• 제목/요약/키워드: emulsifying agent

검색결과 51건 처리시간 0.026초

고분자(高分子) 계면활성제(界面活性劑)에 관한 연구(硏究) (제(第) 4 보(報));나트륨 알파술폰 지방산(脂肪酸) 알릴에스테르 올리고머류(類)의 계면활성(界面活性) (Studies on the Polymeric Surfactants (IV);Synthesis Activities of Sodium ${\alpha}-Sulfo$ Fatty Acid Allyl Ester Oligomers)

  • 이승열;김진현;남기대
    • 한국응용과학기술학회지
    • /
    • 제6권2호
    • /
    • pp.53-58
    • /
    • 1989
  • A series of four sodium ${\alpha}-sulfo$ fatty acid allylester oligomers such as sodium ${\alpha}-sulfo$ lauric acid allylester oligomer, sodium ${\alpha}-sulfo$ myristic acid allyl ester oligomer, sodium ${\alpha}-sulfo$ palmitic acid allyl ester oligomer and sodum ${\alpha}-sulfo$ stearic acid allyl ester oligomer were examined for surface tension, defloculation effect and emulsifying power. Also critical micelle concentration (cmc) was evaluated. Consequently, these sodium allyl ${\alpha}-sulfo$ aliphatic carboxylate aligomers show o/w type emulsifying agent and dispersion effect in 1g/100ml soulution.

Acinetobacter sp. BE-254에 의한 유화제의 생산

  • 김순한;임이종;최경숙;정영기;장경립;이태호
    • 한국미생물·생명공학회지
    • /
    • 제24권2호
    • /
    • pp.206-212
    • /
    • 1996
  • The strain producing bioemulsifier was isolated from soil samples. The isolated strain was identified as the genus Acinetobacter through its morphological, cultural and physiological characteristics. The highest emulsification activity and stability by Acinetobacter sp. BE-254 was observed after 5 days of cultivation in the culture medium containing n-hexadecane 4%, NaNO$_{3}$ 0.2%, KH$_{2}$PO$_{4}$ 0.01%, MgSO$_{4}$-7H$_{2}$O 0.01%, CaCl$_{2}$ 0.01%, and yeast extract 0.01%. The optimum pH and temperature for bioemulsifier production were pH 7.0 and 30$\circ$C, respectively. Furthermore the most of bioemulsifier was produced during the exponential growth phase, and this suggested that the bioemulsifier production was growth-associated. The bioemulsifier showed good emulsification activity on various emulsifying substrates such as hydrocarbons, edible oils, and petroleum fractions.

  • PDF

여러 배양방법하에서 Acinetobacter calcoaceticus RAG-1에 의한 Emulsan의 생산 (Production of Emulsan by Acinetobacter calcoaceticus RAG-1 under Various Culture Modes)

  • 강병철;이필경장호남
    • KSBB Journal
    • /
    • 제6권4호
    • /
    • pp.389-394
    • /
    • 1991
  • Emulsan is an extracellular emulsifying agent produced by the hydrocarbon-degrading Acinetobacter species RAG-1. In this study emulsan production of Acinetobacter calcpaceticus RAG-1 was investigated under various culture modes such as batch, fed-batch, membrane cell recycle, and continuous culture. The productions of emulsan under both ethanol-sufficient fed-batch and membrane cell recycle cultures were all 15.0U/ml, which was 53% increase in emulsan activity compared to that of pH controlled batch culture. Emulsan production was found to be strongly dependent on the residual ethanol concentration. In continuous culture the emulsan productivity increased with dilution rate.

  • PDF

잠재적 화재.폭발 위험 지역 작업용 녹전환형 중방식 코팅제의 특성에 관한 연구 (A Study on the Properties of the Heavy Duty Rust-Converting Agent used in the Potential Hazard Areas of Fire & Explosion)

  • 강영구
    • 한국안전학회지
    • /
    • 제13권3호
    • /
    • pp.102-111
    • /
    • 1998
  • This study was concerned with the development of a heavy duty rust-converting agent, the function of which is to form metal complex coatings, containing vinyl halide-acrylic terpolymer emulsion, defoamer, emulsifying agent, glass flakes, chelating agent such as gallotannic acid, gallic acid, and pyrogallic acid, and other additives. The resulted emulsion products(Sample No.1~No.5) were characterized through test either in the forms of emulsions, which include Viscosity, Penetration rate, Acidity and Film drying rate test, or in the forms of coated layer on rusty steel substrates by FT-IR, which include hardness, gloss, salt spray, adhesion and flame retardant test. The test results are as follows ; Penetration rate(0.1~0.4 mm/min), Solid content(70%), Acidity (pH 1.8~2.0), Specific gravity(1.30~1.35), Film drying rate(108min, RH 40% ; 150min, RH 80%), Gloss(83~92, incident angle $60^{\circ}$; 88~97, incident angle $85^{\circ}$), Pencil hardness(4H~5H), Adhesion (100/100), Salt spray test(>720Hr), LOI(%) value(38%), Vertical burning test(UL 94-v-l). According to the various performance of specimens show above, the evaluation of the availability of this heavy duty rust-converting agent can be concluded that all the samples(No.1~No.5) are capable of being used in the field of chemical plant and in the hazard areas of fire and explosion potential. It was observed that the properties of sample No.2, especially gloss and hardness, were much better than that of the other samples.

  • PDF

유화제의 구조에 따른 W/O 에멀젼의 특성 및 안정도에 관한 연구 (An Experimental Study on the Property and Stability of W/O Emulsion by Various Structures of Emulsifier)

  • 김운하;이광식;이건국
    • 대한화장품학회지
    • /
    • 제38권2호
    • /
    • pp.119-131
    • /
    • 2012
  • w/o 에멀젼은 내수성이 뛰어나고 보습 효과를 오랫동안 지속시킬 수 있으므로 화장품에 많이 사용하지만 안정도가 좋지 않기 때문에 안정한 w/o 에멀젼을 만들기 위해서는 전해질의 농도, 오일의 극성 정도, 수상의 비율, 유화제의 농도 등을 조절하는 것이 매우 중요하다. 안정도에 영향을 주는 여러 가지 요소 중에서 유화제의 구조에 따라 유화가능여부와 안정도가 어떻게 달라지는지에 초점을 맞추고, 유화제를 구조적으로 polyglyceryl ester 계열, silicone 계열, sugar 계열 유화제 등으로 나누어서 실험을 진행하였다. 또한 유상에 사용되는 오일의 실리콘 함량을 다르게 하여 유화제의 유화 능력을 검토하였다. 실험 결과를 참고하여 유화제에 따른 에멀젼의 입자, 점도의 경시 변화 등의 w/o 에멀젼의 특성을 찾아내고, 여러 조건에서 에멀젼의 안정도를 관찰하였다.

Physicochemical Properties of the Exopolysaccharides Produced by Marine Bacterium Zoogloea sp. KCCM10036

  • Lim, Dong-Jung;Kim, Jong-Deog;Kim, Min-Yong;Yoo, Sang-Ho;Kong, Jai-Yul
    • Journal of Microbiology and Biotechnology
    • /
    • 제17권6호
    • /
    • pp.979-984
    • /
    • 2007
  • The physicochemical properties of the exopolysaccharide (EPS) produced by marine bacterium Zoogloea sp. KCCM10036 were investigated. Two types of isolated EPSs were shown to have average relative molecular masses $(M_r)\;of\;4.07{\times}10^6$ of CBP (cell-bound polysaccharide) and $3.43{\times}10^6$ of WSP (water-soluble polysaccharide), respectively. When the CBP was utilized as an emulsifier, it stabilized the emulsifier, for up to 148 h. Compared with other commercially available hydrocolloids such as xanthan gum, the Tween series, and Triton, the CBP showed much better emulsifying capability on a water-in-oil system. Phase separation occurred in the Tween series after 24 h, whereas the emulsion was better stabilized by the CBP. The CBP thus has potential as an emulsifying agent in commercial emulsions. The flocculating activity was also greatest at 0.01% (w/v) and decreased at higher concentrations than the optimized concentration of the WSP and CBP. The results also showed that both types of expolysaccharides from Zoogloea sp. had excellent flocculating activity.

겔 작용에 의한 쿼터늄-18 헥토라이트를 사용한 Water-in-Oil 에멀젼의 안정화 기술 (Stabilizing Technology of water-in-Oil Emulsification with Quaternium-18 Hectorite by Gelling Action)

  • 김인영;조춘구;이주동
    • 대한화장품학회지
    • /
    • 제29권1호
    • /
    • pp.135-150
    • /
    • 2003
  • This study is described the stabilizing technology of water-in-oil (w/o) emulsion and the mechanism of emulsification with quaternium-18 hectorite (Q-18 HTRT) by swelling action. When Q-18 HTRT is dispersed in oil, it swells and constructs card-house structure adding ethanol, and formation of water phase is caused by hydrogen bonding. The gelling activities of Q-18 HTRT were excellent such as mineral oil, squalane, cetostearyl isononanoate, isostearic acid, cetyl octanoate, octyl dodecanol and so on. Especially, when oil gel containing Q-18 HTRT passed one to three times by Roll mill. It made the W/O emulsion cream (W/O-ECRM) having 2.0 w/w% of Q-18 HTRT and also produced the control sample (control) including 3.0 w/w% of cetyl PEG/PPG- l0/l dimethicone. The stability of after 24 weeks, Hardness of W/O-ECRM dropped 7.48%, whereas hardness of control went down 57 71%. As a result of these test emulsification of W/O-ECRM is superior compared with control. In cosmetic, 0-18 HTRT can use as suspending agent, oil adsorbent, emulsifying agent, dispersing agent, viscosifier and pigment.

고분자 계면활성제에 관한 연구(제6보) -알파 술폰 지방산 음이온성 올리고머 계면활성제의 계면성- (Studies on the Polymeric Surface Active Agent(VI) -The Surface Activities of Anionic Oligomer Surfactant with α-Sulfo Alkanoic Acid-)

  • 정노희;박상석;정환경;조경행;남기대
    • 공업화학
    • /
    • 제4권4호
    • /
    • pp.683-691
    • /
    • 1993
  • Sodium dodecyl polyoxyethylene ${\alpha}$-sulfa alkanoates류 15종에 대하여 표면장력, 기포력 및 그 안정성, 유화력, 분산성, 습윤성 및 가용화능 등의 계면활성을 실험하였다. 이들 시료의 묽은 수용액에 대한 임계미셀농도는 $10^{-4}{\sim}10^{-5}mo1/{\ell}$ 범위였고 그 농도범위에서의 표면장력은 30~47dyne/cm였으며, 일정농도 수용액에 대한 기포력 및 그 안정성, 벤젠 및 대두유에 대한 유화력, 탄산칼슘 및 산화철에 대한 분산성, 그리고 습윤력과 Orange OT에 대한 가용화능을 실험하여 검토한 결과 O/W형 유제 및 분산제로서의 응용성이 기대된다.

  • PDF

Production and Characterization of Lipopeptide Biosurfactant from Bacillus subtilis A8-8

  • Lee Sang-Cheol;Yoo Ju-Soon;Kim Sun-Hee;Chung Soo-Yeol;Hwang Cher-Won;Joo Woo-Hong;Choi Yong-Lark
    • Journal of Microbiology and Biotechnology
    • /
    • 제16권5호
    • /
    • pp.716-723
    • /
    • 2006
  • A biosurfactant-producing bacterial strain was selected from oil-contaminated soil because of its ability to degrade crude oil and tributyrin $(C_{4:0})$. The strain was identified as Bacillus subtilis A8-8 based on its morphological, biochemical, and physiological characteristics. When B. subtilis A8-8 was grown with crude oil as the sole carbon source, the biosurfactant from the strain emulsified crude oil, vegetable oil, and hydrocarbons. Soybean oil was the optimum substrate for the emulsifying activity and emulsion stability of the biosurfactant, both of which were superior to those of several commercially available surfactants. The biosurfactant was purified by a procedure including HCl precipitation, methanol treatment, and silica-gel chromatography. The partially purified biosurfactant was analyzed by TLC (thin-layer chromatography), SDS-PAGE, and HPLC and it reduced the surface tension of water from 72 mN/m to 26 mN/m at a concentration of 30 mg/l. Therefore, the purified lipopeptide biosurfactant has strong properties as an emulsifying agent and acts as an emulsion-stabilizing agent.

혼합비이온계면활성제의 조성에 따른 O/W 에멀젼의 유동특성 및 안정성 1. 반전유화법을 이용한 O/W 에멀젼의 상거동 및 유동특성 (The Flow Properties and Stability of O/W Emulsion Composed of Various Mixed Nonionic Surfactants 1. The Phase Behavior and Flow Properties of O/W Emulsion Prepared with the Inversion Emulsification Method)

  • 이호식;김점식
    • 공업화학
    • /
    • 제4권1호
    • /
    • pp.196-203
    • /
    • 1993
  • Glycerin monostearate, polyoxyethylene(100) monostearate, polyoxyethylene(20) sorbitan monostearate를 혼합한 유화제를 분산상인 liquid paraffin, beeswax 혼합물에 용해한 후 연속상인 propylene glycol 수용액을 첨가하는 방법인 agent-in-oil법을 적용한 반전유화법에 의해 O/W 에멀젼을 제조하였고, 제조과정에서 나타나는 상거동 및 점성거동을 관찰하였다. 연속상을 주가함에 따라 액정 영역과 백타겔 영역이 존재하는 유화제 조성(HLB 10.1~12.3)에서만 미세하고 균일한 에멀젼이 형성되었으며, 유상${\rightarrow}$액정상${\rightarrow}$겔상${\rightarrow}$O/W 에멀젼으로 상변화가 일어남을 알 수 있었다. 제조된 에멀젼의 전단속도에 따른 전단응력곡선으로부터 항복치가 존재함에 따라 에멀젼 입자간의 내부구조가 형성됨을 알 수 있었고, 전단력에 의한 내부구조의 파괴가 겉보기상으로는 완전히 비가역적으로 진행되며, 구조 파괴의 척도인 hysteresis loop의 면적은 유화제의 HLB값이 작을수록 큰 것을 알 수 있었다. 시간에 따른 전단응력 변화곡선에서소성점성도의 시간의존성이 큰 것을 확인하였고, 시간유동화현상에 따른 완화시간(${\lambda}$)으로부터 HLB값이 작을수록 상대적 안정성이 큼을 알 수 있었으며, homomixer로 제조한 에멀젼에 비해 반전유화법에 의해 제조한 에멀젼이 더 안정함을 알 수 있었다.

  • PDF