• 제목/요약/키워드: fiber identification

검색결과 144건 처리시간 0.027초

독활(獨活)과 그 위품의 감별기준 연구 : 외·내부형태 및 이화학패턴을 중심으로 (A Study on Identification Keys of Araliae Continentalis Radix and its Adulterants : Focused on External·Internal Morphology and Pattern Analysis)

  • 윤지현;주영승
    • 대한본초학회지
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    • 제33권2호
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    • pp.29-43
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    • 2018
  • Objectives : Araliae Continentalis Radix(AC) is a medicinal herb belonging to the drug efficacy group treating musculoskeletal disorders(MSD) with anti-inflammatory, analgesic and antipyretic action. However, due to morphologic and onomastic similarity, adulterants(Angelicae Pubescentis Radix: AP, Gypsophilae Oldhamianae Radix: GO, Levistici Officinalis Radix: LO) have been included or replaced the standard. Methods : Multilateral methods were carried out on the identification of AC and its adulterants. Macroscopic and microscopic characteristics were observed by using stereoscope and microscope. For the comparison of chromatogram pattern, standard compounds were analyzed simultaneously using high performance liquid chromatography. Results : 1. The macroscopic identification of original plants was determined by the phyllotaxis type, the inflorescence type, the leaf margin and the color of flowers. The macroscopic identification of herbal materials was examined by oil spots, the cambium, heteromorphic vascular bundles, and the pholem. 2. For the microscopic identification, the fact whether its xylem ray is proliferated or not was first determined. Then medicinal herbs were secondly divided by cellular inclusions, fiber bundles, the distribution of secretary canals and the shape of cambium. 3. AC and its adulterants showed different chromatographic fingerprints. AC was containing continentalic acid and kaurenoic acid. AP was containing osthole and columbianadin. LO was containing osthole and falcarindiol. None of the compounds were found in GO. Conclusions : This recent identification keys of might be helpful to discriminate the pharmacopoeia standard and its adulterants for the right usage in clinics.

$\beta$-시클로덱스트린화 셀룰로오스 섬유의 제조 및 소취성 (Preparation of $\beta$-Cyclodextrinized Cellulosic Fiber and Deodouring Property)

  • 최창남;황태연;고봉국;김용;홍성학;김상률
    • 폴리머
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    • 제25권5호
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    • pp.635-641
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    • 2001
  • 포접 기능을 가져 악취의 분리제거에 사용될 수 있을 것으로 보이는 $\beta$-시클로덱스트린 및 $\beta$-시클로덱스트린에 벤조산을 포접시킨 물질($\beta$-시클로덱스트린/벤조산 포접체)에 시아누르산 염화물을 반응시켜 클로로트리아진 유도체를 제조하고, 이를 면섬유와 반응시켜 새로운 소취 기능성 섬유를 제조하였다. 포접체의 형성은 적외선 분광분석 및 가시-자외선 분광분석기를 사용하여 확인하였으며, 반응기의 도입은 EDX로 확인하였다. 소취성능은 제조한 소취기능성 섬유를 컬럼에 채우고, 암모니아 기체를 흘려 보냈을 때 빠져나온 암모니아를 물에 용해시킨 용액의 농도를 0.1N 염산으로 적정하여 평가하였다. 섬유에 부착된 $\beta$-시클로덱스트린 단위가 증가할수록 소취성이 증가하였으며, $\beta$-시클로덱스트린에 벤조산을 포접한 경우에 소취성이 보다 증가하였다. 이는 포접체에 존재하는 벤조산과 암모니아의 결합때문이라고 생각되었다.

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Lamb wave-based damage imaging method for damage detection of rectangular composite plates

  • Qiao, Pizhong;Fan, Wei
    • Structural Monitoring and Maintenance
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    • 제1권4호
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    • pp.411-425
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    • 2014
  • A relatively low frequency Lamb wave-based damage identification method called damage imaging method for rectangular composite plate is presented. A damage index (DI) is generated from the delay matrix of the Lamb wave response signals, and it is used to indicate the location and approximate area of the damage. The viability of this method is demonstrated by analyzing the numerical and experimental Lamb wave response signals from rectangular composite plates. The technique only requires the response signals from the plate after damage, and it is capable of performing near real time damage identification. This study sheds some light on the application of Lamb wave-based damage detection algorithm for plate-type structures by using the relatively low frequency (e.g., in the neighborhood of 100 kHz, more suitable for the best capability of the existing fiber optic sensor interrogator system with the sampling frequency of 500 kHz) Lamb wave response and a reference-free damage detection technique.

광간섭계의 위상변화 신호를 이용한 광케이블 식별방법에 관한 연구 (A Research about the method for the optical cable identification by using phase change signal of the optical interferometer)

  • 정현호;이용기;민경선;정호진
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2006년도 하계종합학술대회
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    • pp.105-106
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    • 2006
  • It is important to identify the exact target optical cable that a worker look for when he executes a cable construction work. Until now, An Optical cable identification work has been done by a manual pulling of an optical cable or by the method of using RF signals. But these methods not only consume much time and labor costs but also have a distance limit of the optical cable to identify. In this paper, we propose a method that uses the phase change signal of the optical interferometer to identify an optical cable. With the proposed method the field worker can have an efficient tool to prevent miscutting the optical cable and can also save operating costs.

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Phytochemical Identification from Boehmeria nivea Leaves and Analysis of (-)-Loliolide by HPLC

  • Cho, Sunghun;Lee, Dong Gu;Jung, Yong-Su;Kim, Ho Bang;Cho, Eun Ju;Lee, Sanghyun
    • Natural Product Sciences
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    • 제22권2호
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    • pp.134-139
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    • 2016
  • Phytochemicals were isolated from leaves of the fiber crop, ramie (Boehmeria nivea, Bn), using open column chromatography and medium pressure liquid chromatography. Their structures were identified as ${\beta}$-sitosterol, (-)-loliolide, rutin, and pyrimidinedione by MS, $^1H$-, and $^{13}C$-NMR spectroscopic analysis. Among them, (-)-loliolide was isolated for the first time from B. nivea. A content analysis of (-)-loliolide in B. nivea collected from different regions and harvest times was conducted by HPLC. The highest content of (-)-loliolide was found in Bn-23 harvested in September. These results will be helpful to use the plant which harvest in September as a high content phytochemical additive in food, health supplements, and medicinal products.

Experimental study on identification of stiffness change in a concrete frame experiencing damage and retrofit

  • Zhou, X.T.;Ko, J.M.;Ni, Y.Q.
    • Structural Engineering and Mechanics
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    • 제25권1호
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    • pp.39-52
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    • 2007
  • This paper describes an experimental study on structural health monitoring of a 1:3-scaled one-story concrete frame subjected to seismic damage and retrofit. The structure is tested on a shaking table by exerting successively enhanced earthquake excitations until severe damage, and then retrofitted using fiber-reinforced polymers (FRP). The modal properties of the tested structure at trifling, moderate, severe damage and strengthening stages are measured by subjecting it to a small-amplitude white-noise excitation after each earthquake attack. Making use of the measured global modal frequencies and a validated finite element model of the tested structure, a neural network method is developed to quantitatively identify the stiffness reduction due to damage and the stiffness enhancement due to strengthening. The identification results are compared with 'true' damage severities that are defined and determined based on visual inspection and local impact testing. It is shown that by the use of FRP retrofit, the stiffness of the severely damaged structure can be recovered to the level as in the trifling damage stage.

합성가죽에서의 잠재지문 현출 (A study on characteristics of latent fingerprint detection on vinyl leather)

  • 최용복;박성우
    • 분석과학
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    • 제24권1호
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    • pp.45-50
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    • 2011
  • 현장조사 시 증거물을 찾는 방법은 육안관찰과 과학수사장비를 활용하게 된다. 감정에 활용되고 있는 현장 증거물은 혈액, 정액, 타액, 모발, 지문, 섬유, 토양, 페인트 등 그 종류는 매우 다양하며 그 중 지문은 현장 감식을 통하여 직접 현출하여 신속하게 개인을 식별 할 수 있다. 본 연구에서는 일상에서 많이 접할 수 있으면서도 선택적 현출 방법이 필요한 가죽류 지갑, 혁대, 쇼파 등에 대하여 다양한 현출 방법을 이용 검토 한 결과 다양한 가죽의 현출방법으로 자석형광분말법 및 형광분말법을 이용한 잠재지문 현출방법이 효율적인 것으로 확인하였다.

열분해-GC에 의한 면/폴리에스터 혼방 직물의 분석 (Analysis of Cotton/Polyester Fabrics using Pyrolysis Gas Chromatograpy)

  • 조미숙;김명덕;박성우;윤기준;남재도;이종훈;이영관
    • 폴리머
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    • 제27권3호
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    • pp.271-274
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    • 2003
  • 열분해 기체 크로마토그래피 (Py-GC)를 이용하여 섬유의 동일성과 함량을 조사하였다. 면사, 폴리에스터, 면과 폴리에스터 혼방사를 Py-GC를 이용하여 그 성분과 함량을 조사하였다. 면과 폴리에스터 성분은 각각의 특성 피이크를 나타내었으며, 특성 피이크의 면적은 각 성분의 함량이 증가함에 따라 비례적으로 증가함을 알 수 있었다. 또한 폴리에스터의 경우에 열분해로부터 생성되는 화합물의 성분을 질량 분광법을 이용하여 테레프탈산, 벤조산, 비닐 벤조산임을 확인할 수 있었으며, 이를 바탕으로 미지의 시료에 포함되어 있는 면과 폴리에스터의 함량을 정량 분석할 수 있었다.

장기 정씨묘 출토복식에 대한 보존처리 (A Study on the Conservation of Buried Clothes were Excavated from Jang-gi Chung's Tomb)

  • 배상경
    • 복식
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    • 제47권
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    • pp.89-100
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    • 1999
  • This study was carried to a textile conservation process included washing effect fiber analysis such as fiber identification fabric density and thickness color fading and of extracted soils. the following results were obtained. 1. AS a result of investigating to fabric surfaces by S.E.M all of cleaning methods wet cleaning-solvent cleaning in charge system were effective to remove soils from fabrics. 2. The buried fabrics were made of silk few of them were cotton ramie and hemp. 3. According to fabric density and thickness used fabrics were almost medium weight fabrics. 4. Low values of L, a, b indicated that the colors of these fabrics were faded to yellow and brown. 5. The soil components were hydrocarbon-alkane group alkyl alcohol and ketone group.

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Extension of the Rotating Planar Waveguide Model to Formation of Interference Patterns in Optical Fibers

  • Pena-Garcia, Antonio;Perez-Ocon, Francisco;Jimenez, Jose Ramon
    • Journal of the Optical Society of Korea
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    • 제15권2호
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    • pp.128-131
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    • 2011
  • After the successful extension of the rotating planar waveguide model to Wave Optics, where a clear identification between the angular velocity of one hypothetical waveguide and the phase differences between two points on the path of one bounded mode was found, an application of the model to explain the interference theory is presented. We demonstrate that, for two bounded modes to create an interference pattern, a constrain to the relative parameters among both is imposed by the fiber optics. This result, not reported in the literature up to date, provides a new horizon to understand the interaction light-light when propagated within optical fibers.