• Title/Summary/Keyword: fiber spinning

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Studies on Melt Spinning of PET Hollow Fibers

  • O Tae-Hwan;Lee Mu-Seok;Kim Sang-Yong;Sim Hyeon-Ju
    • Proceedings of the Korean Fiber Society Conference
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    • 1998.04a
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    • pp.111-115
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    • 1998
  • Fiber spinning is a continuous deformation process by which material is converted into a fiber. The melt spinning process was analyzed mainly by employing an asymptotic method of the so-called thin filament equations which formulates dynamics of spinning process by averaging over the cross-section of filament the set of fundamental equations. The method gives the approximate results for commonly used circular fiber spinning.(omitted)

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A Study of Fine Fiber Formation and Physical Properties of Polyacrylonitrile Copolymer (폴리아크릴로니트릴 공중합체의 극세 섬유제조 및 그 물성)

  • Lee, Shin-Hee
    • Fashion & Textile Research Journal
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    • v.14 no.3
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    • pp.472-477
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    • 2012
  • The conditions of wet spinning were considered in order to prepare the fine denier of acrylic fiber. Polyacrylonitrile copolymer was synthesized by the copolymerization of acrylonitrile (AN) and methyl acrylate (MA) initiated by an aqueous sulfite-chlorate redox system. Acrylic fiber was manufactured through wet-spinning in a dimethyl formamide (DMF) system. The conditions of wet-spinning were investigated by i-value, spinning speed, diameter of spinneret, draw ratio, water content of spinning dope and morphology of protofiber. The physical properties of fibers were investigated by Instron. In this experiment, the minimum i-value decreased with the decreasing spinneret diameter, an increased spinning speed, and an increased coagulation bath (CBC) concentration. The maximum draw ratio increased with an increased CBC. The optimum CBC and water content of the spinning dope were 60%-65% and 3.5%, respectively. The tenacity at the breaking point increased with a decreased fineness of fiber. The elongation at breaking point was almost the same value as a function of the fineness of fiber.

Preparation and Physical Properties of Biodegradable High Performance PLA Fiber using Process Parameters (용융방사에 의한 생분해성 고강도 PLA 섬유 제조 공정 상 주요 공정 변수에 관한 연구)

  • Jeung, Woo Chang;Kim, Sam Soo;Lee, Sang Oh;Lee, Jaewoong
    • Textile Coloration and Finishing
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    • v.34 no.3
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    • pp.197-206
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    • 2022
  • The purpose of this study was to confirm the optimal spinning conditions for PLA (Polylactic acid) as a fiber forming polymer. According to the melt spinning test results of PLA, the optimal spinning temperature was 258℃. However, it needs to note that relatively high pack pressure was required for spinning at 258℃. At an elevated temperature, 262℃, mono filament was broken easily due to hydrolysis of PLA at a higher temperature. In case of fiber strength, it was confirmed that the draw ratios of 2.7 to 3.3 were optimal for maximum strength of melt spun PLA. Above the draw ratio, 3.3, the strength of the PLA fibers was lowered. It was presumed that cleavage of the PLA polymer chain over maximum elongation. The heat setting temperature of GR (Godet roller) showed that the maximum strength of the PLA fibers was revealed around 100℃. The degree of crystallinity and the strength of the PLA fibers were decreased above 100℃. The optimal take-up speed (Spinning speed) was around 4,000m/min. Thermal analysis of PLA showed 170℃ and 57℃ as Tm (melting temperature) and Tg (glass transition temperature), respectively.

Dry-jet Wet Spinning of Polyhydroxyamide Fibers

  • Park, Seung-Koo;Cho, Seo-Hyun;Farris, Richard-John
    • Fibers and Polymers
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    • v.1 no.2
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    • pp.92-96
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    • 2000
  • A high molecular weight polyhydroxyamide (PHA) solution in N, N-dimethyl acetamide (DMAc) was prepared from 3, 3'-dihydroxybenzidine and isophthalic chloride (IPC), which was used for spinning PHA fiber. Before spinning, the diffusion property of DMAc into various coagulants was examined. The fiber was well formed in coagulants such as water/ethanol with a composition of 5/5, ethanol, and ethanol/isopropanol with a composition of 7/3 and 5/5. However, the PHA fiber spun in the water/ethanol mixture contained voids. After the fiber spun in ethanol was annealed at over $350^{\circ}C$, the ultimate stress and initial modulus of the fiber increased from 75.5 MPa and 3.22 GPa to 369 MPa and 29.5 GPa, respectively. These properties of the PHA fiber spun by the dry spinning method were also enhanced, attaining 154 MPa and 5.56 Gpa, respectivel.

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Effect of High-Temperature Spinning and PVP Additive on the Properties of PVDF Hollow Fiber Membranes for Microfiltration

  • Cha, Bong-Jun;Yang, Jung-Mok
    • Macromolecular Research
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    • v.14 no.6
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    • pp.596-602
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    • 2006
  • The effect of high-temperature spinning and poly(vinyl pyrrolidone) (PVP) additive on poly(vinylidene fluoride) (PVDF) hollow fiber membranes was investigated using differential scanning calorimetry, X-ray diffraction measurement, and scanning electron microscopy, together with the corresponding microfiltration performances such as water flux, rejection rate, and elongational strength. Using high-temperature spinning, porous hollow fiber membranes with particulate morphology were prepared through PVDF crystallization. The particulate structure of the membranes was further modified by the addition of miscible PVP with PVDF. Due to these effects, the rejection rate and strength of the fibers were increased at the expense of reduced water flux and mean pore size, which indicates that high-temperature spinning and PVP addition are vary effective to control the morphology of PVDF hollow fiber membranes for microfiltration.

Study on Spinning Behavior and Structure of Polyester Fibers by the Melt-type Electrospinning Method (용융형 전기방사법에 의한 폴리에스테르섬유의 방사거동과 구조에 관한 연구)

  • Lee, Jin-Ah;Lim, Min-Soo;Joo, Chang-Whan
    • Proceedings of the Korean Fiber Society Conference
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    • 2002.04a
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    • pp.273-276
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    • 2002
  • The fiber formation of conventional melt spinning is extruded by forcing the polymer melt through a spinneret by pumping mechanism usually involving high pressure. This is followed by cooling, solidification and appropriate drawing of the fiber. The spinning process is broadly applicable to polyolefin, polyamide, polyester and indeed the whole range of fibers forming thermoplastic polymers. (omitted)

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Studies on the Melting Characterization of Basalt and its Continuous Fiber Spinning (현무암의 용융특성과 연속섬유 방사 연구)

  • Park, Hye-Jung;Park, Sun-Min;Lee, Jae-Won;Roh, Gwang-Chul;Kim, Jae-Keun
    • Composites Research
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    • v.23 no.3
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    • pp.43-49
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    • 2010
  • Basaltic fiber was prepared by continuous spinning process from Jeju Pyosun raw basalt materials. First, for confirming the melting characterization of basalt, basalt raw material put into Pt crucible and melted up to $1550^{\circ}C$ then quenched by dropping it into water. After quenching, the optimum fiber spinning conditions were investigated by measurement and analysis of XRD, TMA, high temperature viscosity, high temperature conductivity and high temperature microscope. The optimum spinning temperature and viscosity for preparation of continuous filament fiber were $1264^{\circ}C$ and $10^{2.8}$ poise at $1264^{\circ}C$, respectively. Properties of prepared spinning fiber were confirmed by tensile strength, FE-SEM, heat resisting test and others. The tensile strength of fiber prepared by spinning conditions of the bushing temperature $1240^{\circ}C$ and winder speed 4600rpm was 3660MPa.

Physical Properties of E-glass Fiber According to Fiberizing Temperature (섬유화 온도 변화에 따른 E-glass fiber의 물리적 특성)

  • Lee, Ji-Sun;Lee, MiJai;Lim, Tae-Young;Lee, Youngjin;Jeon, Dae-Woo;Hyun, Soong-Keun;Kim, Jin-Ho
    • Korean Journal of Materials Research
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    • v.27 no.1
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    • pp.43-47
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    • 2017
  • E (Electric) -glass fibers are the most widely used glass fibers, taking up 90 % of the long glass fiber market. However, very few papers have appeared on the physical characteristics of E-glass fibers and how they depend on the fiberizing temperature of fiber spinning. Glass fiber was fabricated via continuous spinning process using bulk E-glass. In order to fabricate the E-glass specimen, raw materials were put into a Pt crucible and melted at $1550^{\circ}C$ for 2hrs; mixture was then annealed at $621{\pm}10^{\circ}C$ for 2hrs. The transmittance and adaptable temperature for spinning of the bulk marble glass were characterized using a UV-visible spectrometer and a viscometer. Continuous spinning was carried out using direct melting spinning equipment as a function of the fiberizing temperature in the range of $1175{\sim}1250^{\circ}C$, while the winder speed was fixed at 500 rpm. Subsequently we investigated the physical properties of the E-glass fiber. The average diameter of the synthesized glass fiber was measured by optical microscope. The mechanical properties of the fiber were confirmed using a UTM (universal materials testing machine); the maximum tensile strength was measured and found to be $1843{\pm}449MPa$ at $1225^{\circ}C$.

Effects of Spinning Processes on HVI Fiber Characteristics and Spun Yarn Properties

  • Koo Hyun-Jin;Suh Moon W.
    • Fibers and Polymers
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    • v.6 no.1
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    • pp.42-48
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    • 2005
  • The effects of opening, carding, and repeated drawings on single fiber and bundle cotton characteristics were stud­ied by employing $Mantis^{\circledR}$, $AFIS^{\circledR}$ and HVI Testers. Some of the significant changes in single fiber properties were found to be due to process parameters as well as the changes in the fiber crimps, parallelness of fibers within HVI beards, and the actual changes in the tensile properties of the fibers. The study showed that the HVI test data taken just prior to spinning had the highest correlation with the yam tensile properties. Based on the study results, we point out the potential of HVI for future quality and process control in spinning by recommending a set of expanded HVI output that is more scientific and compre­hensive for the future control needs.

A Study on Physical Properties of $PAN-CuSO_4$ Electroconductive Fiber and Wool Blended Fabrics (아크릴-황산동 복합체로 제조한 도전성 섬유 및 혼방한 모직물의 물성에 관한 연구)

  • 정영진;이명환;최해욱;이기환
    • Textile Coloration and Finishing
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    • v.11 no.4
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    • pp.8-15
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    • 1999
  • Electroconductive fiber was obtained by acryl fiber treated with $CuSO_4$. The Properties and structure of fiber and fabric such as mechanical property, electrical conductivity, fine structure, electrification were investigated. The experimental results are as follows 1) The electrical conductivity of the conducting fiber was greatly increased but fine structure and physical properties were similar to acryl fiber 2) Fabric made by mix spinning with conducting fiber was shown great electrification effect. 3) In the mix spinning with conducting fiber, it was necessary to use different. finishing such as milled finish because stiffness of fabric made by mix spinning with conducting fiber was increased and elastic recovery was decreased. 4) The antimicrobial activity of electroconductive fiber blended wool was effective by Cu component for shake flask test.

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