• 소성∙가공
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• 제7권2호
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• pp.150-157
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• 1998

Recently the SPPC technology is being developed in steel rolling industries for the purpose of enhancing mechanical properties of rolled sheets. The technology is to produce steel sheets with finer and more uniformly distributed grains by prediction of recrystallization behaviors and on-line control of rolling parameters during hot rolling process. In this study a finish rolling process was analyzed by a three-dimensional rigid-thermoviscoplastic finite element method and recrystallization behaviors of several locations in the sheet were predicted by Sellars equations. As a result it was found that the initial grain size of 84 ${\mu}m$ became $21-23\;{\mu}m\;20-22{\mu}m\;and\;18-20{\mu}m$ at front middle and end portions of the sheet respectively. It was also found that variations of the grain size became $$0.6{\sim}2{\mu}m\;and\;10{\mu}\mum$$ in thickness and width directions respectively.

• 한국해양학회지
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• 제28권1호
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• pp.72-78
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• 1993

MasterSizer와 SediGraph를 이용하여 표준입자와 여러 종유의 퇴적물을 분석하고 그 결과를 비교하였다. SediGraph에 의해 분석된 퇴적물 시료의 입도분석 결과는 MasterSizer에 의한 결과보다 세립하게 나타나는 데, 특히 심해저의 규질연니 퇴적물 에서 그 차이가 크다. 이러한 차이는 시료의 전처리 과정, 기기에 도입되는 시료 농 도, 세립한 입자(약 1um 이하) 감지 능력, 그리고 비구형 입자가 두 기기에 인지되는 방식 등 두 방법상의 여러 가지 다른 점에 기인할 가능성이 있다.

• 한국표면공학회지
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• 제25권5호
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• pp.223-233
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• 1992

(Ti, Al)N films were deposited on 304 stainless steel by D.C. magnetron sputtering using Al target and Ti plate. The properties of (Ti, Al)N films such as composition, microhardness, grain size, crystal structure were investigated. The chemical composition of (Ti, Al)N films was similar to the sputter area ratio of titanium to aluminum target by means of EDS and AES survey. The higher bias voltage to substrate and the smaller input of N2 gas showedthe increased microhardness and the finer grain size of the films. The results obtained from this study show, it is belived, that the (Ti, Al)N film by D.C.magne-tron sputtering is promising in the wear resistance use.

• 소성∙가공
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• 제31권3호
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• pp.117-123
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• 2022

In this study, a commercial AZ61 magnesium alloy is extruded at 300 ℃ and 400 ℃ and the microstructures, mechanical properties, and high-cycle fatigue properties of the extruded materials are investigated. Both extruded materials have a fully recrystallized microstructure with no Mg₁₇Al₁₂ precipitates. The average grain size and maximum basal texture intensity of the extruded material increase with increasing extrusion temperature. The material extruded at 400 ℃ (AZ61-400) has higher tensile yield strength and lower compressive yield strength than the material extruded at 300 ℃ (AZ61-300) because of the stronger basal texture of the former. Because of coarser grain size, the tensile elongation of AZ61-400 is lower than that of AZ61-300. Despite the differences in microstructures and tensile/compressive properties, the two extruded materials have the same fatigue strength of 110 MPa. This is because the finer grain size of AZ61-300 causes an increase in fatigue strength, but its weaker texture causes a decrease in fatigue strength. In both extruded materials, fatigue cracks initiate at the surface of fatigue specimens at all stress amplitudes tested.

• Nuclear Engineering and Technology
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• 제32권1호
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• pp.77-87
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• 2000

It is reported that the toughness and safety margins of the SA106 Gr.C main steam line piping steel is reduced due to dynamic strain aging (DSA) at the reactor operating temperature for Leak-Before-Break (LBB) application. In this study, intercritical annealing in two-phase ($\alpha$+${\gamma}$）region was performed to investigate the possibility of improving the toughness and reducing DSA susceptibility. The manifestations of DSA were still observed in the tensile tests of the annealed specimens. However, the ductility loss caused by DSA was smaller than that in the as-received material. Furthermore, the intercritical annealing was able to increase the Charpy impact toughness by 1.5 times compared to as-received. With the heat treatment, we could obtain microstructural changes such as the cleaner retained ferrite, increased ferrite content and somewhat finer grain size. It is considered that the reduced DSA was induced by cleaner retained ferrite, which in turn resulted in higher impact toughness in addition to the general toughening due to finer grain sizes and increased ferrite content.

• The Korean Journal of Ceramics
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• 제3권3호
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• pp.199-207
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• 1997

$Al_2O_3$/SiC particulate composites were fabircated by pressureless sintering. The dispersed phase was SiC of which the content was varied from 1.0 to 10 vol%. Three SiC powders having different median diameters from 0.28 $\mu\textrm{m}$ to 1.9 $\mu\textrm{m}$ were used. The microstructure became finer and more uniform as the SiC content increased except the 10 vol% specimens, which were sintered at a higher temperature. Under the same sintering condition, densification as well as grain growth was retarded more severly when the SiC content was higher or the SiC particle size was smaller. The highest flexural strength obtained at 5.0 vol% SiC regardless of the SiC particle size seemed to be owing to the finer and more uniform microstructures of the specimens. Annealing of the specimens at $1300^{\circ}C$ improved the strength in general and this annealing effect was good for the specimens containing as low as 1.0 vol% of SiC. Fracture toughness did not change appreciably with the SiC content but, for the composites containing 10 vol% SiC, a significantly higher toughness was obtained with the specimen containing 1.9$\mu\textrm{m}$ SiC particles.

• 한국재료학회지
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• 제17권10호
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• pp.560-566
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• 2007

AlN plates were fabricated by hot pressing at $1700-1900^{\circ}C$ using yttria and alumina (3 and $10\;{\mu}m$ particle size) powders as additives and characterized: density, thermal conductivity, transverse rupture strength, and grain size measurement by SEM and EDS. Density values of $3.31-3.34\;g/cm^3$ are largely attributed to hot pressing of powder mixtures in carbon mold under $N_2$ atmosphere which caused effective degree of oxygen removal from yttrium-aluminate phase expected to form at $1100^{\circ}C$. The grain size of hot pressed AlN was almost homogeneous, with size approximately from 3.2 to $4.0\;{\mu}m$ after hot pressing. $Al_2O_3$ powder of $3\;{\mu}m$ particle size resulted in better transverse rupture strength and finer grain size compared to $10\;{\mu}m$ $Al_2O_3$ powder. The thermal conductivity of AlN ranged between $83-92.7\;W/m{\cdot}K$ and decreased with $Al_2O_3$ addition. Fine grain size is preferred for better mechanical properties and thermal conductivity.

• 대한원격탐사학회지
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• 제19권2호
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• pp.117-133
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• 2003

이 연구에서는 곰소만 조간대에서 현장 시료채취와 동시에 얻어진 Landsat ETM+ 자료를 이용하여 조간대 환경요인들이 ETM+에 의해 관측된 반사도와 어떤 관계를 가지고 있는 지 밝히고, 광학위성영상을 이용한 조간대 표층퇴적물의 분류의 적용 가능한 기준입도를 제시하고자 하였다. 일반적인 퇴적학적 분류 기준이 되는 4 $\Phi$ 입도를 기준으로 했을 때 입도와 영상의 반사도 간의 상관관계는 매우 낮은 것으로 나타났으나, 2 $\Phi$ 이상의 입자를 기준으로 하였을 때는 상부조간대의 천주변에 작은 입자로 구성된 지역의 자료들을 제외하면 ETM+ 밴드 4번과 0.699의 높은 상관계수를 보인다. 즉, 입도 2 $\Phi$ 곰소만 조간대에서의 광학위성 자료에 의한 표층퇴적물 분류를 위한 기준입도로 사용하는 것이 타당하다. 입도와 함수율은 비교적 높은 음의 상관관계를 보이며 특히 입도 2 $\Phi$ 기준과는 -0.811로서 뚜렷하게 음의 상관관계를 보인다 위성자료의 Factor analysis 결과는 지형요소에 의해 크게 영향을 받는 독일의 조간대와는 다른 특성을 보이며, 이는 곰소만의 경우는 입자가 세립하여 지형보다는 함수율에 더 큰 영향을 받는 것으로 나타났다. 결국 조간대 원격탐사에서는 입도뿐만 아니라 함수율과 지형 등의 환경요소가 함께 고려하여야만 한다.

• 한국분말재료학회지
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• 제3권3호
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• pp.181-187
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• 1996

Cobalt and VC powders were ball milled with M2 grade high speed steel powders under various ball to powder ratios. The powders milled under higher ball to powder ratio become finer, more irregular and have a broader size distribution, and thus possess a lower compressibility and a better sinterability regarding densification. Increasing the ball to powder ratio lowered the sintering temperature to obtain the density level necessary to isolate all the pores. Lowering the sintering temperature is very critical to maintain fine microstructure since grain and carbide coarsening are accelerated by higher sintering temperature due to more liquid phase formation. The powders obtained by ball milling at 20 to 1 ratio has the lowest compressibility but has the best sinterability, almost compatible to unmilled pure M2 powders. A sintered body over 97% theoretical density with fine microstructures having average grain size of ~10 microns was obtained from the powder by sintering at 1260 $^{\circ}C$ for 1 hour in vacuum. XRD results indicate that two types of carbides are mainly present in the sintered structure, MC and $M_{6}C$ type. The MC type carbides are more or less round shaped and mainly located at the grain boundaries whereas the $M_{6}C$ type are angular shaped and mainly located inside the grains.

• 한국해양학회지:바다
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• 제3권3호
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• pp.103-111
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• 1998

본 연구는 경기만 표층 퇴적물의 지화학적 특징과 입도분포와의 관계를 조사하기 위해서 수행되었다. 1995년 12월에 채집한 총 90 개 퇴적물 시료를 대상으로 입도분포, 유기탄소와 중금속 함량(Al, Fe, Mn, V, Co, Ni, Cr, Zn, Cu)을 분석하였다. 또한 1981년에 조사된 자료와 비교함으로써 그 동안의 변화를 파악하고자 하였다. 퇴적물 입자의 크기는 몇몇 지역에서 1981년과는 다른 양상을 보였다. 1994년에 완공된 시화방조제 부근의 퇴적물은 이전에 비해서 세립해졌다. 공항건설을 위한 매립공사가 진행되고 있는 영종도 부근의 퇴적물의 경우 세립한 퇴적상에서 혼합 퇴적상으로 변하였다. 유기물과 중금속 함량은 전반적으로 입도에 의존적인 분포를 보이고 있지만, 인천북항의 퇴적물에서는 입도와 무관하게 유기물과 Ni, Cr, Zn 그리고 Cu 등의 중금속이 높은 농도로 농축되어 있었다.