• 제목/요약/키워드: fiber crystal growth

검색결과 59건 처리시간 0.022초

Segregation Mechanism in Si1-xGex Single Crystal Fiber Growth by Micro-pulling Down Method

  • Uda, Satoshi;Kon, Junichi;Shimamura, Kiyoshi;Fukuda, Tsuguo
    • 한국결정성장학회:학술대회논문집
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    • 한국결정성장학회 1996년도 The 9th KACG Technical Annual Meeting and the 3rd Korea-Japan EMGS (Electronic Materials Growth Symposium)
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    • pp.399-421
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    • 1996
  • (1) The solute distribution mechanism was analyzed for the Si0.95Ge0.05 single crystal fiber by u-PD method. (2) The steady-state solutions were obtained for the molten zone and the capillary zone. (3) The effect of the convection in the molten zone on partitioning was not significant for many cases. (4) Intermediate transient rise of Ge was shown by the sudden change of the growth velocity or molten zone height. (5) Periodic compositional modulation can be designed by using the intermediate transient.

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MICROSTRUCTURE AND HIGH TEMPERATURE MECHANICAL PROPERTIES OF SAPPHIRE/R-Al-O (R=Y,Gd,Er,Ho,Dy) EUTECTIC FIRES GROWN BY MICRO PULLING-DOWN METHOD

  • Hasegawa, K.;Yoshikawa, A.;Durbin, S.;Epelbaum, B.;Fjkuda, T.;Waku, Y.
    • 한국결정성장학회:학술대회논문집
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    • 한국결정성장학회 1999년도 PROCEEDINGS OF 99 INTERNATIONAL CONFERENCE OF THE KACG AND 6TH KOREA·JAPAN EMG SYMPOSIUM (ELECTRONIC MATERIALS GROWTH SYMPOSIUM), HANYANG UNIVERSITY, SEOUL, 06월 09일 JUNE 1999
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    • pp.403-418
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    • 1999
  • Fiber growth of Al2O3/R-Al-O(R=Y, Gd, Dy, Ho, Er) eutectic by the micro-pulling down methods is described. The thermal stability and strength at elevated temperature of each material is evaluated in relation to the microstructure. PACS: 81.05 Mh, 81.10 Fq, 81.30-t.

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Microstructure and high temperature mechanical properties of sapphire/R-Al-O(R = Y, Gd, Er, Ho, Dy) eutectic fibers grown by micro-pulling-down method

  • Hasegawa, K.;Yoshikawa, A.;Durbin, S.D.;Epellbaum, B.M.;Fukuda, T.;Waku, Y.
    • 한국결정성장학회지
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    • 제9권4호
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    • pp.432-436
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    • 1999
  • Fiber growth of $Al_{2}O_{3}/R-Al-O$ (R = Y, Gd, Dy, Ho, Er) eutectic by the micro-pulling down method is described. The thermal stability and strength at elevated temperature of each materials is evaluated in relation to the microstructure.

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Crystal Growth of $Ca_3(Li,Nb,Ga)_5O_{12}$ Garnet Crystals

  • Yu, Young-Moon;Chani, Valery-I.;Shimamura, Kiyoshi;Fukuda, Tsuguo
    • 한국결정성장학회:학술대회논문집
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    • 한국결정성장학회 1996년도 The 9th KACG Technical Annual Meeting and the 3rd Korea-Japan EMGS (Electronic Materials Growth Symposium)
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    • pp.351-374
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    • 1996
  • Various types of garnet compounds were synthsized by iso-and aliovalent substitutions and sintering method. Among them, fiber shapes of garnet crystals were grown from the $Ca_3Li_xNb_{(1.5+x)}Ga_{(3.5-2x)}O_{12}$ melt where x = 0 ~ 0.5 by modified micro-pulling down method in air using Pt crucibles. The measured lattice constants as a function of solidification fraction of grown fiber crystals are about $12.54\;{\AA}$ irrespective of x. It was found that the $Ca_3Li_{0.275}Nb_{1.775}Ga_{2.95}O_{12}$ garnet melts congruently at about $1450\;^{\circ}C$ based on the purities of garnet phase and variations of lattice parameter. Transparent and bubble-free crystals of x = 0.25 and 0.275 were grown by Czochralski techniques in air using Pt crucibles. An absorption spectrum is also reported.

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Fabrication of mineral fiber via melt spinning method from blast furnace slag

  • Wang, Xiao-Song;Hur, Bo-Young
    • 한국결정성장학회지
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    • 제24권4호
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    • pp.158-163
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    • 2014
  • Mineral fiber, or be called mineral wool when it assembles in large amounts, is a kind of wide applied man-made material with excellent thermal and acoustic insulation properties. In this work, mineral fiber was produced via melt spinning method by using iron blast furnace slag as raw material. Two critical experimental parameters for fabrication were investigated: melt pouring temperature and rotating speed of spinning wheels. The mineral fiber produced under the condition of melt pouring temperature $1500^{\circ}C$ and spinning speed 4000 rpm, showed the smoother surface and most quality, while the others had rough surfaces or with heavy shots. In general, mineral fibers with the size in the range of $12{\sim}49{\mu}m$ in diameter and 8~130 mm in length can be fabricated by this method, and the production rate is more than 34 wt.%, which could be up to 57 wt.% at maximum.

유연한 탄화규소 섬유 로프 발열체의 제조와 저항 발열 특성 (Fabrication and resistance heating properties of flexible SiC fiber rope as heating elements)

  • 주영준;조광연
    • 한국결정성장학회지
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    • 제30권6호
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    • pp.258-263
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    • 2020
  • 고분자로부터 제조되는 탄화규소 섬유는 고온 내산화성, 인장강도, 그리고 경량성 때문에 세라믹 복합체의 강화재료로 주로 적용되고 있다. 본 연구에서 탄화규소 연속섬유는 유연한 로프 형태의 고온 발열체(> 650℃)로 제조하기 위해 사용되었다. 특히, 탄화규소 섬유 발열체는 고효율의 저항 발열을 위해 단면적과 길이에 대한 저항 변화를 2-point probe 방법으로 측정하고, 비정질 탄화규소 섬유에 존재하는 산소 불순물과 결정립의 크기 제어를 통해 로프형 섬유 발열체의 저항 값을 최적화하였다. 그 결과, 약 100~200 Ω의 저항 범위를 가지는 탄화규소 섬유 발열체는 탄소 섬유 발열체보다 1.5배의 우수한 소비전력 효율을 가졌다.

도로교 RC 상판 보강을 위한 탄소섬유 기초 carbon fiber sheet와 carbon fiber strand sheet의 역학특성 (Mechanical properties of carbon fiber sheet and carbon fiber strand sheet based on carbon fibers for the reinforcement of highway bridge RC slabs)

  • 원찬호;;안태호
    • 한국결정성장학회지
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    • 제25권6호
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    • pp.290-293
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    • 2015
  • 최근 사회기반시설물의 구조물 유지관리 분야의 관심이 높아짐에 따라 새로운 유지관리 공법 및 신소재에 관한 연구가 활발히 진행되어지고 있다. 그중에서도 유지관리의 주요 대상인 교량 유지관리에는 탄소섬유를 이용한 공법이 주목을 받고 있다. 탄소섬유시트(Carbon Fiber Sheet, 이하 CFS)는 이미 여러 연구자들이 국내에서도 재료시험 및 보강공법에 관한 연구를 진행하여 연구결과가 보고되고 있지만, 탄소섬유 스트랜드 시트(Carbon Fiber Strand Sheet, 이하 CFSS)는 최근 새롭게 개발된 재료로써 아직까지 국내에는 연구 성과가 없는 실정이다. 따라서, 본 연구에서는 CFSS를 RC 상판 공시체에 접착보강하여 내피로성을 평가하였다. 그 결과, 무보강 RC 상판 공시체에 비해 약 25.3배의 보강 효과가 확인되었고, CFS 접착보강 RC 상판 공시체에 비교하여 약 1.2배의 보강 효과가 확인되었다.

$Er^{3+}$ 첨가 $LiNbO_3$ fiber 단결정의 성장 및 upconversion 특성 (Growth and upconversion properties of erbium doped $LiNbO_3$ single crystal fibers)

  • Yang, Woo-Seok;Suh, Su-Jeong;Lee, Jong-Ho;Tsuguo Fukuda;Yoon, Dae-Ho
    • 한국결정성장학회:학술대회논문집
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    • 한국결정성장학회 1999년도 PROCEEDINGS OF 99 INTERNATIONAL CONFERENCE OF THE KACG AND 6TH KOREA·JAPAN EMG SYMPOSIUM (ELECTRONIC MATERIALS GROWTH SYMPOSIUM), HANYANG UNIVERSITY, SEOUL, 06월 09일 JUNE 1999
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    • pp.321-335
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    • 1999
  • Erbium(Er) doped LiNbO3(Er:LiNbO3) single crystal gibers were grown free of cracks along the c-axis by micro-pulling down method. the Er3+ concentration was distributed homogeneously along the growth axis. The samples for optical characterization were cut from as-grown single crystal fibers and polished. When the 980 nm light was incident on the sample, upconversion phenomena were observed at the green range of wavelength 510~570 nm. In addition, the intensity of upconversion was remarkably increased by increasing the concentration of Er2O3 dopant in as-grown Er:LiNbO3 crystals.

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탄소섬유의 고온 연신 열처리에서의 변형 거동 (Strain behavior of carbon fibers during hot stretching)

  • 김홍수
    • 한국결정성장학회지
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    • 제9권1호
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    • pp.64-69
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    • 1999
  • PANrP 탄소섬유의 고온연신에서의 변형 거동을 검토하기 위해서, 일정 하중하에서 내부저항 가열법에 의해 $1200^{\circ}C$부터 $2200^{\circ}C$까지 열처리 온도를 변화시키며 섬유의 strain 변화를 측정하였다. 부하된 응력이 증가함에 따라서 strain 변화가 크게 발생하며 또한 열처리 온도 약 $1700^{\circ}C$를 경계로 해서 그 온도 이상과 이하 사이에는 큰 차이를 보였다. 각 응력에 있어서의 strain 속도 변화로부터 얻어진 활성화 에너지는 70 MPa 및 322 MPa에 대하여 각각 67.46 및 52.27 kJ/mol로써, 큰 응력의 경우가 작은 응력을 부하하는 것 보다 섬유구조 발달에 있어서 더욱 효과적이라는 것을 알았다.

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Preparation of $ZrO_2-CaO$ fiber by using a chemical solution process

  • Hwang, Kyu-Seog;Jeon, Young-Sun;Kim, Sang-Bok;Kim, Chi-Kyun;Oh, Jeong-Sun;An, Jun-Hyung;Kim, Byung-Hoon
    • 한국결정성장학회지
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    • 제13권6호
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    • pp.267-271
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    • 2003
  • In this work, chemical solution derived Ca-doped zirconia fiber has been prepared by using calcium- and zirconium-naphthenate. Fibrous $ZrO_2$-CaO was drawn from a sticky mixture. Dried gel fibers were finally annealed at $1000^{\circ}C$ for 1 h in argon. 91 mol%$ZrO_2$-9 mol%CaO fiber consisted of tetragonal, monoclinic and $CaZrO_3$ phases after annealing at $1000^{\circ}C$. On the other hand, samples annealed at $500^{\circ}C$ consisted of almost tetragonal single phase. Homogeneous fibers surface at $500^{\circ}C$ became rougher after $1000^{\circ}C$-annealing. The sample annealed at $1000^{\circ}C$ with relatively rough surface structure showed a high Calcium phocphate forming ability.