• Title/Summary/Keyword: fiber analysis

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A STUDY FOR THE BONDING STRENGTH OF COMPOSITE RESIN CORE TO GLASS FIBER POST (Glass Fiber Post와 Composite Resin Core의 전단결합강도)

  • Kim Tae-Hyoung;Shim June-Sung;Lee Keun-Woo
    • The Journal of Korean Academy of Prosthodontics
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    • v.43 no.4
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    • pp.415-425
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    • 2005
  • Statement of problem : Fracture of composite resin core will be occulted by progress of crack. Bonding interface of different materials has large possibility of starting point of crack line. Therefore, the bond strength of glass fiber post to composite resin core is important for prevention of fracture. Purpose: This in vitro study tried to find out how to get the higher strength of glass fiber post to composite resin core through surveying the maximum load that fractures the post and cote complex. Materials and methods: 40 specimens made with glass fiber Posts(Style $post^{(R)}$, Metalor, Swiss) and composite resin core ($Z-100^{(R)}$, 3M, USA) were prepared and loaded to failure with push-out type shear-bond strength test in a universal test machine. The maximum fracture load and fracture mode were investigated in the specimens that were restored with four different surface treatments. With the data. ANOVA test was used to validate the significance between the test groups, and Bonferroni method was used to check if there is any significant statistical difference between each test group. Evely analysis was approved with 95% reliance. Results: On measuring the maximum fracture load of specimens, both the treatments of sandblasted and acid-etched one statistically showed the strength increase rather than the control group (p<0.005). The scanning electric microscope revealed that sand blasting made more micro-retention form not only on the resin matrix but on the glass fiber, and acid-etching contributed to increase in surface retention form, eliminated the inorganic particles in resin matrix. Specimen fracture modes investigation represented that sand blasted groups showed lower bonding failure than no-sand blasted groups. Conclusion: Referring to the values of maximum fracture load of specimens, the bonding strength was increased by sand blasting and acid-etching.

The effect of different fiber reinforcements on flexural strength of provisional restorative resins: an in-vitro study

  • Kamble, Vaibhav Deorao;Parkhedkar, Rambhau D.;Mowade, Tushar Krishnarao
    • The Journal of Advanced Prosthodontics
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    • v.4 no.1
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    • pp.1-6
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    • 2012
  • PURPOSE. The aim of this study was to compare the flexural strength of polymethyl methacrylate (PMMA) and bis-acryl composite resin reinforced with polyethylene and glass fibers. MATERIALS AND METHODS. Three groups of rectangular test specimens (n = 15) of each of the two resin/fiber reinforcement were prepared for flexural strength test and unreinforced group served as the control. Specimens were loaded in a universal testing machine until fracture. The mean flexural strengths (MPa) was compared by one way ANOVA test, followed by Scheffe analysis, using a significance level of 0.05. Flexural strength between fiber-reinforced resin groups were compared by independent samples t-test. RESULTS. For control groups, the flexural strength for PMMA (215.53 MPa) was significantly lower than for bis-acryl composite resin (240.09 MPa). Glass fiber reinforcement produced significantly higher flexural strength for both PMMA (267.01 MPa) and bis-acryl composite resin (305.65 MPa), but the polyethylene fibers showed no significant difference (PMMA resin-218.55 MPa and bis-acryl composite resin-241.66 MPa). Among the reinforced groups, silane impregnated glass fibers showed highest flexural strength for bis-acryl composite resin (305.65 MPa). CONCLUSION. Of two fiber reinforcement methods evaluated, glass fiber reinforcement for the PMMA resin and bis-acryl composite resin materials produced highest flexural strength. Clinical implications. On the basis of this in-vitro study, the use of glass and polyethylene fibers may be an effective way to reinforce provisional restorative resins. When esthetics and space are of concern, glass fiber seems to be the most appropriate method for reinforcing provisional restorative resins.

A Probabilistic Structural Design Method of Composite Propulsion System (복합재 추진기관의 확률적 구조 설계 기법)

  • Hwang, Tae-Kyung;Kim, Hyung-Kun;Kim, Seong-Eun
    • Journal of the Korean Society of Propulsion Engineers
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    • v.17 no.5
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    • pp.80-85
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    • 2013
  • This paper describes a probabilistic structural design method of composite propulsion system by comparing safety factor based on average value and allowable value with structural reliability. Generally, the required structural safety factor and reliability of composite pressure vessel are 1.5 and 0.999, respectively. In the case of structural design using average strength, the safety factor which satisfies the required structural reliability depends on the variation of fiber strength. However, the structural design using allowable value shows constant safety factor for the variation of fiber strength, because the allowable value of fiber strength is calculated by considering the variation of fiber strength. Through the analysis results, it was known that the fiber strength is the most important design random variable for the structural design of composite pressure vessel and the variation of fiber strength must be minimized to develop the high performance composite propulsion system.

An Experimental Study on Moisture Sensitivity of High Performance Cellulose Fiber Reinforced Cement Composites (고성능 셀룰로우스 섬유보강 시멘트 복합체의 수분영향에 관한 연구)

  • 원종필;문제길
    • Magazine of the Korea Concrete Institute
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    • v.8 no.5
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    • pp.163-170
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    • 1996
  • Cellulose fibers, being fairly strong and stiff as well as cheap and plentiful with low energy demand during manufacture, are strong contenders for the reinforcement of cement-based materials. Cellulose fiber-cement composites, generally manufactured by slurry-dewatering procedure, can find applications in the production of flat and corrugated cement sheets and many other thin-sheet cement products. This paper presents the results of an experimental study concerned with the effects of fiber content and moisture conditions on the flexural performance of these composites. An effort was also made to study the effect of pozzolanic admixtures on the flexural performance in different moisture conditions. The test results obtained were analyzed statistically using the analysis of variance in order to derive reliable conclusions. The results generated in this study were indicative of significant effects of fiber content and moisture condition of flexural performance. There is a tendency in flexural strength to increase in increase in fiber content up to 8%: flexural toughness values continue to increase even at higher fiber contents. Moisture content has a significant effect on the flexural performance. There is a tendency in flexural strength to decrease and flexural toughness to increase with increasing moisture content Composites incorporating pozzolans showed an increase in the flexural strength while slightly reducing the flexural toughness and were sensitive to variations in moisture content.

Fundamental Properties and Reduction of Autogenous Shrinkage of HPFRCC Depending on Various Fiber Contents and ERCO Dosages (섬유 및 ERCO 혼입율 변화에 따른 HPFRCC의 기초적 특성 및 자기수축 저감)

  • Jo, Sung-Jun;Han, Cheon-Goo
    • Journal of the Korea Institute of Building Construction
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    • v.17 no.1
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    • pp.1-8
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    • 2017
  • Recently, because of the terrorisms or warfare, the damages of human life or facilities have been increased. Hence, the Korean government launched the research group for high performance fiber reinforced cementitious composite (HPFRCC) with increased demanding on protecting and anti-explosive structures. Therefore, in this research, to apply the HPFRCC on military facilities with optimum performance on workability and performance, the fundamental properties and reduction of autogenous shrinkage of HPFRCC with various combinations of steel and organic fiber and emulsified refined cooking oil (ERCO) were evaluated. As a result, based on the comprehensive analysis, for favorable workability, strength, and autogenous shrinkage, 1.5 % of combined fiber of short steel fiber and long organic fiber and 0.5 % of ERCO was suggested as an optimum conditions.

Asbestos and Non-Asbestos Fiber Content in Lungs of Autopsied Subjects in Pohang with no Known History of Occupational Asbestos Exposure (포항지역 부검 폐조직에서 석면과 비석면 섬유농도에 관한 연구)

  • Lim, Hyun-Sul;Kim, Dong-Hoon;Sakai, Kiyoshi;Hisanaga, Naomi;Kim, Ji-Yong
    • Journal of Preventive Medicine and Public Health
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    • v.33 no.4
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    • pp.477-483
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    • 2000
  • Objectives : To obtain reference values for the pulmonary asbestos and non-asbestos fiber contents of residents in Korea and to compare them with similar results from Japan. Methods : The autopsied lung specimens from 22 deceased people (20 males and 2 females) in Pohang, without any known occupational history of asbestos exposure, were analyzed for incidence of asbestos and non-asbestos fibers by transmission electron microscopy with energy dispersive X-ray analysis after using low temperature ashing procedures. Results : Chrysotite fiber (46.2%) was the major fiber type found in the lungs of the subjects. The asbestos fiber concentrations found in males and females were $0.09\times10^6$ fiberss(g of dry lungs) and $0.30\times10^6$ fibers/(g of dry lungs), respectively, showing a geometric mean concentration $0.09\times10^6$ fibers/(g of dry lung tissue), due to the predominance of males in the sample. The non-asbestos fiber contents in males and females were $4.61\times10^6$ fibers/(g of dry lungs) and $17.79\times10^6$ fibers/(g of dry lungs), respectively, with a geometric mean concentration $5.21\times10^6$ fibers/(g of dry lung tissue). Conclusions : Residents in Pohang had significantly lower levels of both asbestos and non-asbestos fibers than urban residents in Korea. Furthermore, Koreans had significantly lower levels of both asbestos and non-asbestos fibers than Japanese.

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Processing and Characterization of Polyamide 610/Carbon Fiber/Carbon Nanotube Composites through In-Situ Interfacial Polymerization (계면중합법을 이용한 폴리아마이드 610/탄소섬유/탄소나노튜브 복합재 제조 및 물성 평가)

  • Cho, Beom-Gon;Hwang, Sang-Ha;Park, Young-Bin
    • Composites Research
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    • v.33 no.6
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    • pp.415-420
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    • 2020
  • The interfacial properties in carbon fiber composites, which control the overall mechanical properties of the composites, are very important. Effective interface enhancement work is conducted on the modification of the carbon fiber surface with carbon nanotubes (CNTs). Nonetheless, most surface modifications methods do have their own drawbacks such as high temperatures with a range of 600~1000℃, which should be implemented for CNT growth on carbon fibers that can cause carbon fiber damages affecting deterioration of composites properties. This study includes the use of in-situ interfacial polymerization of polyamide 610/CNT to fabricate the carbon fiber composites. The process is very fast and continuous and can disperse CNTs with random orientation in the interface resulting in enhanced interfacial properties. Scanning electron microscopy was conducted to investigate the CNT dispersion and composites morphology, and the thermal stability of the composites was analyzed via thermogravimetric analysis. In addition, fiber pull-out tests were used to assess interfacial strength between fiber and matrix.

Effect of the Alignment of Milled Carbon Fiber Dispersed in Various Solvents (Solvent 별 분산에 따른 Milled Carbon Fiber의 배열성 연구)

  • Lee, Sung-Kwon;Choi, Sung-Woong
    • Composites Research
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    • v.35 no.1
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    • pp.47-51
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    • 2022
  • In order to efficiently control the heat generation of electronic devices, many research has been conducted on thermally conductive composite materials. In this study, milled carbon fiber was dispersed in four solvent to investigate the relationship of carbon fiber alignment according to dispersion by solvents, and carbon fiberreinforced composite material(CFRP) was manufactured using vacuum filtration. To evaluate the arrangement of CFRP the arrangement of the prepared specimen was observed under an optical microscope, and thermal conductivity was measured by Laser Flash Analysis. The Through-plane thermal conductivity of CFRP using NMP and Ethanol was 10.79 W/mK and 10.57 W/mK respectively, which were improved by 218% and 209% compared to the In-plane thermal conductivity. The high viscosity of the solvent greatly affects the shear of the fluid, and it seemed to determine the alignment of the filler.

Development of Dietary Fiber Enriched Menu for the Aged and Analysis of Sensory and Physicochemical Characteristics (고령 소비자를 위한 식이섬유 강화식단 개발 및 관능적 이화학적 특성 분석)

  • Park, Ji-Hyun;Kim, Hae-Young
    • Journal of the Korean Society of Food Culture
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    • v.21 no.5
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    • pp.516-523
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    • 2006
  • Four dietary fiber enriched menus for the aged were developed and physicochemical were analyzed. Major foods enriching the dietary fiber were as following; kimchi & bean sprouts soup and sweet potato for menu 1, chamcheunamul and grape for menu 2, mushroom and kimchi for menu 3, dried radish leaves and green pepper for menu 4. One portion of calorie, carbohydrate, protein and fats for the aged were calculated as 567 kcal, 92.8 g, 21.3 g and 12.6 g, respectively based on recommended daily allowances for adults. Dietary fiber content increased in the menus 1, 2, 3 and 4 were 17.27%, 20.84%, 16.91%, and 23.64%, respectively. The menu 1 had significantly the highest acceptance scores among the rice, soups, side dishes and overall desirability with the acceptance sores of 4.77, 4.58, 4.62 and 4.69, respectively(p<0.05). Female showed significantly the higher acceptance scores of all of the enriched fiber menu than those of male. Moisture contents of the boiled rice with barely in menu 3 had significantly the highest value of all(p<0.05) and the side dishes of all menus did not show any significant differences at p<0.05. The pH value of boiled rice with barely in menu 3 was significantly the highest and menu 1 of kimchi & bean sprouts soup had significantly the lowest pH values(p<0.05). Hunter L value was significantly the highest in boiled rice with barley. The dietary fiber enriched menus were successfully developed for application and standardization in the meal service planning for the aged as one of trials of basic data collection.

Preparation and Improvement of Physicochemical and Functional Properties of Dietary Fiber from Corn Cob Fermented by Aspergillus niger

  • Yadi Zhou;Qijie Sun;Chao Teng;Mingchun Zhou;Guangsen Fan;Penghui Qu
    • Journal of Microbiology and Biotechnology
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    • v.34 no.2
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    • pp.330-339
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    • 2024
  • Corn cobs were fermented with Aspergillus niger to produce soluble dietary fiber (SDF) of high quality and excellent food safety. In this work, the fermentation process was optimized by single-factor test and response surface methodology (RSM). The optimal fermentation conditions were determined to be a material-liquid ratio of 1:30, an inoculum concentration of 11%, a temperature of 32℃, a time of 6 days, and a shaking speed of 200 r/min. Under these conditions, the SDF yield of corn cob increased from 2.34% to 11.92%, and the ratio of soluble dietary fiber to total dietary fiber (SDF/TDF) reached 19.08%, meeting the requirements for high-quality dietary fiber (SDF/TDF of more than 10%). Scanning electron microscopy (SEM) and Fourier-transformed infrared spectroscopy (FT-IR) analysis revealed that the fermentation effectively degraded part of cellulose and hemicellulose, resulting in the formation of a loose and porous structure. After fermentation the water swelling capacity, water-holding capacity, and oil-holding capacity of the corn cob SDF were significantly improved and the adsorption capacity of glucose, cholesterol, and nitrite ions all increased by more than 20%. Moreover, the total phenolic content increased by 20.96%, which correlated with the higher antioxidant activity of SDF. Overall, the fermentation of corn cobs by A. niger increased the yield and enhanced the functional properties of dietary fiber (DF) as well.