• Title/Summary/Keyword: failure testing

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Shear bond strength of brackets bonded with different self etching primers (Self etching primer를 사용하여 부착된 교정용 브라켓의 전단결합강도의 비교)

  • Yang, Jin-Young;Kim, Min-Ji;Lim, Yong-Kyu;Lee, Dong-Yul
    • The korean journal of orthodontics
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    • v.37 no.4
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    • pp.283-292
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    • 2007
  • The purpose of this study was to evaluate the clinical usefulness of 4 self etching primers by measuring the shear bond strength of orthodontic brackets and examining the failure pattern of bracket-tooth interfaces. Methods: Seventy-five, defect-free, premolars were randomly assigned into five groups: control group (37% phosphoric acid + Transbond XT primer) and self etching primer treated groups (Transbond Plus self etching primer, Unifil bond, Clearfil SE bond, and Adhese). The shear bond strength was measured with a universal testing machine and the amount of residual adhesive remaining on the brackets after debonding was assessed by the adhesive remnant index (ARI). Results: The results showed that the groups conditioned with self etching primer had significantly lower shear bond strength than the control group (p < 0.05), although clinically acceptable. However, there were no significant differences in shear bond strength among the self etching primer groups (p > 0.05). Evaluation of the ARI scores indicated there was less resin remnant on the teeth in the groups conditioned with self etching primers, although not statistically significant. Conclusion: The results of this study suggest that all four of the self etching primers have shown acceptable bond strength for clinical use.

The Influence of Surface Treatments on Shear Bond Strength between Zirconia Core and Heat Press Ceramic Interface (지르코니아 코어의 표면처리방법이 열 가압 세라믹과의 전단결합강도에 미치는 영향)

  • Park, Hang-Min;Chung, In-Sung
    • Journal of Technologic Dentistry
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    • v.31 no.2
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    • pp.23-30
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    • 2009
  • All-ceramic restorations have gained acceptance among clinicians and patients because of their superior esthetics. Most all-ceramic systems have a 2-layer structure, using a weak veneering ceramic over a strong supporting core. often, failure of all-ceramic restorations occurs when the veneering ceramic fractures, exposing the core material. The purpose of this study was to compare the shear bond strength of heat press ceramic system (Zirpress) to zirconia core with various surface treatments. 10 metal cores and 50 zirconia cores were fabricated and divided into six groups according to surface treatment such as Zirliner application, aluminium oxide blasting, and 9.5% HF etching. Sixty specimens were prepared using Zirpress, veneered 8mm height and 3mm in diameter, over the zirconia cores (n=10). The shear bond strength test was performed in a universal testing machine with a crosshead speed of 1/min. Ultimate shear bond strength data were analyzed with One-way ANOVA and the Scheffe's test (p=.05). Within the limits of this study, the following conclusions were drawn: The mean shear bond strengths (MPa) were: 12.93 for $110{\mu}m$ aluminium oxide blasting/Rexillium III/IPS e.Max Zirpress; 14.92 for $50{\mu}m$ aluminium oxide blasting ${\pm}9.5%$ HF etching/Zirconis core/IPS e.Max Zirpress; 16.37 for $110{\mu}$ aluminium oxide blasting + 9.5% HF etching/Zirconis core/IPS e.Max Zirpress; 12.89 for $200{\mu}$ aluminium oxide blasting + 9.5% HF etching/Zirconis core/IPS e.Max Zirpress; 19.30 for 9.5% HF etching/Zirconis core/IPS e.Max Zirpress; 19.55 for Zirliner/Zirconis core/IPS e.Max Zirpress. The mean shear bond strength for ZNTZH (Zirliner/Zirconis core) and ZNTEH (9.5% HF etching/Zirconis core) were significantly superior to MS110H ($110{\mu}$ aluminium oxide blasting/Rexillium III) and ZS200EH ($200{\mu}$ aluminium oxide blasting + 9.5% HF etching/Zirconis core) (p<0.05).

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The Effect of Surface Treat`ment on Bond Strength of Polycarbonate Bracket (폴리카보네이트 브라켓 부착 시 결합강도 증진을 위한 표면처리 효과)

  • Kim, Seok-Pil;Kim, Nyeon-Kyeong;Lee, Hyun-Jung;Hwang, Hyeon-Shik
    • The korean journal of orthodontics
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    • v.36 no.5
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    • pp.331-338
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    • 2006
  • Objective: The purpose of this study was to evaluate whether the bond strength of polycarbonate brackets can be increased through surface treatment. Methods: One hundred polycarbonate brackets (Alice) were bonded to bovine incisors with light-cured adhesive. The bracket bases were treated with one of three methods; sandblasting, plastic conditioner application, and combined treatment with sandblasting and plastic conditioner. The brackets without any suraace treatment served as the control. The shear bond strength was tested with a universal testing machine, and failure pattern was assessed with the adhesive remnant index. Results: The shear bond strength in all experimental groups was higher than that of the control group (p < 0.001). The group treated with plastic conditioner after sandblasting showed statistically higher shear bond strength than the sandblasting only group to (p < 0.05). The group treated with plastic conditioner after sandblasting showed higher shear bond strength than plastic conditioner only group, but the difference was not statistically significant. Conclusion: The above results suggest that the surface treatments of polycarbonate bracket is mandatory to improve bond strength, and the most effective method is an application of plastic conditioner after sandblasting.

Suggestion for Non-Destructive Testing Equation to Estimate Compressive Strength of Early Strength Concrete (조기강도 콘크리트의 압축강도 추정을 위한 비파괴검사 실험식의 제안)

  • Lee, Tae-Gyu;Kang, Yeon-Woo;Choi, Hyeong-Gil;Choe, Gyeong-Choel;Kim, Gyu-Yong
    • Journal of the Korea Institute of Building Construction
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    • v.16 no.3
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    • pp.229-235
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    • 2016
  • In construction field, it used various technique for concrete formwork. Part of them, non-destructive test has been conducted to estimate a compressive strength of concrete easily such as rebound method and ultrasonic pulse velocity method etc. Former research has recommend proposed equation based on experimental data to investigate strength of concrete but it was sometimes deferent actual value of that from in field because of the few of data in case of early strength concrete. In this study, an experiment was conducted to analyze strength properties for early strength concrete using cylinder mold and $1,000mm{\times}1,000mm{\times}200mm$ rectangular specimen. And compressive strength of concrete was tested by non-destructive test, and calculated by the equation proposed former research. As a result, the non-destructive test results showed approximately 70 percent of the failure test value for all conditions, and worse reliability was obtained for high strength concrete samples when the ultrasonic pulse velocity method was used. Based on the scope of this study, the experimental equation for estimating compressive strength of early strength concrete from 24MPa to 60MPa was proposed.

Relationship between Eradication of Helicobacter pylori Infection and Clarithromycin Resistance (Helicobacter pylori 감염의 치료와 Clarithromycin 내성간의 연관성)

  • Sohn Seung Ghyu;Lee Jong Hwa;Lee Jung Hun;Lee Sang Hee
    • Korean Journal of Microbiology
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    • v.41 no.3
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    • pp.177-182
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    • 2005
  • H. pylori strains were isolated from antral biopsies taken during upper endoscopy in 114 dyspeptic patients with no previous therapy against H. pylori. Rapid urease test, PCR amplification of SSA and cagA gene for H. pylori detection, and Western blot for CagA expression detection were performed. H. pylori infected patients were treated with omeprazole, clarithromycin (a macrolide), and amoxicillin. At 6 weeks after the discontinuation of therapy, the bacterial eradication rate was determined by endoscopy. The resistance rate to clarithromycin and amoxicillin was $20.2\%$ and $0.0\%$, respectively. The clarithromycin resistance was mainly caused by the A2142G mutation in the 23S rRNA gene of H. pylori. MICs of clarithromycin for the A2142G mutant isolates were significantly higher than MICs for the A2143G mutant isolates. H. pylori eradication was obtained in all patients with clarithromycin-susceptible isolates but not in patients with clarithromycin-resistant isolates (P = 0.0001). These results did not appear to be biased by any differences in CagA expression. The resistance of H. pylori to clarithromycin included in the therapeutic regimens is the most important reason for treatment failure. H. pylori antimicrobial susceptibility testing of the gastric biopsy culture should be performed before choosing the first triple therapy in infected patients and the increase in prevalence of clarithromycin resistance in Korea was problematic.

THE EFFECT OF ETCHING TIME ON SHEAR BOND STRENGTH AND ADAPTIBILITY OF ONE-BOTTLE DENTIN ADHESIVE (One-bottle 상아질 접착제의 전단결합강도와 접착성에 관한 부식시간의 효과)

  • Park, Kwang-Soo;Park, Il-Yoon;Cho, Young-Gon
    • Restorative Dentistry and Endodontics
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    • v.24 no.1
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    • pp.240-250
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    • 1999
  • The purpose of this study was to evaluate the effect of different etching time on the shear bond strength and adaptibility of composite to enamel and dentin when used one-bottle adhesive Prime & Bond$^{TM}$ 2.0. The proximal and occlusal surfaces of 88 extracted human molars were ground to expose enamel(n=44) and dentin (=44) using diamond wheel saw. Teeth were randomly assigned to four test groups(n=11) and received the following treatments : Control group were conditioned with 36% phosphoric acid for 20 sec. according to the manufacturer's directions. Experimental 10 sec. group, 30 sec. group and 60 sec. group were conditioned with 36% phosphoric acid for 10 sec., 30 sec. and 60 sec., respectively. Teeth were rinsed and dried for 2 sec. Prime & Bond$^{TM}$ 2.0 were applied according to the manufacturer's directions and Spectrum$^{TM}$ TPH composite resins were bonded to enamel and dentin surfaces. All specimens were stored in distilled water for 24 hours. Eighty specimens were sheared in a Universal Testing Machine with a crosshead speed of 5mm/minute. One way ANOVA and LSD test were used for statistical analysis of the data. Failure modes of all specimens after shear bond strength test were examined and listed. Also, representive postfracture modes and eight specimens were examined under scanning electron microscope. The results of this study were as follows: 1. The shear bond strength to enamel was the highest value in 30 sec. group (20.68${\pm}$8.54MPa) and the lowest value in 10 sec. group (14.92${\pm}$6.07MPa), so there was significant difference of shear bond strength between two groups (p<0.05). But there was no significant difference among other groups (p>0.05). With longer etching time to enamel from 10 sec. to 30 sec., higher the shear bond strength was obtained, but the shear bond strength was decreased at 60 sec. etching time. 2. The shear bond strength to dentin was the highest value in control group (13.08${\pm}$6.25MPa) and the lowest value in 60 sec. group (9.47${\pm}$3.35MPa), but there was no significant difference among the all groups (p>0.05). The eching time over 20 sec. decreased the shear bond strength to dentin. 3. In SEM observation, the enamel and resin interfaces were showed close adaptation with no relation to etching time of enamel. And the dentin and resin interfaces were showed close adaptation at 20 sec. and 30 sec. etching time, but showed some gaps at 10 sec. and 60 sec. etching time. Accordingly, these results indicated that a appropriate etching time in Prime & Bond$^{TM}$ 2.0 was required to be 30 sec. in enamel and 20 sec. in dentin for the high shear bond strength and good adaptation between the composite resin and tooth substance.

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The method of development for enhancing reliability of missile assembly test set (유도탄 점검 장비의 신뢰성 향상을 위한 개발 방법)

  • Koh, Sang-Hoon;Han, Seok-Choo;Lee, Kye-Shin;Lee, You-Sang;Kim, Young-Kuk;Park, Dong-Hyun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.8
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    • pp.37-43
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    • 2018
  • A developer solves problems with isolating failures if faults are detected when inspecting missiles using the missile assembly test set (MATS) and then resumes the testing. In order to identify faults, it is necessary to analyze the data coming from the equipment, but the information received may not be sufficient, depending on the inspection environment. In this case, the developer repeats the test until the problem is reproduced or checks the performance of each piece of equipment that is related to the fault. When this task is added, schedule management becomes problematic, and development costs rise. To solve this problem, we need to design a MATS in a systematic way to increase fault coverage while satisfying the required reliability. By designing the necessary processes for each procedure, it is possible to reduce the fault identification time when a fault is detected during operations. But it is not possible to guarantee 100% fault coverage, so we provide another method by comparing costs and effects. This paper describes a development method to enhance the reliability of the missile assembly test set; it describes the expected effects when it is adapted, and describes the limitations of this method.

A Burn-in Test System with Dynamic Bone Allocation (동적 존 할당이 가능한 번인 시험 시스템)

  • Oh, Sam-Kweon;Shin, Joong-Han
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.10 no.1
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    • pp.75-80
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    • 2009
  • Bum-in test is one for eliminating semiconductor devices that are subject to early failures and other operational problems; it is usually carried out on the devices by imposing severe test conditions such as elevated voltages, temperatures, and time. In order for such a test to be performed, each burn-in board having devices to be tested, needs to be inserted into a corresponding slot. A set of such slots is called a zone. The slots comprising a zone can only have the burn-in boards with the devices of the same type. In order to test many different types of semiconductor devices, it is desirable to build a burn-in test system to have as many zones as possible. A zone controller controlling a zone, is a device that performs a burn-in test and collects test results. In case of existing systems, each zone controller takes care of a zone that consists of a fixed number of slots. Since a zone controller is, in most cases, embedded into a workstation that controls the overall testing process, adding new zone controllers is restricted by the spaces for them. As a way to solve or alleviate these problems, a dynamic zone system in which the number of slots in a zone can be dynamically allocated, is presented. This system maximizes the efficiency of system utilization, by altering the number of slots and hence minimizing the idle slots of a zone. In addition, all the test operations being performed must be aborted for maintenance in existing systems. In dynamic zone systems, however, a separate and independent maintenance is allowed for each slot, as long as the main power supply system has no problem.

Effects of Composite Floor Slab on Seismic Performance of Welded Steel Moment Connections (철골모멘트 용접접합부의 내진성능에 미치는 합성슬래브의 영향)

  • Lee, Cheol Ho;Jung, Jong Hyun;Kim, Jeong Jae
    • Journal of Korean Society of Steel Construction
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    • v.26 no.5
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    • pp.385-396
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    • 2014
  • Traditionally, domestic steel design and construction practice has provided extra shear studs to moment frame beams even when they are designed as non-composite beams. In the 1994 Northridge earthquake, connection damage initiated from the beam bottom flange side was prevalent. The upward moving of the neutral axis due to the composite action between steel beam and floor deck was speculated to be one of the critical causes. In this study, full-scale seismic testing was conducted to investigate the side effects of the composite action in steel seismic moment frames. The specimen PN700-C, designed following the domestic connection and floor deck details, exhibited significant upward shift of the neutral axis under sagging (or positive) moment, thus producing high strain demand on the bottom flange, and showed a poor seismic performance because of brittle fracture of the beam bottom flange at 3% story drift. The specimen DB700-C, designed by using RBS connection and with the details of minimized floor composite action, exhibited superior seismic performance, without experiencing any fracture or concrete crushing, almost identical to the bare steel counterpart (specimen DB700-NC). The results of this study clearly indicate that the beams and connections in seismic steel moment frames should be constructed to minimize the composite action of a floor deck if possible.

Peel strength of denture liner to PMMA and polyamide: laser versus air-abrasion

  • Korkmaz, Fatih Mehmet;Bagis, Bora;Ozcan, Mutlu;Durkan, Rukiye;Turgut, Sedanur;Ates, Sabit Melih
    • The Journal of Advanced Prosthodontics
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    • v.5 no.3
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    • pp.287-295
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    • 2013
  • PURPOSE. This study investigated the effect of laser parameters and air-abrasion on the peel strength of silicon-based soft denture liner to different denture resins. MATERIALS AND METHODS. Specimens (N=180) were prepared out of three different denture base resins (Rodex, cross-linked denture base acrylic resin; Paladent, heat-cured acrylic resin; Deflex, Polyamide resin) ($75mm{\times}25mm{\times}3mm$). A silicon-based soft denture liner (Molloplast B) was applied to the denture resins after the following conditioning methods: a) Air-abrasion ($50{\mu}m$), b) Er,Cr:YSGG laser (Waterlase MD Turbo, Biolase Technology) at 2 W-20 Hz, c) Er,Cr:YSGG laser at 2 W-30 Hz, d) Er,Cr:YSGG laser at 3 W-20 Hz, e) Er,Cr:YSGG laser at 3 W-30 Hz. Non-conditioned group acted as the control group. Peel test was performed in a universal testing machine. Failure modes were evaluated visually. Data were analyzed using two-way ANOVA and Tukey's test (${\alpha}$=.05). RESULTS. Denture liner tested showed increased peel strength after laser treatment with different parameters ($3.9{\pm}0.4-5.58{\pm}0.6$ MPa) compared to the control ($3.64{\pm}0.5-4.58{\pm}0.5$ MPa) and air-abraded groups ($3.1{\pm}0.6-4.46{\pm}0.3$ MPa), but the results were not statistically significant except for Paladent, with the pretreatment of Er,Cr:YSGG laser at 3 W-20 Hz. Polyamide resin after air-abrasion showed significantly lower peel strength than those of other groups ($3.1{\pm}0.6$ MPa). CONCLUSION. Heat-cured acrylic resin, PMMA, may benefit from Er,Cr:YSGG laser treatment at 3 W-20 Hz irradiation. Air-abrasion of polyamide resins should be avoided not to impair their peel bond strengths to silicon-based soft denture liners.