of Ceramic Processing Research
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• 제19권5호
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• pp.419-423
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• 2018

A newly conceived geopolymer composite was fabricated by a combination of the geopolymer and polyurethane sponge. The density and porosity of hardened geopolymer composite, corresponded to different pore sizes of polyurethane sponge, exhibited no significant differences from each other. However, the mechanical behavior, the compressive strength and flexural strength, showed slight differences accordingly. Fracture of the geopolymer composite exposed to high compressive load was not observed from all specimens containing polyurethane sponge. The toughness enhancement of the geopolymer composite, due to spontaneous elasticity of polyurethane sponge, crack spread, and crack diffraction, was identified through the stress-strain curve and microstructure of fracture surface. The newly designed geopolymer composite having a 3-dimensional sponge skeleton showed relatively higher flexural strength of 8.0 MPa than other conventional geopolymer composites.

• Computers and Concrete
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• 제17권4호
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• pp.553-566
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• 2016

Fracture energy is one of the key parameters reveal cracking resistance and fracture toughness of concrete. The main purpose of this study is to determine fracture behavior, mechanical properties and microstructural analysis of high strength basalt fiber reinforced concrete (HSFRC). For this purpose, three-point bending tests were performed on notched beams produced using HSFRCs with 12 mm and 24mm fiber length and 1, 2 and $3kg/m^3$ fiber content in order to determine the value of fracture energy. Fracture energies of the notched beam specimens were calculated by analyzing load versus crack mouth opining displacement curves by the help of RILEM proposal. The results show that the effects of basalt fiber content and fiber length on fracture energy are very significant. The splitting tensile and flexural strength of HSFRC increased with increasing fiber content whereas a slight drop in flexural strength was observed for the mixture with 24mm fiber length and $3kg/m^3$ fiber content. On the other hand, there was no significant effect of fiber addition on the compressive strength and modulus of elasticity of the mixtures. In addition, microstructural analysis of the three components; cement paste, aggregate and basalt fiber were performed based on the Scanning Electron Microscopy and Energy-Dispersive X-ray Spectroscopy examinations.