• 제목/요약/키워드: encapsulation technique

검색결과 67건 처리시간 0.019초

A Case Study of Paraffin Double-walled Microencapsulation Preparation Using Acrylic Polymer and Melamine Polymer for Thermal Energy Storage

  • Nguyen, Hang Vo-Minh;Kim, Chae-Hyun;Kim, Jong-Kuk
    • 한국태양에너지학회 논문집
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    • 제39권5호
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    • pp.65-78
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    • 2019
  • In this study, we investigated the paraffin encapsulation using double-walled encapsulation technique. The first encapsulation used methyl methacrylic acid as the main component in acrylic polymer and the second encapsulation used melamine polymer. Particles size and distribution of the capsules were analyzed using scanning electron microscopy. In the first encapsulation, the stable capsules were obtained at 67% of phase change material ratio to methyl methacrylic acid monomer and the size of the capsule was from 0.2 to $0.3{\mu}m$. In the second encapsulation, the size of the capsules was almost the same with those capsules prepared in the first encapsulation. The particle size of single wall and double wall was about $0.3{\mu}m$. As a result of the encapsulation of paraffin using double-walled encapsulation technique, it was confirmed that the particle size was determined in the process of encapsulating using the acrylic polymer at the first wall material, and the physical and thermal stability of the capsules were imparted using melamine at the secondary wall material.

Cryopreservation of Zygotic Embryos of Herbaceous Peony (Paeonia lactiflora Pall.) by Encapsulation-Dehydration

  • Kim Hyun-Mi;Shin Jong-Hee;Sohn Jea-Keun
    • 한국작물학회지
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    • 제49권4호
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    • pp.354-357
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    • 2004
  • A simplified technique which cryoprotects zygotic embryos by encapsulation-dehydration was developed for the germplasm conservation of herbaceous peony (Paeonia lactiflora Pall.). The highest survival rate $(85\%)$ was obtained from embryos treated by encapsulation-dehydration. The zygotic embryos were precultured on MS medium containing 0.3mg/L $GA_3$ for 1 day. The precultured embryos were encapsulated in $3\%$ (w/v) alginate beads and immersed for 1 h in MS medium containing 2 M glycerol and 0.5 M sucrose. The encapsulated embryos were dehydrated for 5h by air drying prior to direct immersion in liquid nitrogen. This encapsulation-dehydration method appears to be a promising technique for germplasm cryopreservation of a herbaceous peony.

Density Compatibility of Encapsulation of White Inorganic $TiO_2$ Particles Using Dispersion Polymerization Technique for Electrophoretic Display

  • Kim, Mi-Kyung;Joung, Meyoung-Ju;Kim, Chul-Am;Lee, Yong-Eui;Ahn, Seong-Deok;Kang, Seung-Roul;Suh, Kyung-Soo
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2002년도 International Meeting on Information Display
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    • pp.825-827
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    • 2002
  • The polymer encapsulation of white inorganic $TiO_2$ pigment particles was prepared by a two stage dispersion polymerization technique for applications in electrophoretic displays (EPDs). In order to give functionality for inorganic pigment particles in the EPD, we have investigated the density of the polymer encapsulated $TiO_2$ particles. The average density of the polymer encapsulated $TiO_2$ particles was 2.2 at 25$^{\circ}C$. The average density of the polymer encapsulated $TiO_2$ particles is suitable to 1.7, due to density matching with suspending media. Therefore, we will attempt density compatibility of dispersion polymerization technique for encapsulation of $TiO_2$ particles in suspending media.

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Encapsulation of Semiconductor Gas Sensors with Gas Barrier Films for USN Application

  • Lee, Hyung-Kun;Yang, Woo Seok;Choi, Nak-Jin;Moon, Seung Eon
    • ETRI Journal
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    • 제34권5호
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    • pp.713-718
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    • 2012
  • Sensor nodes in ubiquitous sensor networks require autonomous replacement of deteriorated gas sensors with reserved sensors, which has led us to develop an encapsulation technique to avoid poisoning the reserved sensors and an autonomous activation technique to replace a deteriorated sensor with a reserved sensor. Encapsulations of $In_2O_3$ nanoparticles with poly(ethylene-co-vinyl alcohol) (EVOH) or polyvinylidene difluoride (PVDF) as gas barrier layers are reported. The EVOH or PVDF films are used for an encapsulation of $In_2O_3$ as a sensing material and are effective in blocking $In_2O_3$ from contacting formaldehyde (HCHO) gas. The activation process of $In_2O_3$ by removing the EVOH through heating is effective. However, the thermal decomposition of the PVDF affects the property of the $In_2O_3$ in terms of the gas reactivity. The response of the sensor to HCHO gas after removing the EVOH is 26%, which is not significantly different with the response of 28% in a reference sample that was not treated at all. We believe that the selection of gas barrier materials for the encapsulation and activation of $In_2O_3$ should be considered because of the ill effect the byproduct of thermal decomposition has on the sensing materials and other thermal properties of the barrier materials.

Evaluation of Bacillus velezensis for Biological Control of Rhizoctonia solani in Bean by Alginate/Gelatin Encapsulation Supplemented with Nanoparticles

  • Moradi-Pour, Mojde;Saberi-Riseh, Roohallah;Esmaeilzadeh-Salestani, Keyvan;Mohammadinejad, Reza;Loit, Evelin
    • Journal of Microbiology and Biotechnology
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    • 제31권10호
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    • pp.1373-1382
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    • 2021
  • Plant growth promoting rhizobacteria (PGPR) are a group of bacteria that can increase plant growth; but due to unfavorable environmental conditions, PGPR are biologically unstable and their survival rates in soil are limited. Therefore, the suitable application of PGPR as a plant growth stimulation is one of the significant challenges in agriculture. This study presents an intelligent formulation based on Bacillus velezensis VRU1 encapsulation enriched with nanoparticles that was able to control Rhizoctonia solani on the bean. The spherical structure of the capsule was observed based on the Scanning Electron Microscope image. Results indicated that with increasing gelatin concentration, the swelling ratio and moisture content were increased; and since the highest encapsulation efficiency and bacterial release were observed at a gelatin concentration of 1.5%, this concentration was considered in mixture with alginate for encapsulation. The application of this formulation which is based on encapsulation and nanotechnology appears to be a promising technique to deliver PGPR in soil and is more effective for plants.

애드 혹 네트워크에서 위치 정보와 홉 카운트 기반 ETWAD(Encapsulation and Tunneling Wormhole Attack Detection) 설계 (A Design of ETWAD(Encapsulation and Tunneling Wormhole Attack Detection) based on Positional Information and Hop Counts on Ad-Hoc)

  • 이병관;정은희
    • 한국컴퓨터정보학회논문지
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    • 제17권11호
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    • pp.73-81
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    • 2012
  • 본 논문에서는 애드 혹 네트워크의 노드 위치 정보와 홉 수를 이용하여 캡슐화 웜홀 공격과 터널링 웜홀 공격을 탐지하는 ETWAD(Encapsulation and Tunneling Wormhole Attack Detection) 기법을 설계하였다. ETWAD 탐지 기법은 애드 혹 네트워크 내의 노드 ID와 그룹 키로 노드의 신분을 확인할 수 있는 GAK(Group Authentication Key)를 생성하여 RREQ와 RREP에 추가하여 애드 혹 네트워크의 구성원임으로 인증할 수 있도록 설계하였다. 또한, ETWAD 탐지 기법은 RREP 메시지 내의 홉 수를 카운트하고, 근원지 노드 S와 목적지 노드 D의 거리를 계산하여 임계치와 홉 수를 이용하여 캡슐화 웜홀 공격, 터널링 공격을 탐지하는 GeoWAD 알고리즘을 설계하였다. 그 결과, 평균 웜홀 공격 탐지율이 91%, 평균 FPR이 4.4%로 평가되므로 ETWAD 탐지 기법은 웜홀 공격 탐지율과 웜홀 공격 탐지의 신뢰성을 향상시켰다고 볼 수 있다.

IPv4 방화벽에 호환성을 갖는 IPv6 터널링 (IPv6 over IPv4 tunneling compatible with IPv4 Firewalls)

  • 이정남;장주욱
    • 정보처리학회논문지C
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    • 제10C권4호
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    • pp.519-524
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    • 2003
  • 본 논문은 방화벽에 독립적인 IPv6 터널링 기법의 연구에 관한 것이다. IPv4망의 인프라를 유지하면서 점진적으로 IPv6망을 확대해 나가고 있는 철재, IPv6망간의 연동을 위해서 터널링을 널리 사용하고 있으나 방화벽에 의해 IPv4로 캡슐화된 패킷이 방화벽을 통과하지 못하는 문제점이 확인되었다. 즉, 방화벽 내부의 사용자들은 IPv6망의 접속에 제한을 받게 되며 방화벽 없이 IPv6망을 구축해야 한다. 본 논문에서는 방화벽에 의해 캡슐화된 패킷이 차단되는 것을 해결하기 위한 방법으로 Double-encapsulation 방식과 HTTP 터널링 기법을 응용한 방식을 제안하였으며 실험결과 패킷 차단없이 IPv6망간의 연동이 이루어짐을 확인하였다.

Development of New Reverse Micellar Microencapsulation Technique to Load Water-Soluble Drug into PLGA Microspheres

  • Kim Hyun Joo;Cho Mi Hyun;Sah Hong Kee
    • Archives of Pharmacal Research
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    • 제28권3호
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    • pp.370-375
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    • 2005
  • The objective of this study was to develop a new reverse micelle-based microencapsulation technique to load tetracycline hydrochloride into PLGA microspheres. To do so, a reverse micellar system was formulated to dissolve tetracycline hydrochloride and water in ethyl formate with the aid of cetyltrimethylammonium bromide. The resultant micellar solution was used to dissolve 0.3 to 0.75 g of PLGA, and microspheres were prepared following a modified solvent quenching technique. As a control experiment, the drug was encapsulated into PLGA microspheres via a conventional methylene chloride-based emulsion procedure. The micro­spheres were then characterized with regard to drug loading efficiency, their size distribution and morphology. The reverse micellar procedure led to the formation of free-flowing, spherical microspheres with the size mode of 88 ~m. When PLGA microspheres were prepared follow­ing the conventional methylene chloride-based procedure, most of tetracycline hydrochloride leached to the aqueous external phase: A maximal loading efficiency observed our experimental conditions was below $5\%$. Their surfaces had numerous pores, while their internal architecture was honey-combed. In sharp contrast, the new reverse micellar encapsulation technique permitted the attainment of a maximal loading efficiency of 63.19 $\pm$$0.64\%$. Also, the microspheres had smooth and pore-free surfaces, and hollow cavities were absent from their internal matrices. The results of this study demonstrated that PLGA microspheres could be successfully prepared following the new reverse micellar encapsulation technique.

W/O/W 다중유화법을 이용한 젬시타빈 함유 Methoxy Poly(ethylene glycol)-b-Poly(L-lactide) 미립자 제조 (Preparation of Gemcitabine-Loaded Methoxy Poly(ethylene glycol)-b-Poly(L-lactide) Microparticles Using W/O/W Double Emulsion)

  • 유종훈;정인일;이지은;임교빈
    • KSBB Journal
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    • 제26권4호
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    • pp.333-340
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    • 2011
  • In this study, gemcitabine-loaded methoxy poly(ethylene glycol)-b-poly(L-lactide) (MPEG-PLLA) microparticles with different PEG block lengths were prepared by a W/O/W double emulsion technique. The present study focuses on the investigation of the influence of various preparative parameters such as the ratio of internal water phase and oil phase, polymer concentration, solvent composition of organic phase and salt concentration of external water phase on the morphology and encapsulation efficiency of the microparticles. The microparticles fabricated at high volume ratios of internal water phase to oil phase and at high polymer concentrations showed a relatively high encapsulation efficiency and low porosity. When a dichloromethane/ethyl acetate mixture was used as solvent, both the encapsulation efficiency and drug loading of the microparticles decreased as the level of ethyl acetate increased. The addition of a salt (NaCl) to the external water phase significantly improved the encapsulation efficiency up to 40%, and the microparticles became more spherical with their size and porosity decreased.

Zn-Ion Coated Structural $SiO_2$ Filled LDPE: Effects of Epoxy Resin Encapsulation

  • Reddy C. S.;Das C. K.;Agarwal K.;Mathur G N.
    • Macromolecular Research
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    • 제13권3호
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    • pp.223-228
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    • 2005
  • In the present work, a low-density polyethylene (LDPE) composite, filled with Zn-ion coated structural silica encapsulated with the diglycidyl ether of bisphenol-A (DGEBA), was synthesized using the conventional melt-blending technique in a sigma internal mixer. The catalytic activity of the Zn-ions (originating from the structural silica) towards the oxirane group (diglycidyl ether of bisphenol-A (DGEBA): encapsulating agent) was assessed by infrared spectroscopy. Two composites, each with a filler content of $2.5 wt\%$ were developed. The first one was obtained by melt blending the Zn-ion coated structural silica with LDPE in a co-rotating sigma internal mixer. The second one was obtained by melt blending the same LDPE, but with DGEBA encapsulated Zn-ion coated structural silica. Epoxy resin encapsulation of the Zn-ion coated structural silica resulted in its having good interfacial adhesion and a homogeneous dispersion in the polymer matrix. Furthermore, the encapsulation of epoxy resin over the Zn-ion coated structural silica showed improvements in both the mechanical and thermal properties, viz. a $33\%$ increase in the elastic modulus and a rise in the onset degradation temperature from 355 to $371^{\circ}C$, in comparison to the Zn-ion coated structural silica.