• Title/Summary/Keyword: fiber analysis

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Plasma Etching and Polymerization of Carbon Fiber (플라즈마 에칭과 중합에 의한 탄소섬유의 표면 개질)

  • H. M. Kang;Kim, N. I.;T. H. Yoon
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.05a
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    • pp.143-146
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    • 2002
  • Unsized AS-4 carbon fibers were etched by RF plasma and then coated via plasma polymerization in order to enhance adhesion to vinyl ester resin. The gases utilized for the plasma etching were Ar, $N_2 and O_2$, while the monomers used for the plasma polymerization coating were acetylene, butadiene and acrylonitrile. The conditions for the plasma etching and the plasma polymerization were optimized by measuring interfacial adhesion with vinyl ester resin via micro-droplet tests. Among the treatment conditions, the combination of Ar plasma etching and acetylene plasma polymerization provided greatly improved interfacial shear strength (IFSS) of 69MPa compared to 43MPa with as-received carbon fiber. Based on the SEM analysis of failure surface and load-displacement curve, it was assume that the failure might be occurred at the carbon fiber and plasma polymer coating. The plasma etched and plasma polymer coated carbon fibers were subjected to analysis with SEM, XPS, FT-IR or Alpha-Step, and dynamic contact angles and tensile strengths were also evaluated. Plasma polymer coatings did not change tensile strength and surface roughness of fibers, but decreased water contact angle except butadiene plasma polymer coating, possibly owing to the functional groups introduced, as evidenced by FT-IR and XPS.

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The Factor Analysis of Airborn Fiber Concentrations at Parking Lots in Seoul (서울 시내 일부 주차장의 공기중 섬유농도에 영향을 미치는 인자 분석)

  • Moon, Ji Young;Kim, Hyunwook
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.4 no.2
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    • pp.157-167
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    • 1994
  • This study was conducted to analyze the relationship between the types of fiber and its content and the levels of airborne fiber concentrations at eight parking lots where sprayed insulation material was found on the walls and ceilings. Also this study was designed to find the relationship between the levels of airborne fiber concentrations and such variables as air current, humidity, total exhaust volume, surface condition of insulation material and building age. The results obtained were as follows : 1. No significant correlation was found between the levels of airborne tiber concentration and the building age, air current, humidity, total exhaust volume, space and the number of traffics. 2. A significant correlation was found between the levels of airborne fiber concentration and the MMMF content of the insulation material(r=0.7594). However, no significant correlation was found between the levels of airborne fiber concentration and total fiber content of insulation material. 3. The differences of the airborne fiber concentrations among Cateogory 1, 2 and 3 classified by the degrees of surface insulation material maintenance were very significant. 4. Two bulk samples contained 30% crodicolite and 1% anthophylite. The MMMFs, in all parking lots, included mineral wool, cellulose fiber, trace cellulose fiber, trace tiber glass and vermiculite. 5. The mean value and the range of airborne fiber concentrations at 8 parking lots were $0.0239{\pm}0.0095f/cc$ and 0.0054-0.0447 f/cc, respectively. The fiber concentrations of 35 out of 38 samples(92%) were over 0.01 f/cc which is the Environment Administration's recommended asbestos level for the underground space. This study suggests that most of building insulation materials used in Korea, contain MMMF and sometimes asbestos. Currently, MMMF pollution levels may exceed the Environment Administration's recommended level for underground space. It has been found that airborne fiber concentrations increased significantly with MMMF content and with the maintenance condition of surface material. Therefore, it is recommended that a proper management technique should be developed and immediately implemented since the conditions of surface material will be gradually deteriorated due to building age and usage. Since health hazards of the MMMF, similar to those of asbestos, are being gradually acknowledged, a proper management technique which is applicable to control total airborne fiber concentrations, both asbestos and MMMF, be developed and an acceptable indoor air standard be promulgated as early as possible.

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A study on evaluation of flexural toughness of synthetic fiber reinforced shotcrete (구조용 합성섬유 보강 숏크리트 휨인성 평가에 관한 연구)

  • Moon, Kyoung-Sun;Kim, Seog-Jin;Kim, Yeon-Deok;Min, Byeong-Heon;Kim, Sang-Hwan
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.21 no.3
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    • pp.433-452
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    • 2019
  • This study deals with shotcrete reinforcing performance according to the amount of synthetic fiber (PP fiber) and proper evaluation method. The shotcrete compressive strength, flexural strength and flexural toughness were tested by setting the mixing amounts of steel fiber ($37.0kg/m^3$) and synthetic fiber (PP fiber) as parameters ($5.0kg/m^3$, $7.0kg/m^3$ and $9.0kg/m^3$). Particularly, circular panel flexural toughness test (Road and Traffic Authority, RTA) was performed to evaluate the shotcrete energy absorption capacity. As a result, the compressive strength and the bending strength of the steel fiber reinforced shotcrete were large, but the flexural toughness of the synthetic fibe (PP fiber) reinforced shotcrete was large. Therefore, synthetic fiber (PP fiber) reinforced shotcrete is considered to have a reinforcing effect comparable to that of steel fiber reinforced shotcrete. Analysis of the relationship between the flexural toughness and the energy absorption capacity of synthetic fiber (PP fiber) reinforced shotcrete revealed that the energy absorbing ability is exhibited at a flexural toughness lower than the allowable standard (3.0 MPa). (Class A: 2.55 MPa = 202J, Class B: 2.72 MPa = 282J, Class C: 3.07 MPa = 403J). As a result of this study, it can be concluded that the actual shotcrete support performance can be evaluated by evaluating the support performance of the shotcrete measured at less than the allowable standard (3.0 MPa) at the actual tunnel site.

A Progressive Failure Analysis Procedure for Composite Laminates II - Nonlinear Predictive Finite Element Analysis (복합재료 거동특성의 파괴해석 II - 비선형 유한요소해석)

  • Yi, Gyu-Sei
    • Journal of the Korean Society for Advanced Composite Structures
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    • v.5 no.4
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    • pp.11-17
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    • 2014
  • A progressive failure analysis procedure for composite laminates is completed in here. An anisotropic plastic constitutive model for fiber-reinforced composite material is implemented into computer program for a predictive analysis procedure of composite laminates. Also, in order to describe material behavior beyond the initial yield, the anisotropic work-hardening model and subsequent yield surface are implemented into a computer code, which is Predictive Analysis for Composite Structures (PACS). The accuracy and efficiency of the anisotropic plastic constitutive model and the computer program PACS are verified by solving a number of various fiber-reinforced composite laminates with and without geometric discontinuity. The comparisons of the numerical results to the experimental and other numerical results available in the literature indicate the validity and efficiency of the developed model.

Fiber Distribution Characteristics and Flexural Performance of Extruded ECC Panel (압출성형 ECC 패널의 섬유분포 특성과 휨 성능)

  • Lee, Bang-Yeon;Han, Byung-Chan;Cho, Chang-Geun;Kwon, Young-Jin;Kim, Yun-Yong
    • Journal of the Korea Concrete Institute
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    • v.21 no.5
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    • pp.573-580
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    • 2009
  • This paper presents the mix composition, production method, and curing condition applied to the extruded ECC(Engineered Cementitious Composite) panel which are able to exhibit multiple cracking and potential pseudo strain-hardening behavior. In addition to the production technique of extruded ECC panel, the effect of fiber distribution characteristics, which are uniquely created by applying extrusion process, on the flexural behavior of the panel is also focussed. In order to demonstrate fiber distribution, a series of experiments and analyses, including image processing/analysis and micro-mechanical analysis, was performed. The optimum mix composition of extruded ECC panel was determined in terms of water matrix ratio, the amount of cement, ECC powder, and silica powder. It was found that flexural behavior of extruded ECC panel was highly affected by the slight difference in mix composition of ECC panel. This is mainly because the difference in mix composition results in the change of micro-mechanical properties as well as fiber distribution characteristics, represented by fiber dispersion and orientation. In terms of the average fiber orientation, the fiber distribution was found to be similar to the assumption of two dimensional random distribution, irrespective of mix composition. In contrast, the probability density function for fiber orientation was measured to be quite different depending on the mix composition.

Analysis of Dietary Fiber Content in Korean Vegetable Foods (국내산 식물성 식품중 식이섬유 함량의 분석)

  • Lee, Kyung-Sook;Lee, Su-Rae
    • Korean Journal of Food Science and Technology
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    • v.25 no.3
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    • pp.225-231
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    • 1993
  • Total dietary fiber and crude fiber contents were analyzed for 54 different kinds of Korean vegetable foods by AOAC method. On the fresh matter basis, total dietary fiber and crude fiber contents of tested food samples ranged from $1.19{\sim}10.35%,\;0.19{\sim}1.28%$ in cereals, $1.12{\sim}1.81%,\;0.29{\sim}0.64%$ in potatoes, $2.05{\sim}18.14%,\;0.38{\sim}4.42%$, in pulses, $0.99{\sim}7.42%,\;0.35{\sim}2.61%$ in fresh vegetables, $2.28{\sim}41.14%,\;0.97{\sim}20.96%$ in processed vegetables, $0.19{\sim}2.91%,\;0.10{\sim}0.79%$ in fruits, $4.27{\sim}10.83%,\;0.96{\sim}4.62%$ in nuts and seeds, $1.62{\sim}3.94%,\;0.79{\sim}0.89%$ in mushrooms, $28.70{\sim}38.19%,\;2.17{\sim}6.41%$ in seaweeds, and $4.65{\sim}6.67%,\;2.49{\sim}3.44%$ in seasonings, respectively. The ratio of total dietary fiber/crude fiber contents ranged from 2 to 13, showing a wide variation among food commodities, necessitating the analysis of total dietary fiber content for individual food items.

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Analysis of Wind-Turbine Blade Behavior Under Static Dual-Axis Loads (풍력 블레이드에서 정적 이축하중 부하에 따른 거동 분석)

  • Son, Byung-Jik;Huh, Yong-Hak;Kim, Dong-Jin;Kim, Jong-Il
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.36 no.3
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    • pp.297-304
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    • 2012
  • For the assessment of the performance of a wind-turbine blade, a simulated loading test may be required. In this study, the blade behavior was investigated through numerical analysis using a dual-axis loading test, closely simulating the real operation conditions. The blade structure for the 100-kW-class wind-turbine system was modeled using the finite element (FE) program ANSYS. The failure criteria and buckling analysis under dual-axis loading were examined. The failure analysis, including fiber failure and inter-fiber failure, was performed with Puck's failure criterion. As the dual-axis load ratio increases, the relatively increased stress occurs at the trailing edge and skin surface 3300-3600 mm away from the root. Furthermore, it is revealed that increasing the dual-axis load ratio makes the location that is weakest against buckling move toward the root part. Thus, it is seen that the dual-axis load test may be an essential requirement for the verification of blade performance.

3D micro-CT analysis of void formations and push-out bonding strength of resin cements used for fiber post cementation

  • Uzun, Ismail Hakki;Malkoc, Meral Arslan;Keles, Ali;Ogreten, Ayse Tuba
    • The Journal of Advanced Prosthodontics
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    • v.8 no.2
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    • pp.101-109
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    • 2016
  • PURPOSE. To investigate the void parameters within the resin cements used for fiber post cementation by micro-CT (${\mu}CT$) and regional push-out bonding strength. MATERIALS AND METHODS. Twenty-one, single and round shaped roots were enlarged with a low-speed drill following by endodontic treatment. The roots were divided into three groups (n=7) and fiber posts were cemented with Maxcem Elite, Multilink N and Superbond C&B resin cements. Specimens were scanned using ${\mu}CT$ scanner at resolution of $13.7{\mu}m$. The number, area, and volume of voids between dentin and post were evaluated. A method of analysis based on the post segmentation was used, and coronal, middle and apical thirds considered separately. After the ${\mu}CT$ analysis, roots were embedded in epoxy resin and sectioned into 2 mm thick slices (63 sections in total). Push-out testing was performed with universal testing device at 0.5 mm/min cross-head speed. Data were analyzed with Kruskal-Wallis and Mann-Whitney U tests (${\alpha}=.05$). RESULTS. Overall, significant differences between the resin cements and the post level were observed in the void number, area, and volume (P<.05). Super-Bond C&B showed the most void formation ($44.86{\pm}22.71$). Multilink N showed the least void surface ($3.51{\pm}2.24mm^2$) and volume ($0.01{\pm}0.01mm^3$). Regional push-out bond strength of the cements was not different (P>.05). CONCLUSION. ${\mu}CT$ proved to be a powerful non-destructive 3D analysis tool for visualizing the void parameters. Multilink N had the lowest void parameters. When efficiency of all cements was evaluated, direct relationship between the post region and push-out bonding strength was not observed.

Free Vibration Analysis based on HSDT of Laminated Composite Plate Structures Using Multi-scale Approach (멀티 스케일 접근 방법에 의한 복합소재 적층 판구조의 HSDT 기반 고유진동 해석)

  • Lee, Sang-Youl
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.34 no.1
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    • pp.61-71
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    • 2014
  • This study carried out finite element vibration analysis of composite plate structures for construction using multi-scale approaches, which is based on the higher-order theory. The finite element (FE) models for composite structures using multi-scale approaches described in this paper is attractive not only because it shows excellent accuracy in analysis but also it shows the effect of the material combination. The FE model is used for studying free vibrations of laminated composite plates for various fiber-volume fractions. In particular, new results reported in this paper are focused on the significant effects of the fiber-volume fraction for various parameters, such as fiber angles, layup sequences, and length-thickness ratios. It may be concluded from this study that the combination effect of fiber and matrix, largely governing the dynamic characteristics of composite structures, should not be neglected and thus the optimal combination could be used to design such civil structures for better dynamic performance.

Central Composite Design Matrix (CCDM) for Phthalocyanine Reactive Dyeing of Nylon Fiber: Process Analysis and Optimization

  • Ravikumar, K.;Kim, Byung-Soon;Son, Young-A
    • Textile Coloration and Finishing
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    • v.20 no.2
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    • pp.19-28
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    • 2008
  • The objective of this study was to apply the statistical technique known as design of experiments to optimize the % exhaustion variables for phthalocyanine dyeing of nylon fiber. In this study, a three-factor Central Composite Rotatable Design (CCRD) was used to establish the optimum conditions for the phthalocyanine reactive dyeing of nylon fiber. Temperature, pH and liquor ratio were considered as the variable of interest. Acidic solution with higher temperature and lower liquor ratio were found to be suitable conditions for higher % exhaustion. These three variables were used as independent variables, whose effects on % exhaustion were evaluated. Significant polynomial regression models describing the changes on % exhaustion and % fixation with respect to independent variables were established with coefficient of determination, R2, greater than 0.90. Close agreement between experimental and predicted yields was obtained. Optimum conditions were obtained using surface plots and Monte Carlo simulation techniques where maximum dyeing efficiency is achieved. The significant level of both the main effects and interaction was observed by analysis of variance (ANOVA) approach. Based on the statistical analysis, the results have provided much valuable information on the relationship between response variables and independent variables. This study demonstrates that the CCRD could be efficiently applied for the empirical modeling of % exhaustion and % fixation in dyeing. It also shows that it is an economical way of obtaining the maximum amount of information in a short period of time with least number of experiments.