• Title/Summary/Keyword: fiber analysis

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Preparation and characterization of isotropic pitch-based carbon fiber

  • Zhu, Jiadeng;Park, Sang Wook;Joh, Han-Ik;Kim, Hwan Chul;Lee, Sungho
    • Carbon letters
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    • v.14 no.2
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    • pp.94-98
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    • 2013
  • Isotropic pitch fibers were stabilized and carbonized for preparing carbon fibers. To optimize the duration and temperature during the stabilization process, a thermogravimetric analysis was conducted. Stabilized fibers were carbonized at 1000, 1500, and $2000^{\circ}C$ in a furnace under a nitrogen atmosphere. An elemental analysis confirmed that the carbon content increased with an increase in the carbonization temperature. Although short graphitic-like layers were observed with carbon fibers heat-treated at 1500 and $2000^{\circ}C$, Raman spectroscopy and X-ray diffraction revealed no significant effect of the carbonization temperature on the crystalline structure of the carbon fibers, indicating the limit of developing an ordered structure of isotropic pitch-based carbon fibers. The electrical conductivity of the carbonized fiber reached $3.9{\times}10^4$ S/m with the carbonization temperature increasing to $2000^{\circ}C$ using a four-point method.

Property Evaluation of Epoxy Resin based Aramid and Carbon Fiber Composite Materials (에폭시 수지 적용 아라미드 및 탄소섬유 복합재료의 물성연구)

  • Seo, Dae-Kyung;Ha, Na Ra;Lee, Jang-Hun;Park, Hyun-Gyu;Bae, Jin-Seok
    • Textile Coloration and Finishing
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    • v.27 no.1
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    • pp.11-17
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    • 2015
  • Recently, super fiber reinforced composite materials are widely used in many industries due to high mechanical properties. In this study, 2 different types of composite materials were manufactured in order to compare their mechanical properties. Carbon and Aramid fibers were used for reinforcement materials and Bisphenol-A type epoxy resin was for matrix. Two kinds of fiber-reinforced materials were manufactured by RIM(Resin Injection Molding) method. Before manufacturing composite materials, the optimal manufacturing and curing process condition were established and the ratio of reinforcement to epoxy resin was discussed. FT-IR analysis was conducted to clarify the structure of epoxy resin. Thermal and mechanical property test were also carried out. The cross-section of composite materials was observed using a scanning electron microscope(SEM).

Free vibration analysis of thick CGFR annular sector plates resting on elastic foundations

  • Tahouneh, Vahid
    • Structural Engineering and Mechanics
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    • v.50 no.6
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    • pp.773-796
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    • 2014
  • This paper deals with free vibration analysis of continuous grading fiber reinforced (CGFR) and bi-directional FG annular sector plates on two-parameter elastic foundations under various boundary conditions, based on the three-dimensional theory of elasticity. The plates with simply supported radial edges and arbitrary boundary conditions on their circular edges are considered. A semi-analytical approach composed of differential quadrature method (DQM) and series solution is adopted to solve the equations of motion. Some new results for the natural frequencies of the plate are prepared, which include the effects of elastic coefficients of foundation, boundary conditions, material and geometrical parameters. Results indicate that the non-dimensional natural frequency parameter of a functionally graded fiber volume fraction is larger than that of a discrete laminated and close to that of a 2-layer. It results that the CGFR plate attains natural frequency higher than those of traditional discretely laminated composite ones and this can be a benefit when higher stiffness of the plate is the goal and that is due to the reduction in spatial mismatch of material properties. Moreover, it is shown that a graded ceramic volume fraction in two directions has a higher capability to reduce the natural frequency than conventional one-dimensional functionally graded material. The multidirectional graded material can likely be designed according to the actual requirement and it is a potential alternative to the unidirectional functionally graded material. The new results can be used as benchmark solutions for future researches.

Quality Characteristics of Sugar Snap-Cookie Added to Carrot Powder (II) - Quality Characteristics of Sugar Snap-Cookie - (당근 분말을 첨가한 Sugar Snap-Cookie의 품질 특성에 관한 연구(2) - 쿠키의 품질 특성 -)

  • Hwang, Seung-Hwan
    • Journal of the East Asian Society of Dietary Life
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    • v.20 no.2
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    • pp.307-312
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    • 2010
  • Sugar snap cookies were prepared with the addition of carrot powder (2~12%) as a source of dietary fiber. Analyses of physiochemical properties, rheology and sensory evaluation of the cookies were conducted. Increasing carrot powder content weakened the flour, as evidenced by decreased diameter and increased thickness, which resulted in decreased spread factor. The water content of the carrot powder-amended cookies and unamended flour was not significantly different. The pH and L values progressively decreased and a and b values progressively increased with increasing addition of carrot powder. Textural analysis revealed no significant differences in brittleness with carrot powder addition, even though brittleness did decrease with the addition of more carrot powder. Sensory evaluation revealed a preference for cookies prepared with 2~4% carrot powder, with decreased preference at powder concentrations exceeding 6%. Addition of a dried vegetable with high fiber content caused the dietary fiber to absorb much water content, resulting in decreased diameter, increased thickness and decreased spread factor. Therefore, it is deemed desirable to increase the spread factor by controlling the water content and adding emulsifiers so as to enhance the functionality and maintain the quality of cookies.

Near field scanning optical interferometer using facet reflection of a tapered optical fiber (광섬유 탐침의 반사를 이용한 파면 분석 근접장 주사 광간섭계)

  • 유장훈;임상엽;이현호;박승한
    • Korean Journal of Optics and Photonics
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    • v.15 no.3
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    • pp.248-253
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    • 2004
  • We propose a near- field scanning optical interferometer (NSOI) based on the facet reflection of a nano-sized moveable tapered optical fiber. The interferometer can measure the position and the wave-front of a focused spot simultaneously. The interfering fringes are generated by the reflected beams from the sample surface and from the fiber facet. The wave-front analysis at the focusing position is obtained by using a phase shifting technique with a four-step algorithm. It is found that the resolution for controlling the focal position of our proposed NSOI is less than λ/3 and the measured wave-front aberration at the focal position is in good agreement with the ones obtained by a Twyman-Green interferometer.

Preparation of Activated Carbon Fiber Adsorbent for Enhancement of CO2 Capture Capacity (이산화탄소 포집능 향상을 위한 활성탄소 섬유 흡착제 제조)

  • Hwang, Su-Hyun;Park, Hyun-Soo;Kim, Dong-woo;Jo, Young-Min
    • Journal of Korean Society for Atmospheric Environment
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    • v.31 no.6
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    • pp.538-547
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    • 2015
  • Test activated carbon fiber (ACF) was prepared from Polyacrylonirile (PAN) through oxidation and chemical activation. Immersion of ACF precursors in the aqueous KOH solution enhanced the surface structure, as examined by BET pore analysis. Specific surface area increased greatly from less than $70m^2/g$ to $1226m^2/g$ with 4 M KOH, and total pore volume also rose up to $0.483cm^3/g$. In particular, it was found that micropores favorable for $CO_2$ molecule capture occupied more than 95%. Maximum $CO_2$ adsorption capacity was 3.59 mmol/g at 298 K. Low depth of pores in the present ACF may facilitate the molecules' desorption for its regeneration.

Recycling of Sound Insulation Headliner Waste Material (흡음재 폐기물의 재활용 방안)

  • Hong, Young-Ho
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.14 no.6
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    • pp.3089-3095
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    • 2013
  • The headliner was made of polyurethane(PU) and glass fiber(GF) composite materials are widely used as a sound insulation material. A large amount of waste materials occurs as a by-product in the headliner manufacturing process. In order to efficiently reuse the headliner waste materials, separation process of the components are very necessary. According to the results of thermal analysis, weight loss showed increase in the order polyurethane foam> non-foaming polyurethane> non-woven fabric> 1st layer> glass fiber in the range of up to $400^{\circ}C$. Analysis of the DSC characteristics, HDPE, LLDPE, PP, and Master Batch by adding additives the wasted scrap. As a result, except for the PP, there was no exothermic transition due to the crystallization.

Microstructural analyses of soyprotein fibers (대두 단백섬유의 미세구조 연구)

  • Kim, J.C.;Cho, S.J.;Byun, P.H.;Yoon, S.K.;Rhee, K.C.;Byun, S.M.
    • Applied Biological Chemistry
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    • v.34 no.4
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    • pp.353-359
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    • 1991
  • As a tool for the texture analyses of the soyprotein fibers, the scanning electron microscopical microstructure were studied. With the results of TPA(Texture Profile Analysis), microstructural analyses of the soyprotein fibers showed that the disulfide and hydrogen bonds are one of the most important factors determining the shape and maintenance of fiber struture. The microstructures of the hydrated soyprotein dispersion and dope, as starting materials of the soyprotein fiber were presented.

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Characteristics of Pore Development for Activated Carbon Fiber from Polyacrylonitrile(II) -Activation- (PAN계 활성탄소 섬유의 세공발달 특성(II) -활성화-)

  • Park, Jong-Hak;Cho, Byung-Rin
    • Applied Chemistry for Engineering
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    • v.4 no.1
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    • pp.113-124
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    • 1993
  • Thermogravimetric analysis of copolymer of acrylonitrile(95%) and methyl acrylate(5%) have been carried out to investigate the activation under $H_2O$(30%) -$N_2$atmosphere at various heating rates. The kinetic equation [$f=1-\exp(-a{\Delta}T)^b$] which was derived on the basis of the nonisothermal activation process of carbon fiber in the $H_2O$(30%)-$N_2$system showed good agreement with experimetal results. The pore volume upon conversion was in good agreement with the model of theoretical pore volume. The pore structures of the activated carbon fiber were influenced by the heating rate, activation temperature and internal-external conversions.

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Buckling Strength Analysis of Stiffened Composite Plates for the Optimum Laminate Structure (최적 적층구조를 위한 보강된 복합적층판의 좌굴강도 해석)

  • H.R.,Kim;J.W.,Lee
    • Bulletin of the Society of Naval Architects of Korea
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    • v.26 no.3
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    • pp.21-28
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    • 1989
  • The optimun laminated composition of the stiffened composite plates is studied from the view point of buckling strength. The finite element method is applied to the buckling analysis of the composite plates taking into account the effect of shear deformation through the plate thickness. The stiffened plate model is discretized using plate thickness and symmetrically stacked. Parametric study is carried out for the selection of the optimum laminate structure; optimum fiber angle sequence through the thickness. Laminate structure of $[-45^{\circ}/45^{\circ}/90^{\circ}/0^{\circ}]$, is found to give the best buckling strength. For the case of that layer number is more than eight, best result is obtained when layers of the same fiber angle are put together, leaving the laminate has the same fiber angle sequence as a whole.

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