• 한국재료학회지
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• 제21권5호
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• pp.263-267
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• 2011

The present study was carried out to evaluate the microstructural and mechanical properties of cross-roll rolled pure copper sheets, and the results were compared with those obtained for conventionally rolled sheets. For this work, pure copper (99.99 mass%) sheets with thickness of 5 mm were prepared as the starting material. The sheets were cold rolled to 90% thickness reduction and subsequently annealed at $400^{\circ}C$ for 30 min. Also, to analyze the grain boundary character distributions (GBCDs) on the materials, the electron back-scattered diffraction (EBSD) technique was introduced. The resulting cold-rolled and annealed sheets had considerably finer grains than the initial sheets with an average size of 100 ${\mu}M$. In particular, the average grain size became smaller by cross-roll rolling (6.5 ${\mu}M$) than by conventional rolling (9.8 ${\mu}M$). These grain refinements directly led to enhanced mechanical properties such as Vickers micro-hardness and tensile strength, and thus the values showed greater increases upon cross-roll rolling process than after conventional rolling. Furthermore, the texture development of <112>//ND in the cross-roll rolling processed material provided greater enhancement of mechanical properties relative to the case of the conventional rolling processed material. In the present study, we systematically discuss the enhancement of mechanical properties in terms of grain refinement and texture distribution developed by the different rolling processes.

• 한국재료학회지
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• 제23권1호
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• pp.41-46
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• 2013

The microstructural evolution of AA1050/AA6061 complex aluminum alloy, which is fabricated using an accumulative roll-bonding (ARB) process, with the proceeding of ARB, was investigated by electron back scatter diffraction (EBSD) analysis. The specimen after one cycle exhibited a deformed structure in which the grains were elongated to the rolling direction for all regions in the thickness direction. With the proceeding of the ARB, the grain became finer; the average grain size of the as received material was $45{\mu}m$; however, it became $6.3{\mu}m$ after one cycle, $1.5{\mu}m$ after three cycles, and $0.95{\mu}m$ after five cycles. The deviation of the grain size distribution of the ARB processed specimens decreased with increasing number of ARB cycles. The volume fraction of the high angle grain boundary also increased with the number of ARB cycles; it was 43.7% after one cycle, 62.7% after three cycles, and 65.6% after five cycles. On the other hand, the texture development was different depending on the regions and the materials. A shear texture component {001}<110> mainly developed in the surface region, while the rolling texture components {011}<211> and {112}<111> developed in the other regions. The difference of the texture between AA1050 and AA6061 was most obvious in the surface region; {001}<110> component mainly developed in AA1050 and {111}<110> component in AA6061.

• 한국주조공학회지
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• 제15권6호
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• pp.574-587
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• 1995

The $SiC_p-reinforced$ preforms fabricated by spray casting process were hot-extruded and subsequently T6-treated, and the morphology of the silicon phase and the grain size for these preforms and extruded samples were examined by Image Analyzer. Experimental observation revealed that with increase in volume percent of SiC particles, the grain size and silicon phase of the $Al-Si/SiC_p$ composites become finer, the shape of Si phase is changed from blocky to granular type, and aspect ratio of Si phase tend to become unity. Wear-tests with various sliding velocities, show that the wear resistance of spray cast specimen is increased remarkably compare to the permanent mold cast specimen at the sliding velocity range of $1.98{\sim}2.38m/sec$.. Microstructural observations for the worn surfaces of specimens revealed that wear resistance of Al-Si alloys at certain sliding velocities could be improved not only by the fine grain size of aluminum matrix but also the fine size and granular shape of silicon phases. The wear resistance of $SiC_p$ reinforced aluminum composites was found to be sensitive to the volume percentage of the reinforcing particles. The worn surfaces with various sliding velocities, show that change in wear mechanism seems to occur at the sliding velocity of near 2m/sec for all samples, and such a change in mechanism is delayed with increase in $SiC_p$ volume fraction.

• 한국해안해양공학회지
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• 제15권1호
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• pp.33-38
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• 2003

가덕도 인근 연안해역에서 채취된 해저 퇴적물과 연직방향으로 배열된 표사포획장치로부터 획득된 부유물질을 이용하여 탁도계 검교정을 수행하였다. 포획된 부유물질은 모래 함량이 약 6%인 해저 퇴적물에 비하여 주로 실트 및 점토로 조성되었으며, 해저면으로부터의 놀이가 증가함에 따라 세립화하는 경향을 보였다. 해저 퇴적물에 대한 탁도계 검교정 선형 회귀식의 기울기는 최소값으로 나타났으며, 수심별로 포획된 부유물질에 의한 선형 회귀식의 기울기는 포획 고도가 증가함(즉, 입도가 감소함)에 따라서 점진적으로 증가하였다. 이러한 결과는 해저 퇴적물에 대한 탁도계 검교정 결과로부터 부유물질 농도를 환산할 경우 과대추정의 오차가 발생되며, 본 연구해역의 경우에는 그 오차가 최대 25％까지 증가할 수 있다는 것을 보여준다. 따라서 해저 퇴적물보다는 수층에서 포획된 부유물질의 입도분포를 고려하여 보정된 검교정식을 적용하는 것이 부유물질 농도의 측정오차를 최소화하는 방법으로 사료된다.

• 한국세라믹학회지
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• 제42권3호
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• pp.171-177
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• 2005

서로 다른 입자크기를 갖는 WC와 Co 분말 원료를 사용하여 $WC-10\;wt\%$Co 초경합금을 제조하였다. 이로부터 WC와 Co 원로. 입자크기가 제조된 초경합금의 성질에 미치는 영향에 대해 고찰하였다. WC 원료 입자크기가 클수록 제조된 초경합금이 파괴인성이 높고 경도는 낮게 나타나는데, 이러한 경향은 Co 원료 입자크기에 크게 영향 받지 않음을 알 수 있었다. Co 원료 크기의 영향 외에도 Co 원료 크기가 초경합금의 특성에 영향을 주는 것으로 밝혀졌는데, 동일한 WC 원료를 사용하여도 미세한 Co 원료를 사용할 경우, 보다 조대한 WC를 함유하여 인성이 우수한 초경합금을 제조할 수 있었다. 이로부터 Co 원료 입자크기가 초경합금의 미세구조 및 그 특성에 중요한 역할을 함을 알 수 있었다

• 대한치과기공학회지
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• 제15권1호
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• pp.5-25
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• 1993

Effects of hydrogenation on microstructure and mechanical properties of pure Ti and Ti-0.15Pd alloy have been studied by means of optical microscopy, differential scanning calorimeter(DSC), Xray diffraction and micro vicker's hardness test. Grain size of pure Ti and Ti-0.15Pd alloy decresed largely by hydrogenation finer than that of pure Ti and the grain size refinement was evedent in Ti-0.15Pd alloy than that in pure Ti. Ti-.015Pd alloy carried out solution treatment at 950$^{\circ}C$, the transformation of $\alpha$' martensite was occured. The amount of Hydrogen absorption in Ti-.015Pd alloy was higher than that in pure Ti. Decomposition of hydride in pure titanium and Ti-0.15Pd alloy increased largely by hydrogenation, and micro vicker's hardness of Ti-.015Pd alloy was largely than that of pure Ti by 30% after hydrogenation. The micro vicker's hardness of Ti-0.15Pd alloy after solution treatment and dehydrogenation were higher at $\beta$ phase ranger(950$^{\circ}C$) than that phase range(750$^{\circ}C$).

• 한국물환경학회지
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• 제25권6호
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• pp.935-942
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• 2009

During period of the rainy season of spring tide Aug. 2005, the suspended sediment transport rate from Seomjin River increased ten times as high as neap tide of low river discharge. During ebb tide of high terrestrial input, the grain size of suspended particles of both surface and bottom layer of the water column, showed a uni-modal distribution with a dominant peak at coarse fraction, which suggests a characteristic development of floc-sized particles of low mean effective density. On the contrary, the particles supplied toward upstream of Seomjin river from Gwangyang Bay during flood tide showed a bi-modal distribution with a secondary peak at finer fraction, possibly due to the resuspension and the deflocculation associated with the increased shear velocity at near bottom. Break-up of large flocs is also suggested by the increased mean effective density. However, settling velocity was lower during flood tide because of smaller grain size. Thus, net deposition of suspended sediment is expected at within Gwangyang Bay instead of upstream of Seomjin River, even though suspended sediment transport rate at near bottom water was three times higher than that at surface water during flood tide.

• 열처리공학회지
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• 제7권1호
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• pp.3-10
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• 1994

The structure and mechanical properties of the extruded specimens were investigated in rapid solidified Al-(1, 3, 5) Cr alloys after mechanical alloying. Finer lamellar microstructure could no longer be resolved in the bars obtained by extrusion of the spherical particles after 200 min. of processing time. The structure of extruded bars are highly depended on the processing time of splats. The isothermal annealing of the extruded bars showed that all the alloys had good thermal stability up to $400^{\circ}C$ and did not show the recrystallization phenomena. Severe working of Al-(1, 3, 5) Cr splats produced a very fine grain size and substructural strengthening (high dislocation density and fine grain size). Effects of mechanical alloying on the thermal stability of the extruded bars Al-(1, 3, 5) Cr alloys decreases, with increasing Cr content. But the ultimate tensile Strength in the extruded bars increases with increasing Cr content.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2004년도 추계학술대회논문집
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• pp.111-114
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• 2004

It is many devices to obtain the globular structure because the globularity of the structure is the key to the low apparent viscosity and also to good rheological properties. In this study, the morphology of the change of primary Al phase in A356 alloy by electro magnetic stirrer was investigated to obtain the globular structure. The parameters are the current, stirring time, pouring temperature individually. The greater current and longer stirring time was to get the finer the primary however in case of over the 80A of current and 60sec of stirring time, the primary Al was merged together and was increased. The effect of pouring temperature has an important effect on the size of primary phase. About the $675^{\circ}C$, the primary Al was very fined.

• Ocean and Polar Research
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• 제25권2호
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• pp.133-145
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• 2003

Deep-sea surface sediments were collected using a multiple corer at 20 stations of Clarion-Clipperton fracture zone in the northeast equatorial Pacific to understand latitudinal and longitudinal variations of geotechnical properties. There was a distinct latitudinal variation of geotechnical properties in the study area. The northern sediments showed finer grain size, lower water content and porosity, higher bulk density and specific grain density, lower liquid limits and plastic limits than their southern counterparts. The northern sediments are classified into inorganic clays of low plasticity (fat clays) on plasticity charts and normal to active clay on activity chart, whereas, the southern sediments are classified into fine-grained, highly-plastic, inorganic and biogenic silt or organic clays on plasticity chart and normal to very active clay on activity chart. When shear strength are considered, the northern sediments were found to be in unconsolidated states, while the southern ones to be normal to over-consolidated states. These latitudinal variations in sediment characteristics are likely caused by differences in productivity of surface water that controls sediment compositions, sedimentation rates, and grain solubility.