• Title/Summary/Keyword: fiber analysis

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Water Repellent Finishes of Polyester Fiber Using Glow Discharge (글로우방전을 이용한 폴리에스테르섬유의 발수가공)

  • Mo, Sang Young;Kim, Gi Lyong;Kim, Tae Nyun;Chun, Tae Il
    • Textile Coloration and Finishing
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    • v.5 no.4
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    • pp.29-41
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    • 1993
  • In order to surface Hydrophobilization of Poly(ethylene terephthalate) (PET) fiber samples were treated in the atmosphere of CF$_{4}$ or $C_{2}$F$_{6}$glow discharge. The sample used in this study was PET film which is 75$\mu$m thick made by Teijin, O-Type(Japan). The cleaned samples were placed in plasma reactor made of pyrex glass cylinder, and plasma processing was carried out by glow discharge of CF$_{4}$ or $C_{2}$F$_{6}$ gas, being continuously fed by gas flow and continuously pumped out by a vacuum system. Electric power source for generate plasma state was sustained alternating current(60Hz) and voltage was sustained 600 volt. The duration of plasma treatment varied from 15 to 120 seconds except special case, the monomer gase pressure varied from 0.02 to 0.3 Torr and power range was 10 to 90 watts. The hydrophobic features of changed PET surface were evaluated by contact angle measurement and surface chemical characteristics were analyzed by ESCA. Results can be summerized as follows. 1. The most favorable setting position of substrate was the center area between the two electrodes. 2. $C_{2}$F$_{6}$ discharge current was lower than that of CF$_{4}$ when same voltage was sustained. Treated efficiency between CF$_{4}$ and $C_{2}$F$_{6}$ did not revealed significant differences under same electric power(wattage). 3. When monomer pressure is very low below 0.02 torr, as though substrate is exposed to CF$_{4}$ or $C_{2}$F$_{6}$ plasma, it tend to be hydrophilic through a little of fluorine bond and a great deal of oxidizing reaction. 4. There brought good hydrophobilization when monomer pressure was more 0.1 torr and duration of glow discharge treatment was over 45 seconds. When monomer pressure was too high, discharge current became low. Although prolong the duration, there was no more high hydrophobilization. 5. According to ESCA analysis, there were a little CF bond and a prevailing CF$_{2}$ bond in CF$_{4}$-treated substrate. There were CF$_{3}$, a little CF and a prevailing CF$_{2}$ bond in $C_{2}$F$_{6}$-treated substrate.d substrate.

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Effect of Processing Factors on the Properties of Melt-blown PP/Ba-ferrite Composite Fabrics (Melt-blown 방사에 의한 PP/Ba-ferrite 복합 부직포 제조시의 공정인자가 부직포의 특성에 미치는 영향)

  • Han, Jong-Hun;Lee, Dong-Jin;Lim, Hyung Mi;Lee, Seung-Ho;Oh, Sung Geoun
    • Applied Chemistry for Engineering
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    • v.17 no.3
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    • pp.267-273
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    • 2006
  • We have prepared PP/Ba-ferrite composite fabrics by a melt-blown spinning method and investigated the relationship between the properties of PP/Ba-ferrite composite fabrics and melt-blown processing factors. A PP composite containing Ba-ferrite as a magnetic particulate filler was prepared in the form of pellet from PP resin and Ba-ferrite powder by melt compounding using a single extruder. Screw turning force (rpm), DCD (die-to-collector distance), and Ba-ferrite content were changed. We measured diameters of fiber, mechanical, thermal, and magnetic properties for the composited PP fabrics. The elongation was increased and a fiber diameter and tensile strength were decreased as the spinning distance increased or screw turning force decreased. The crystallinity was increased with increasing spinning distance according to XRD. It was assumed that the orientation of crystalline domain in the neat PP without ferrite was increased by drawing in mechanical direction, however, the orientation in the PP composite was decreased according to XRD analysis. We measured a magnetic property of PP nonwoven fabric containing Ba-ferrite powder. A coercive force, maximum magnetization, and residual magnetization are reduced with the spinning distance. According to the result of TGA measurement, the heat resistance was increased with the Ba-ferrite powder content and with decreasing the spinning distance.

Improvement of Durability in Concrete Structures Using CRM (내화학성 적층보강공법(CRM)을 활용한 콘크리트 구조물의 내구성능 향상)

  • Kim, Chun-Ho;Kim, Sang-Doh;Kim, Nam-Wook
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.6
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    • pp.145-152
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    • 2013
  • As a typical construction material, concrete has been used in building all kinds of structures since the late $19^{th}$ century. Although it was recognized to secure durability as long as the regulations on design and construction have been reasonably complied, the trends of life-shortening and deterioration have frequently occurred due to all kinds of the external effects that have been experienced during the procedures of using the structures. To make matters even worse, deterioration of the concrete structures according to deterioration can not be controlled any more. Finally, the reality is that repair and maintenance are necessary in the maintenance aspect of the concrete structure. In this study, CRM(Chemical Resistance of Laminating Reinforcement Method), which had been developed to reinforce the surface of concrete and specially improve chemical resistance performance, has been applied to enhance the existing repairing and maintenance method. Therefore, the result has been drawn with comparison and analysis of the specimens applied with the general repairing and maintenance method and CRM through a variety of durability test in this study. With the result of the test, durability of the specimen applied with CRM has been more improved than the existing repairing and maintenance method, which is judged as because of the laminating effect due to reinforcement of epoxy impregnated of alkali-resistance fiber and double layered fiber reinforced seat.

Statistical Evaluation of the Physico-Chemical Characteristics Affecting the Palatability of Black Tea (홍차(紅茶) 기호도(嗜好度)와 관련된 이화학적(理化學的) 특성(特性)에 대(對)한 통계적(統計的) 분석(分析))

  • Kim, Young-Soo;Kim, Hea-Young;Nam, Young-Jung;Ko, Young-Su
    • Korean Journal of Food Science and Technology
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    • v.18 no.1
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    • pp.16-23
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    • 1986
  • Physico-chemical and sensory characteristics of 28 black tea samples prepared by oaring the mixing ratio of 1 kind of Korean and 9 kinds of foreign black tea were determined, and their relationship was statistically analysed. Korean black tea was found to be lower in bulk density, caffeine, theobromine, crude protein, theaflavin, thearubigin and soluble solids, and higher in Hunter L- and b- value, neutral detergent fiber, calcium and ratio of oxidized matter as compared with foreign black tea. The palatability for 8 kinds of foreign black tea was generally increased by mixing with Korean black tea. The number of black tea whose palatability were higher than that of Korean black tea was 12, which was mostly mixed black tea. Theaflavin. Hunter a-value, soluble solids of the tea infusion, and potassium of the manufactured tea were the major guiding characteristics as a result of stepwise multiple regression analysis, and about 67% of the total variations in the palatability of black tea could be explained by the regression equation formulated by the preceding 4 characteristics.

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Development of a new lactic acid bacterial inoculant for fresh rice straw silage

  • Kim, Jong Geun;Ham, Jun Sang;Li, Yu Wei;Park, Hyung Soo;Huh, Chul-Sung;Park, Byung-Chul
    • Asian-Australasian Journal of Animal Sciences
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    • v.30 no.7
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    • pp.950-956
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    • 2017
  • Objective: Effects of newly isolated Lactobacillus plantarum on the fermentation and chemical composition of fresh rice straw silage was evaluated in this study. Methods: Lactic acid bacteria (LAB) from good crop silage were screened by growing them in MRS broth and a minimal medium with low carbohydrate content. Selected LAB (LAB 1821) were Gram-positive, rods, catalase negative, and were identified to be Lactobacillus plantarum based on their biochemical characteristics and a 16S rRNA analysis. Fresh rice straw was ensiled with two isolated LAB (1821 and 1841), two commercial inoculants (HM/F and P1132) and no additive as a control. Results: After 2 months of storage at ambient temperature, rice straw silages treated with additives were well-preserved, the pH values and butyric and acetic acid contents were lower, and the lactic acid content and lactic/acetic acid ratio were higher than those in the control (p<0.05). Acidity (pH) was lowest, and lactic acid highest, in 1821-treated silage (p<0.05). The $NH_3-N$ content decreased significantly in inoculant-treated silage (p<0.05) and the $NH_3-N$ content in 1821-treated silage was lowest among the treatments. The dry matter (DM) content of the control silage was lower than that of fresh rice straw (p<0.05), while that of the 1841- and p1174-inoculant-treated silages was significantly higher than that of HM/F-treated silage. Microbial additives did not have any significant (p>0.05) effect on acid detergent fiber or neutral detergent fiber contents. Crude protein (CP) content and in vitro DM digestibility (IVDMD) increased after inoculation of LAB 1821 (p<0.05). Conclusion: LAB 1821 increased the CP, IVDMD, lactic acid content and ratio of lactic acid to acetic acid in rice straw silage and decreased the pH, acetic acid, $NH_3-N$, and butyric acid contents. Therefore, adding LAB 1821 improved the fermentation quality and feed value of rice straw silage.

Thermal Behavior and Abrasion Properties of Glass Fiber Reinforced Nylon 12 Crosslinked by Electron Beam Irradiation (전자선 가교된 유리섬유 강화 나일론 12의 열적 거동 및 내마모 특성)

  • Shin, Bum-Sik;Jeun, Joon-Pyo;Kim, Hyun-Bin;Kang, Phil-Hyun
    • Polymer(Korea)
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    • v.35 no.1
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    • pp.30-34
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    • 2011
  • In this study, the effects of the electron beam irradiation on the thermal behavior and the abrasion properties of the glass fiber reinforced nylon 12 was investigated. The electron beam irradiation was carried out over a range of irradiation dose from 100 to 600 kGy with additive crosslinking agents such as triallyl cyanurate (TAC), triallyl isocyanurate (TAIC) and trimethylolpropane trimethacrylate (TMPTMA) for enhancing the crosslinking effects. The gel contents were increased dramatically above 200 kGy. It was verified that the degree of crosslinking depends on the radiation dose. The decreases of the melting temperature and the area of endothermic peak were observed as increasing the absorbed dose in the results of DSC analysis. The enhanced thermal stability was confirmed by the increases of decomposition temperature by electron beam irradiation. Furthermore, the negative deviations of the abrasion loss and the abrasion coefficients confirmed the improvement of the abrasion properties of irradiated nylon 12, as evidenced by SEM observation on the abrasion surfaces. The addition of the crosslinking agents to nylon 12 during effectively improved the thermal behavior and the abrasion properties of nylon 12 by the electron beam irradiation.

Evaluation of Feed Value of IRG in Middle Region Using UAV

  • Na, Sang-Il;Kim, Young-Jin;Park, Chan-Won;So, Kyu-Ho;Park, Jae-Moon;Lee, Kyung-Do
    • Korean Journal of Soil Science and Fertilizer
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    • v.50 no.5
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    • pp.391-400
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    • 2017
  • Italian ryegrass (IRG) is one of the fastest growing grasses available to farmers. It offers rapid establishment and starts growing early in the following spring and has fast regrowth after defoliation. So, IRG can be utilized as the dominant/single species of grass used in a farming system, or to play a role as a large producing pasture and sacrificial paddock. The objective of this study was to develop the use of unmanned aerial vehicle (UAV) for the evaluation of feed value of IRG. For this study, UAV imagery was taken on the Nonsan regions two times during the IRG growing season. We analyzed the relationships between $NDVI_{UAV}$ and feed value parameters such as fresh matter yield, dry matter yield, acid detergent fiber (ADF), neutral detergent fiber (NDF), total digestible nutrient (TDN) and crude protein at the season of harvest. Correlation analysis between $NDVI_{UAV}$ and feed value parameters of IRG revealed that $NDVI_{UAV}$ correlated well with crude protein (r = 0.745), and fresh matter yield (r = 0.655). According to the relationship, the variation of $NDVI_{UAV}$ was significant to interpret feed value parameters of IRG. Eight different regression models such as Linear, Logarithmic, Inverse, Quadratic, Cubic, Power, S, and Exponential model were used to estimate IRG feed value parameters. The S and exponential model provided more accurate results to predict fresh matter yield and crude protein than other models based on coefficient of determination, p- and F-value. The spatial distribution map of feed values in IRG plot was in strong agreement with the field measurements in terms of geographical variation and relative numerical values when $NDVI_{UAV}$ was applied to regression equation. These lead to the result that the characteristics of variations in feed value of IRG according to $NDVI_{UAV}$ were well reflected in the model.

COMPARISON OF MECHANICAL PROPERTIES OF VARIOUS POST AND CORE MATERIALS

  • Ahn Seung-Geun;Sorensen John A.
    • The Journal of Korean Academy of Prosthodontics
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    • v.41 no.3
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    • pp.288-299
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    • 2003
  • Statement of problem: Many kinds of post and core systems are in the market, but there are no clear selection criteria for them. Purpose: The purpose of this study was to compare the flexural strength and modulus of elasticity of core materials, and measure the bending strength of post systems made of a variety of materials. Material and Methods: The flexural strength and elastic modulus of thirteen kinds core buildup materials were measured on beams of specimens of $2.0{\times}2.0{\times}24{\pm}0.1mm$. Ten specimens per group were fabricated and loaded on an lnstron testing machine at a crosshead speed of 0.25mm/min. A test span of 20 mm was used. The failure loads were recorded and flexural strength calculated with the measured dimensions. The elastic modulus was calculated from the slopes of the linear portions of the stress-stram graphs. Also nine kinds commercially available prefabricated posts made of various materials with similar nominal diameters, approximately 1.25mm, were loaded in a three-point bend test until plastic deformation or failure occurred. Ten posts per group were tested and the obtained data were anaylzed with analysis of variance and compared with the Tukey multiple comparison tests. Results: Clearfil Photo Core and Luxacore had flexural strengths approaching amalgam, but its modulus of elasticity was only about 15% of that of amalgam. The strengths of the glass ionomer and resin modified glass ionomer were very low. The heat pressed glass ceramic core had a high elastic modulus but a relatively low flexural strength approximating that of the lower strength composite resin core materials. The stainless steel, zirconia and carbon fiber post exhibited high bending strengths. The glass fiber posts displayed strengths that were approximately half of the higher strength posts. Conclusion: When moderate amounts of coronal tooth structure are to be replaced by a post and core on an anterior tooth, a prefabricated post and high strength, high elastic modulus core may be suitable. CLINICAL IMPLICATIONS In this study several newly introduced post and core systems demonstrated satisfactory physical properties. However when the higher stress situation exists with only a minimal ferrule extension remaining a cast post and core or zirconia post and pressed core are desirable.

Properties of Rice Flours Prepared from Domestic High Amylose Rices (국내산 고아밀로오스 쌀가루의 특성)

  • Choi, Sin-Young;Shin, Mal-Shick
    • Korean Journal of Food Science and Technology
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    • v.41 no.1
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    • pp.16-20
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    • 2009
  • To develop health functional foods using high amylose rice flours, the properties of flours prepared from domestic high amylose rice varieties, Goamy2 and Goamy, and imported rice from Thailand were investigated. After soaking the rice grains and drying, the dry-milled rice flours were passed through a 120-mesh sieve. The protein and total starch contents of the Goamy2 rice flour were lowest, but its crude lipid and ash contents were highest among the flours. In addition, apparent amylose content, water binding capacity, and total dietary fiber were highest in the Goamy2 flour (36.2, 255.0, and 9.2%, respectively). The Thai rice flour had the highest swelling power, whereas the Goamy2 flour had the lowest swelling power and solubility. By Rapid visco-analysis, the Thai flour showed the highest peak and total setback viscosities and lowest breakdown viscosity. The pasting pattern of the Goamy2 flour was different from that of the other flour, where low viscosity was maintained during heating and cooling. Goamy and Thai rice flours showed an A type crystallinity, but Goamy2 flour showed a B type crystallinity similar to high amylose maize starch. The Goamy2 flour presented a dull and yellowish color, and the lowest lightness (L) value and the highest yellowness (+b) value.

Application of Lower Body Girth Change Analysis Using 3D Body Scanning to Pants Patterns

  • Choi, Sun-Yoon;Ashdown, Susan P.
    • Journal of the Korean Society of Clothing and Textiles
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    • v.34 no.6
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    • pp.955-968
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    • 2010
  • Three-dimensional body data has been used in many industry fields including the apparel industry. This research used data from a study of the changes in lower body girth measurements from a 3D scan study of 25 female subjects aged 18 to 24 in four postures; a standing posture, a $120^{\circ}$ knee bend posture, a one pace stepping posture, and a sitting posture with a $90^{\circ}$ knee bend. We used the information on the difference between standing and seated measurements to adjust ease values for pants patterns an evaluation of the appearance, and the comfort of the pants. Waist girth in the sitting posture increased 8% compared to a standing posture and the hip girth measurement increased 7%. A basic pants pattern (pants A) with 2.4cm ease at the waist and 2.6cm ease at the hip was developed and a pants pattern (pants B) was developed using the rates of lower body girth change with a 5.7cm ease (8% change) at the waist and 7cm ease (7% change) at the hip. The appearance assessment items of pants A in a standing posture were higher than pants B. On the other hand, most appearance assessment items of pants B in a sitting posture were higher than pants A, especially the ease of pants back waistline and the appearance of the whole back. Comfort assessment items of pants B in both standing and sitting postures were higher than the comfort assessment items for pants A, especially the location of pants waistline, the ease of pants at the waistline, and the ease at the abdomen. In order to find the best level of ease for better appearance and comfort in both standing and sitting postures, 20 pants were constructed with ease values at the waist and hip in increments of 1.1cm in the range between the ease values of pants A and pants B. A fit test was conducted to compare the average appearance and comfort ratings that identified the pants with the best ease values at the waist and hip. The highest total mean was achieved in the pants with a waist ease of 4.6cm and hip ease of 4.8cm.