• Title/Summary/Keyword: fiber analysis

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Bismuth Coated Carbon Fiber Microelectrode with Gallic Acid n-Propyl Ester for Trace Copper Analysis (비스무스코팅 탄소섬유전극과 갤릭산 착물을 사용한 구리 이온의 흔적량 분석)

  • Ly, Suw-Young;Lee, Chang-Hyun;Jung, Young-Sam
    • Journal of Environmental Science International
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    • v.16 no.10
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    • pp.1111-1118
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    • 2007
  • A bismuth-coated carbon fiber microelectrode was prepared using cyclic voltammetry (CV). An analytical application was performed for the copper analysis with Square Wave Stripping Voltammetry (SWSV). Gallic acid n-propyl ester (PG) was used for the complex formation with a copper ion, and electrochemical measurements were performed with a pre-amplifier of a low-current module for nano am per detection. The effects of various parameters on the response were optimized. Analytical working ranges of $0.03-25.9\;{\mu}gl^{-1}$ and $0-25\'mgl^{-1}$ Cu(II) were obtained. The relative standard deviation at $13\;mgl^{-1}$ Cu was 0.9% (n = 12) in optimum conditions. The detection limit was found to have been $0.019\;{\mu}gl^{-1}$, with a 30-sec accumulation time. The developed methods were applied to a copper assay in water samples.

The Effect of Electron Beam Irradiation on Chemical and Morphological Properties of Hansan Ramie Fibers

  • Lee, Jung Soon
    • Fashion & Textile Research Journal
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    • v.15 no.3
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    • pp.430-436
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    • 2013
  • The purpose of this study investigates the effects of electron beam(EB) irradiation on the chemical and morphological properties of Hansan ramie fiber. Hansan ramie fibers were irradiated with electron beam doses of 0, 1, 3, 5 and 10kGy. The effect of electron beam irradiation on the chemical components of fibers as well as the surface chemical and morphological properties were investigated using chemical component analysis methods based on TAPPI standards, XPS, and SEM. The results indicate that the surface layers can be removed under suitable EB irradiation doses. Alcohol-benzene extraction and lignin content increases gradually with an increase in EB irradiation and reaching a maximum at an EB dose of 3kGy, and decreases at 10kGy. The surface chemical changes measured by XPS corresponded to the chemical composition analysis results. The C1 peak and the O/C ratio decreased with the removal of the multi-layer and primary layer by EB irradiation. The SEM images show the inter-fibrillar structure etched by EB irradiation up to 5kGy. At 10kGy, the surface structure of the ramie fiber shows highly aligned and distinctive striations in a longitudinal direction. The removal of these exterior layers of the fiber was confirmed by changes in surface morphology as observed in SEM images.

Wear of the Alumina Short Fiber Reinforced Tin-Bronze Matrix Composites at the Room Temperature and an Elevated Temperature (알루미나 단섬유 보강 청동기지 복합재의 상온 및 고온 마모)

  • 최준호;허무영
    • Tribology and Lubricants
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    • v.11 no.4
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    • pp.45-52
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    • 1995
  • The wear behavior of alumina short fiber reinforced tin-bronze matrix composites was studied at the room temperature and an elevated temperature. The effect of the composition of specimens and the variation of wear conditions on the wear properties was examined by a pin-on-disc type wear testing machine. The wear mechanism according to the compositon of specimens at various wear conditions was discussed by the observation of the microstructure and the analysis of the composition on the worn surfaces. A thicker oxide layer on worn surfaces led to a lower wear loss because of the lubricating effect of oxide layers between pin and disc. As the testing temperature was raised to 350$^{\circ}$C, the fiber reinforced composites exibited markedly increased wear resistance even at a higher applied load since the reinforcement of composites with alumina fibers was not affected to a large extent by raising temperature. The results obtained by AES and EDS analysis indicated that the oxide layer of the worn surfaces formed at 350$^{\circ}$C was proved as Fe-oxide. This was explained by the faster formation of Fe-oxide than Cu-oxide at 350$^{\circ}$C.

Mechanical Properties of 2-D Silica-Silica Continuous Fiber-reinforced Ceramic-matrix Composite Fabricated by Sol-Gel Infiltration

  • Kim, Ha-Neul;Kim, Dong-Jun;Kang, Eul-Son;Kim, Do-Kyung
    • Korean Journal of Materials Research
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    • v.19 no.7
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    • pp.391-396
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    • 2009
  • 2-dimensional silica-silica Continuous Fiber-reinforced Ceramic.matrix Composites (CFCCs) were fabricated by a sol-gel infilitration method that has a changing processing condition, such as the repetitions of infilitration. In order to investigate the relationship between the processing condition and the mechanical properties of composites, the mechanical properties of specimens were measured by means of a 4-point flexural strength test while the evidence of strength degradation were microstructurally characterized. There seemed to be a minimum density value that existed at which the delamination between the fabrics would not occur. In the case that the density of silica CFCCs exceeded 1.55 g/$cm^3$, the flexural strength also exceeded approximately 18 MPa at least. By applying the Minimum Solid Area (MSA) analysis of the porous structure, the correlation between the relative density and the mechanical properties of composites will be discussed.

Design and Experimental Analysis of Fiber Reinforced Elastomeric Isolator (섬유보강 탄성받침의 설계 및 실험적 해석)

  • Moon, Byung-Young;Kang, Gyung-Ju;Kang, Beom-Soo;Kim, Kye-Soo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.10
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    • pp.2026-2033
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    • 2002
  • The purpose of this study is to investigate the effect of mechanical properties of the FREI using horizontal stiffness and vertical stiffness by experiments. Two kinds of FREI are designed and fabricated. The steel plates of SREI are replaced with fibers in order to reduce the cost of fabrication and installation. At first, the Nylon fiber is adopted as feasibility study of FREI. The experimental results of Nylon FREI and SREI show that the vertical stiffness of Nylon FREI is lower than SREI, and effective damping is two times higher than SREI. Carbon is adopted, by these rusults, as strong reinforcement than Nylon and full scale of carbon FREI was designed and fabricated. By the experimental test results, it is shown that the vertical stiffness of carbon FREI is three times higher than SREI, and two times higher in effective damping. As a result, the proposed FREI can replace the SREI as a seismic isolator.

Economical selection of optimum pressurized hollow fiber membrane modules in water purification system using RbLCC

  • Lee, Chul-sung;Nam, Young-wook;Kim, Doo-il
    • Membrane and Water Treatment
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    • v.8 no.2
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    • pp.137-147
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    • 2017
  • A water treatment utility in South Korea operates a large system of pressurized hollow fiber membrane (PHFM) modules. The optimal selection of membrane module for the full scale plant was critical issue and carried out using Risk-based Life Cycle Cost (RbLCC) analysis based on the historical data of operation and maintenance. The RbLCC analysis was used in the process of decision-making for replacing aged modules. The initial purchasing cost and the value at risk during operation were considered together. The failure of modules occurs stochastically depending on the physical deterioration with usage over time. The life span of module was used as a factor for the failure of Poisson's probability model, which was used to obtain the probability of failure during the operation. The RbLCC was calculated by combining the initial cost and the value at risk without its warranty term. Additionally, the properties of membrane were considered to select the optimum product. Results showed that the module's life span in the system was ten years (120 month) with safety factor. The optimum product was selected from six candidates membrane for a full scale water treatment facility. This method could be used to make the optimum and rational decision for the operation of membrane water purification facility.

Research on eccentric compression of ultra-high performance fiber reinforced concrete columns

  • Ma, Kaize;Ma, Yudong;Liu, Boquan
    • Structural Engineering and Mechanics
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    • v.71 no.3
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    • pp.211-221
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    • 2019
  • To study the eccentric compression behavior of ultra-high performance fiber reinforced concrete (UHPFRC) columns, six UHPFRC columns and one high-strength concrete (HSC) column were tested. Variation parameters include load eccentricity, volume of steel fibers and stirrup ratio. The crack pattern, failure mode, bearing capacity, and deformation of the specimens were studied. The results showed that the UHPFRC columns had different failure modes. The large eccentric compression failure mode was the longitudinal tensile reinforcements yielded and many horizontal cracks appeared in the tension zone. The small eccentric compression failure mode was the longitudinal compressive reinforcements yielded and vertical cracks appeared in the compressive zone. Because of the bridging effect of steel fibers, the number of cracks significantly increased, and the width of cracks decreased. The load-deflection curves of the UHPFRC columns showed gradually descending without sudden dropping, indicating that the specimens had better deformation. The finite element (FE) analysis was performed to stimulate the damage process of the specimens with monotonic loading. The concrete damaged plasticity (CDP) model was adopted to characterize the behaviour of UHPFRC. The contribution of the UHPFRC tensile strength was considered in the bearing capacity, and the theoretical calculation formulas were derived. The theoretical calculation results were consistent with the test results. This research can provide the experimental and theoretical basis for UHPFRC columns in engineering applications.

Antimicrobial and Water Repellency Effect of Functional PET Fibers with ODDMAC(octadecyldimethyl(3-triethoxy silylpropyl) ammonium chloride) (ODDMAC를 이용한 항균성 및 발수성 동시 발현이 가능한 기능성 PET 섬유)

  • Yang, Heejin;Jeon, Hyeji;Lee, Sang Oh;Lee, Jaewoong
    • Textile Coloration and Finishing
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    • v.32 no.4
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    • pp.265-273
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    • 2020
  • In this study, octadecyldimethyl(3-triethoxy silylpropyl)ammonium chloride (ODDMAC) incorporated with Polyethylene terephthalate (PET) fabrics with different environmental conditions such as various temperature and time intervals. First, ODDMAC (15 weight %) was dissolved in ethanol. Then PET fabrics immersed in the ODDMAC solution at 25 ℃ for 10 minutes and dried at 80 ℃ for 5 minutes. The dried PET/PDDMAC fabrics carried out for curing process out at 110 ℃ ~ 190 ℃. The treated PET/ODDMAC has examined the surface and side coating properties through SEM analysis and elemental analysis. PET/ODDMAC fabric washed with water up to 50 times and studied the durability of the materials. It was confirmed that the treated PET fabric also exhibited good water repellency. In addition, the antimicrobial activity against the gram-positive bacteria Staphylococcus aureus and gram-negative bacteria Escherichia coli were studied by the disc diffusion method on the treated fabric.

Impact response of ultra-high performance fiber-reinforced concrete filled square double-skin steel tubular columns

  • Li, Jie;Wang, Weiqiang;Wu, Chengqing;Liu, Zhongxian;Wu, Pengtao
    • Steel and Composite Structures
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    • v.42 no.3
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    • pp.325-351
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    • 2022
  • This paper studies the lateral impact behavior of ultra-high performance fiber-reinforced concrete (UHPFRC) filled double-skin steel tubular (UHPFRCFDST) columns. The impact force, midspan deflection, and strain histories were recorded. Based on the test results, the influences of drop height, axial load, concrete type, and steel tube wall thickness on the impact resistance of UHPFRCFDST members were analyzed. LS-DYNA software was used to establish a finite element (FE) model of UHPFRC filled steel tubular members. The failure modes and histories of impact force and midspan deflection of specimens were obtained. The simulation results were compared to the test results, which demonstrated the accuracy of the finite element analysis (FEA) model. Finally, the effects of the steel tube thickness, impact energy, type of concrete and impact indenter shape, and void ratio on the lateral impact performances of the UHPFRCFDST columns were analyzed.

Progressive collapse resistance of low and mid-rise RC mercantile buildings subjected to a column failure

  • Demir, Aydin
    • Structural Engineering and Mechanics
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    • v.83 no.4
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    • pp.563-576
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    • 2022
  • This study aimed to evaluate the progressive collapse potential of buildings designed using conventional design codes for the merchant occupancy classification and subjected to a sudden column failure. For this purpose, three reinforced concrete buildings having different story numbers were designed according to the seismic design recommendations of TSCB-2019. Later on, the buildings were analyzed using the GSA-2016 and UFC 4-023-03 to observe their progressive collapse responses. Three columns were removed independently in the structures from different locations. Nonlinear dynamic analysis method for the alternate path direct design approach was implemented for the design evaluation. The plasticity of the structural members was simulated by using nonlinear fiber hinges. The moment, axial, and shear force interaction on the hinges was considered by the Modified Compression Field Theory. Moreover, an existing experimental study investigating the progressive collapse behavior of reinforced concrete structures was used to observe the validation of nonlinear fiber hinges and the applied analysis methodology. The study results deduce that a limited local collapse disproportionately more extensive than the initial failure was experienced on the buildings designed according to TSCB-2019. The mercantile structures designed according to current seismic codes require additional direct design considerations to improve their progressive collapse resistance against the risk of a sudden column loss.