• Title/Summary/Keyword: fiber crystal growth

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Segregation Mechanism in Si1-xGex Single Crystal Fiber Growth by Micro-pulling Down Method

  • Uda, Satoshi;Kon, Junichi;Shimamura, Kiyoshi;Fukuda, Tsuguo
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1996.06a
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    • pp.399-421
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    • 1996
  • (1) The solute distribution mechanism was analyzed for the Si0.95Ge0.05 single crystal fiber by u-PD method. (2) The steady-state solutions were obtained for the molten zone and the capillary zone. (3) The effect of the convection in the molten zone on partitioning was not significant for many cases. (4) Intermediate transient rise of Ge was shown by the sudden change of the growth velocity or molten zone height. (5) Periodic compositional modulation can be designed by using the intermediate transient.

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MICROSTRUCTURE AND HIGH TEMPERATURE MECHANICAL PROPERTIES OF SAPPHIRE/R-Al-O (R=Y,Gd,Er,Ho,Dy) EUTECTIC FIRES GROWN BY MICRO PULLING-DOWN METHOD

  • Hasegawa, K.;Yoshikawa, A.;Durbin, S.;Epelbaum, B.;Fjkuda, T.;Waku, Y.
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1999.06a
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    • pp.403-418
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    • 1999
  • Fiber growth of Al2O3/R-Al-O(R=Y, Gd, Dy, Ho, Er) eutectic by the micro-pulling down methods is described. The thermal stability and strength at elevated temperature of each material is evaluated in relation to the microstructure. PACS: 81.05 Mh, 81.10 Fq, 81.30-t.

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Microstructure and high temperature mechanical properties of sapphire/R-Al-O(R = Y, Gd, Er, Ho, Dy) eutectic fibers grown by micro-pulling-down method

  • Hasegawa, K.;Yoshikawa, A.;Durbin, S.D.;Epellbaum, B.M.;Fukuda, T.;Waku, Y.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.4
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    • pp.432-436
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    • 1999
  • Fiber growth of $Al_{2}O_{3}/R-Al-O$ (R = Y, Gd, Dy, Ho, Er) eutectic by the micro-pulling down method is described. The thermal stability and strength at elevated temperature of each materials is evaluated in relation to the microstructure.

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Crystal Growth of $Ca_3(Li,Nb,Ga)_5O_{12}$ Garnet Crystals

  • Yu, Young-Moon;Chani, Valery-I.;Shimamura, Kiyoshi;Fukuda, Tsuguo
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1996.06a
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    • pp.351-374
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    • 1996
  • Various types of garnet compounds were synthsized by iso-and aliovalent substitutions and sintering method. Among them, fiber shapes of garnet crystals were grown from the $Ca_3Li_xNb_{(1.5+x)}Ga_{(3.5-2x)}O_{12}$ melt where x = 0 ~ 0.5 by modified micro-pulling down method in air using Pt crucibles. The measured lattice constants as a function of solidification fraction of grown fiber crystals are about $12.54\;{\AA}$ irrespective of x. It was found that the $Ca_3Li_{0.275}Nb_{1.775}Ga_{2.95}O_{12}$ garnet melts congruently at about $1450\;^{\circ}C$ based on the purities of garnet phase and variations of lattice parameter. Transparent and bubble-free crystals of x = 0.25 and 0.275 were grown by Czochralski techniques in air using Pt crucibles. An absorption spectrum is also reported.

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Fabrication of mineral fiber via melt spinning method from blast furnace slag

  • Wang, Xiao-Song;Hur, Bo-Young
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.24 no.4
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    • pp.158-163
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    • 2014
  • Mineral fiber, or be called mineral wool when it assembles in large amounts, is a kind of wide applied man-made material with excellent thermal and acoustic insulation properties. In this work, mineral fiber was produced via melt spinning method by using iron blast furnace slag as raw material. Two critical experimental parameters for fabrication were investigated: melt pouring temperature and rotating speed of spinning wheels. The mineral fiber produced under the condition of melt pouring temperature $1500^{\circ}C$ and spinning speed 4000 rpm, showed the smoother surface and most quality, while the others had rough surfaces or with heavy shots. In general, mineral fibers with the size in the range of $12{\sim}49{\mu}m$ in diameter and 8~130 mm in length can be fabricated by this method, and the production rate is more than 34 wt.%, which could be up to 57 wt.% at maximum.

Fabrication and resistance heating properties of flexible SiC fiber rope as heating elements (유연한 탄화규소 섬유 로프 발열체의 제조와 저항 발열 특성)

  • Joo, Young Jun;Cho, Kwang Youn
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.30 no.6
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    • pp.258-263
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    • 2020
  • Silicon carbide (SiC) fibers mainly fabricated from polycarbosilane, a ceramic precursor, are applied as reinforcing materials for ceramic matrix composites (CMCs) because of their high temperature oxidation resistance, tensile strength, and light weight. In this study, continuous SiC fibers used to fabricate rope-type flexible heating elements capable of generating high-temperature heat (> 650℃). For high-efficiency heating elements, the resistance of SiC fiber rope was measured by 2-point probe method according to the cross-sectional area and length. In addition, the fabrication conditions of rope-type SiC fiber heating elements were optimized by controlling the oxygen impurities and the size of crystal grains present in the amorphous SiC fiber. As a result, the SiC fiber heating element having a resistance range of about 100~200 Ω exhibited an excellent power consumption efficiency of 1.5 times compared to that of the carbon fiber heating element.

Mechanical properties of carbon fiber sheet and carbon fiber strand sheet based on carbon fibers for the reinforcement of highway bridge RC slabs (도로교 RC 상판 보강을 위한 탄소섬유 기초 carbon fiber sheet와 carbon fiber strand sheet의 역학특성)

  • Won, Chan Ho;Abe, Tadashi;Ahn, Tae-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.25 no.6
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    • pp.290-293
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    • 2015
  • Recently, a lot of interest has been shown in structural maintenance managements of civil infrastructures. Many researchers have been conducted on various maintenance techniques and repair materials. Among other fiber materials the carbon fiber materials are especially focused on maintenance management of Highway Bridges. Extensive work has been done on Carbon Fiber Sheet (CFS). Nevertheless, Carbon Fiber Strand Sheet (CFSS) is a newly developed material, on which limited work has been done until now. Therefore, in this study bonding the CFSS to RC slab specimen and fatigue resistance evaluation has been conducted. The results demonstrated an increase of 25.3 times more reinforcement of RC slab compared to non-reinforced RC slab. Moreover, compared to CFS-bonded RC slab, The CFSS-bonded RC slab showed 1.2 times greater reinforcement.

Growth and upconversion properties of erbium doped $LiNbO_3$ single crystal fibers ($Er^{3+}$ 첨가 $LiNbO_3$ fiber 단결정의 성장 및 upconversion 특성)

  • Yang, Woo-Seok;Suh, Su-Jeong;Lee, Jong-Ho;Tsuguo Fukuda;Yoon, Dae-Ho
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1999.06a
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    • pp.321-335
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    • 1999
  • Erbium(Er) doped LiNbO3(Er:LiNbO3) single crystal gibers were grown free of cracks along the c-axis by micro-pulling down method. the Er3+ concentration was distributed homogeneously along the growth axis. The samples for optical characterization were cut from as-grown single crystal fibers and polished. When the 980 nm light was incident on the sample, upconversion phenomena were observed at the green range of wavelength 510~570 nm. In addition, the intensity of upconversion was remarkably increased by increasing the concentration of Er2O3 dopant in as-grown Er:LiNbO3 crystals.

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Strain behavior of carbon fibers during hot stretching (탄소섬유의 고온 연신 열처리에서의 변형 거동)

  • 김홍수
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.1
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    • pp.64-69
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    • 1999
  • Polyacrylonitrile(PAN)-based carbon fiber tows were heat-treated by the internal resistance heating method under the certain load. To consider the strain behavior of the fiber tows during heat-treatments, 1200~$2200^{\circ}C$, strain changes of those were measured. It was observed that the larger longitudinal strain was induced under the larger stretching stress. The changes in the strain are different from the temperature regions below and above $1700^{\circ}C$. Obtained apparent activation energies under the stretching stresses of 70 and 322 MPa from time-strain curves were 67.46 and 52.27kJ$mol^{-1}$, respectively. Therefore, it was known that the larger stretching stresses effectively reduce the apparent activation energy of the fiber structure development of the fiber tows.

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Preparation of $ZrO_2-CaO$ fiber by using a chemical solution process

  • Hwang, Kyu-Seog;Jeon, Young-Sun;Kim, Sang-Bok;Kim, Chi-Kyun;Oh, Jeong-Sun;An, Jun-Hyung;Kim, Byung-Hoon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.13 no.6
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    • pp.267-271
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    • 2003
  • In this work, chemical solution derived Ca-doped zirconia fiber has been prepared by using calcium- and zirconium-naphthenate. Fibrous $ZrO_2$-CaO was drawn from a sticky mixture. Dried gel fibers were finally annealed at $1000^{\circ}C$ for 1 h in argon. 91 mol%$ZrO_2$-9 mol%CaO fiber consisted of tetragonal, monoclinic and $CaZrO_3$ phases after annealing at $1000^{\circ}C$. On the other hand, samples annealed at $500^{\circ}C$ consisted of almost tetragonal single phase. Homogeneous fibers surface at $500^{\circ}C$ became rougher after $1000^{\circ}C$-annealing. The sample annealed at $1000^{\circ}C$ with relatively rough surface structure showed a high Calcium phocphate forming ability.