• Title/Summary/Keyword: fabricating temperature

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Characteristics of graphene sheets synthesized by the Thermo-electrical Pulse Induced Evaporation (전계 펄스 인가 증발 방법을 이용한 그라핀의 특성 연구)

  • Park, H.Y.;Kim, H.W.;Song, C.E.;Ji, H.J.;Choi, S.K.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.412-412
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    • 2009
  • Carbon-based nano materials have a significant effect on various fields such as physics, chemistry and material science. Therefore carbon nano materials have been investigated by many scientists and engineers. Especially, since graphene, 2-dimemsonal carbon nanostructure, was experimentally discovered graphene has been tremendously attracted by both theoretical and experimental groups due to their extraordinary electrical, chemical and mechanical properties. Electrical conductivity of graphene is about ten times to that of silicon-based material and independent of temperature. At the same time silicon-based semiconductors encountered to limitation in size reduction, graphene is a strong candidate substituting for silicon-based semiconductor. But there are many limitations on fabricating large-scale graphene sheets (GS) without any defect and controlling chirality of edges. Many scientists applied micromechanical cleavage method from graphite and a SiC decomposition method to the fabrication of GS. However these methods are on the basic stage and have many drawbacks. Thereupon, our group fabricated GS through Thermo-electrical Pulse Induced Evaporation (TPIE) motivated by arc-discharge and field ion microscopy. This method is based on interaction of electrical pulse evaporation and thermal evaporation and is useful to produce not only graphene but also various carbon-based nanostructures with feeble pulse and at low temperature. On fabricating GS procedure, we could recognize distinguishable conditions (electrical pulse, temperature, etc.) to form a variety of carbon nanostructures. In this presentation, we will show the structural properties of OS by synthesized TPIE. Transmission Electron Microscopy (TEM) and Optical Microscopy (OM) observations were performed to view structural characteristics such as crystallinity. Moreover, we confirmed number of layers of GS by Atomic Force Microscopy (AFM) and Raman spectroscopy. Also, we used a probe station, in order to measure the electrical properties such as sheet resistance, resistivity, mobility of OS. We believe our method (TPIE) is a powerful bottom-up approach to synthesize and modify carbon-based nanostructures.

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Fabrication of Nanopatterns for Biochip by Nanoimprint Lithography (나노임프린트를 이용한 바이오칩용 나노 패턴 제작)

  • Choi, Ho-Gil;Kim, Soon-Joong;Oh, Byung-Ken;Choi, Jeong-Woo
    • KSBB Journal
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    • v.22 no.6
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    • pp.433-437
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    • 2007
  • A constant desire has been to fabricate nanopatterns for biochip and the Ultraviolet-nano imprint lithography (UV-NIL) is promising technology especially compared with thermal type in view of cost effectiveness. By using this method, nano-scale to micro-scale structures also called nanopore structures can be fabricated on large scale gold plate at normal conditions such as room temperature or low pressure which is not possible in thermal type lithography. One of the most important methods in fabricating biochips, immobilizing, was processed successfully by using this technology. That means immobilizing proteins only on the nanopore structures based on gold, not on hardened resin by UV is now possible by utilizing this method. So this selective nano-patterning process of protein can be useful method fabricating nanoscale protein chip.

Effect of the pore size in a 3D bioprinted gelatin scaffold on fibroblast proliferation

  • Choi, Dong Jin;Park, Sang Jun;Gu, Bon Kang;Kim, Young-Jin;Chung, Seok;Kim, Chun-Ho
    • Journal of Industrial and Engineering Chemistry
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    • v.67
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    • pp.388-395
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    • 2018
  • Significant efforts have been applied toward fabricating three-dimensional (3D) scaffolds using 3D-bioprinting tissue engineering techniques. Gelatin has been used in 3D-bioprinting to produce designed 3D scaffolds; however, gelatin has a poor printability and is not useful for fabricating desired 3D scaffolds using 3D-bioprinting. In this study, we fabricated pore size controlled 3D gelatin scaffolds with two step 3D-bioprinting approach: a low-temperature ($-10^{\circ}C$) freezing step and a crosslinking process. The scaffold was crosslinked with 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide hydrochloride (EDC) and N-hydroxysuccinimide (NHS). The pore sizes of the produced 3D gelatin scaffolds were approximately 30% smaller than the sizes of the designed pore sizes. The surface morphologies and pore sizes of the 3D gelatin scaffolds were confirmed and measured using scanning electron microscopy (SEM). Human dermal fibroblasts (HDFs) were cultured on a 3D gelatin scaffold to evaluate the effect of the 3D gelatin scaffold pore size on the cell proliferation. After 14 days of culture, HDFs proliferation throughout the 3D gelatin scaffolds prepared with more than $580{\mu}m$ pore size was approximately 14% higher than proliferation throughout the 3D gelatin scaffold prepared with a $435{\mu}m$ pore size. These results suggested that control over the 3D gelatin scaffold pore size is important for tissue engineering scaffolds.

Preparation of Low Voltage ZnO Varistor Using Seed Grain Method and Its Electrical Properties (종결정법을 이용한 저전압 ZnO 배리스터의 제조 및 전기적 특성)

  • 강승구;오재희
    • Journal of the Korean Ceramic Society
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    • v.25 no.5
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    • pp.552-560
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    • 1988
  • ZnO low voltage varistor was obtained by varying a) the amount of seed grains, b) the size of seed grains, and c) sintering temperature. Also, the optimum condition for fabricating the ZnO seed grains was studied. Large ZnO seed grains were obtained by washing a ZnO sintered body containing 1m/of BaCO3 in boiling water. When the seed grains were added, abnormal grain growth occurred, and the varistor voltage sharply decreased. However, when more than 5w/o of seed grain content was added, the varistor voltage gradually increased. When 10w/o seed grains of 75~106${\mu}{\textrm}{m}$ were added and sintered for 2 hours at 1200 to 125$0^{\circ}C$, low voltage varistor properties with V1mA/mm of 19V/mm and nonlinear exponent ($\alpha$) of 12 occurred.

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Characterization of Planar Optical Waveguides by Ag$^{+}$ -Na$^{+}$ Ion Exchange in BK7 Glass (Ag$^{+}$ -Na$^{+}$이온교환법을 이용한 BK7 유리 평판형 광도파로의 특성)

  • 전금수;반재경
    • Journal of the Korean Institute of Telematics and Electronics D
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    • v.35D no.1
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    • pp.84-93
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    • 1998
  • Planar graded index optical waveguides have been formed by Ag$^{+}$ ion exchange in the BK7 optical glass. The experimental results of diffusion and modal characteristics of Ag$^{+}$-Na$^{+}$ exchanged BK7 glass waveguides are presented. Measurements of the mode indices have been measured. We found the relations between the process and device parameters such as the diffusion depth and the square root of the diffusion time, diffusion coefficient and diffusion temperature, and diffusion ion concentration and surface index change. A theoretical gaussian function refractive index profile matched best with the measured data for all the guided modes. The empirical relations between the process and the device parameters are derived and subsequently used to formulate a systematic procedure for fabricating singlemode and multimode waveguides.uides.

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Humidity Sensing Properties of 90[wt%] SnO2-10[wt%] TiO2 Ceramics (90[wt%] SnO2-10[wt%] TiO2 세라믹스의 습도감지특성)

  • You, Do-Hyun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.63 no.9
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    • pp.1227-1232
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    • 2014
  • The purpose of this paper is to establish the optimum fabricating condition of specimens using silk screen printing, and to develop humidity sensor which has good humidity sensing properties. The specimens are fabricated under the condition of 90[wt%] $SnO_2$-10[wt%] $TiO_2$, and their microstructure, crystalline structure, humidity sensing properties are examined. From the microstructure analyses, porosity is best at 700[$^{\circ}C$]. From the crystalline structure analyses, intensity of peak becomes strong according to increasing heat treatment temperature. From the humidity sensing properties analyses, an overall results of capacitance changes, linearity and hysteresis for the specimens is best at 600[$^{\circ}C$] and 700[$^{\circ}C$]. Capacitance of specimens increases according to decreasing measurement frequency, and to increasing relative humidity.

Quality Evaluations of Induction Motors Bracket Castings during Fabrication Processes (유도전동기 브라켓 제작시 품질평가)

  • Park, Sang-Chul
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.9
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    • pp.5474-5479
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    • 2014
  • This study evaluated the residual stress and deformation for bracket castings of induction motors. Numerical analyses were performed to evaluate the residual stress distributions and displacements of bracket castings after the casting and final machining processes. Based on the analysis results, it was found that bracket casting was satisfied with the internal quality standards during the fabricating processes.

Effect of Pore Formers and Sintering Temperatures on Microstructure and Bending Strength of the Porous Zirconia Ceramics (기공 형성제 조절과 소결 온도의 변화가 다공질 지르코니아 세라믹스의 미세구조 및 강도에 미치는 영향)

  • Lee, Eun-Jung;Song, In-Hyuck;Ha, Jang-Hoon;Hahn, Yoo-Dong;Kim, Yang-Do
    • Journal of Powder Materials
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    • v.18 no.6
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    • pp.502-509
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    • 2011
  • In this study, a novel-processing route for fabricating microcellular zirconia ceramics has been developed. The proposed strategy for making the microcellula zirconia ceramics involved hollow microspheres as pore former. Compared to conventional dense microspheres pore former, well-defined pore structured zirconia ceramics were successfully fabricated. Effects of hollow microsphere content and sintering temperature on microstructure, porosity, pore distribution, and strength were investigated in the processing of microcellular zirconia ceramics.

Ag Nanowires Prepared by a Modified Polyol Method with 1,4-Benzoquinone Additives

  • Kang, Miseon;Chung, Eunseon;Kim, Sang-Ho;Rhee, Seog Woo
    • Bulletin of the Korean Chemical Society
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    • v.35 no.11
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    • pp.3209-3212
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    • 2014
  • This paper describes a selective synthetic method of fabricating Ag nanowires by using a modified polyol process. To synthesize the Ag nanowire, an ethylene glycolic solution of silver nitrate and an ethylene glycolic solution of polyvinylpyrrolidone solution containing a small amount of organic oxidant, 1,4-benzoquinone, were slowly added to a hot ethylene glycol medium at $160^{\circ}C$ for 8 min using a syringe pump. The reaction mixtures were heated for an additional 45 min and cooled to room temperature. Finally, the silver nanomaterials were isolated from the mixture by centrifugation. The crystal structure of the nanomaterials was investigated by powder X-ray diffraction analyses, and their morphology was investigated by scanning electron microscopy. A small amount of organic oxidant, 1,4-benzoquinone, played a significant role in controlling the morphology during crystal growth. Consequently, Ag nanowires rather than Ag nanoparticles were selectively obtained.

Nanoparticles-induced Alignment in Liquid Crystal Cells

  • Jeng, Shie-Chang;Kuo, Chia-Wei;Lin, Yan-Rung;Wang, Hsing-Lung;Liao, Chi-Chang;Yang, Chen-Yu;Hwang, Shug-June
    • 한국정보디스플레이학회:학술대회논문집
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    • 2008.10a
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    • pp.1077-1079
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    • 2008
  • Nanoparticles-induced vertical alignment (NIVA) in the liquid crystal (LC) devices was observed and has been applied successfully on fabricating the hybrid-aligned nematic LC cells and guest-host LC cells. In this talk, we will discuss the characteristics of the electric and optical properties of NIVA-LC cells with different dopant concentrations and demonstrate that nanoparticles can be spin-coated on the substrate at a low temperature.

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