• Journal of Plant Biology
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• 제38권3호
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• pp.275-280
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• 1995

The formation of osmiophilic globules related to the granal lysis has been investigated with a shade plant ginseng (Panax ginseng C. A. Meyer) exposed to full sunlight. The changes of chloroplast were examined as a function of time over 9 days under full sunlight exposure. The ultrastructure of ginseng leaf showed swelling of the granal thylakoid during an early stage of the light exposure. The thylakoid membrane faded and small electron-opaque dots were aggregated on the edges of the granal thylakoid membrane when the exposure time was increased over 1 day. Then, the sahpe of the grana changed into round. After the exposure over 3 days, there appeared many osmiophilic globules with multi-lamellated concentric structure. The globules at this stage were partly accumulated with osmiophilic substances. The outermost membrane of these multi-lamellated osmiophilic globules was attached to the stromal thylakoid membrane connecting to the deforming grana. The osmiophilic globules were elongated after 9 days. In this stage, the multi-lamellated structure was difficult to identify due to severe accumulation of osmiophilic substances. The number of the osmiophilic globules also increased along with the full sunlight exposure time. This observation leads us to believe that the multi-lamellated osmiophilic globules came from the deformation of grana.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2004년도 제5회 압연심포지엄 신 시장 개척을 위한 압연기술
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• pp.11-18
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• 2004

Asymmetric rolling, in which the circumferential velocities of the upper and lower rolls are different, can give rise to intense plastic shear strains and in turn shear deformation textures through the sheet thickness. The ideal shear deformation texture of fcc metals can be approximated by the <111> // ND and $\{001\}<110>$ orientations, among which the former improves the deep drawability. The ideal shear deformation texture for bcc metals can be approximated by the Goss $\{110\}<001>\;and\;\{112\}<111>$ orientations, among which the former improves the magnetic permeability along the <100> directions and is the prime orientation in grain oriented silicon steels. The intense shear strains can result in the grain refinement and hence improve mechanical properties. Steel sheets, especially ferritic stainless steel sheets, and aluminum alloy sheets may exhibit an undesirable surface roughening known as ridging or roping, when elongated along RD and TD, respectively. The ridging or roping is caused by differently oriented colonies, which are resulted from the <100> oriented columnar structure in ingots or billets, especially for ferritic stainless steels, that is not easily destroyed by the conventional rolling. The breakdown of columnar structure and the grain refinement can be achieved by asymmetric rolling, resulting in a decrease in the ridging problem.

• EDISON SW 활용 경진대회 논문집
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• 제4회(2015년)
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• pp.48-52
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• 2015

Control of polymer conformations in heterogeneous confinement plays an important role in natural and engineering processes. We present a simulation study on the conformational structure and dynamics of a single, flexible polymer in a dense array of nanoposts with different sizes and separations, especially, when the volume of the interstitial space formed between four nanoposts is less than the size of the polymer chain. When a polymer is placed in the array of nanoposts, the size of polymer increases compared with that in the absence of nanoposts due to the confinement effect. It is shown that when a polymer is confined in the array of nanoposts the chain is elongated in the direction parallel to the nanoposts. As the interstitial volume between four nanoposts decreases either by increasing the nanopost diameter or by decreasing the separation between nanoposts, the chain elongation becomes more pronounced. On the contrary, the polymer size varies in a non-monotonic fashion, with an initial elongation followed by a chain contraction, as the interstitial volume is reduced both by increasing the nanopost diameter and decreasing the separation at the same time while keeping constant the width of the passageway between two nanoposts. The simulation analysis shows that the non-monotonic dependence of polymer size is determined by interplay between the chain alignment along the nanoposts in each interstitial volume and the chain spreading through passageways over several interstitial volume.

• Journal of Welding and Joining
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• 제23권5호
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• pp.61-68
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• 2005

Dissimilar joining of Al 6013-T4 alloys and austenite stainless steel was carried out using friction stir welding technique. Microstructures near the weld zone and mechanical properties of the joint have been investigated. Microstructures in the stainless steel side were composed of the heat affected zone and the plastically deformed zone, while those in the Al alloy side were composed of the recrystallized zone including stainless steel particles, the thermo-mechanically affected zone and the heat affected zone. TEM micrographs revealed that the interface region was composed of the mixed layers of elongated stainless steel and ultra-fine grained Al alloy with lamella structure and intermetallic compound layer. Thickness of the intermetallic layer was approximately 300nm and was identified as the A14Fe with hexagonal close packed structure. Mechanical properties, such as tensile and fatigue strengths were lower than those of 6013 Al alloy base metal, because tool inserting location was deviated to Al alloy from the butt line, which resulted in the lack of the stirring.

• 한국수산과학회지
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• 제56권6호
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• pp.916-922
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• 2023

An abnormal shape of Bathyraja brachyurops was first reported from the catch of a bottom trawl in the southwest Atlantic Ocean in June 2022. Both pectoral fins of the specimen did not fuse with the head, resulting in a horn-like structure separated from the sides of the eyes. Analysis of mitochondrial DNA cytochrome c oxidase subunit I sequences showed that our specimen was perfectly matched to Bathyraja brachyurops registered with the National Center for Biotechnology Information. Our specimen possessed the following morphological features: a pair of flexible but elongated and pointed horns on the head; rough dorsal disc, densely covered with numerous small denticles on the head, anterior margin of pectoral fins and median line of the disc; a thorn between the first and second dorsal fins; and a pair of large ocelli at the base of pectoral fins. Unlike the normal B. brachyurops, our specimen had a slender clasper and no nuchal thorns, which may be related to the morphological abnormality. The horn-like structure on the head may be owing to the lack of fusion between the pectoral fins and head during early embryonic development.

• 분석과학
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• 제18권5호
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• pp.381-385
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• 2005

The title compound, $\{H_2NCH_2CH_2NH_2CH_2CH_2\}\{Cu(H_2O)_6\}(SO_4)_2$, I, has been synthesized under solvo/hydrothermal conditions and their crystal structure analyzed by X-ray single crystallography. Compound I crystallizes in the monoclinic system, $P2_1/n$ space group with a = 6.852(1), b = 10.160(2), $c=11.893(1){\AA}$, ${\beta}=92.928(8)^{\circ}$, $V=826.9(2){\AA}^3$, Z = 2, $D_x=1.815g/cm^3$, $R_1=0.031$ and ${\omega}R_2=0.084$. The crystal structure of the piperazine templated Cu(II)-sulfate demonstrate zero-dimensional compound constituted by doubly protonated piperazine cations, hexahydrated copper cations and sulfate anions. The central Cu atom has a elongated octahedral coordination geometry. The crystal structure is stabilized by three-dimensional networks of the intermolecular $O_{water}-H{\cdots}O_{sulfate}$ and $N_{pip}-H{\cdots}O_{sulfate}$ hydrogen bonds between the water molecules and sulfate anions and protonated piperazine cations. Based on the results of thermal analysis, the thermal decomposition reaction of compound I was analyzed to have three distinctive stages.

• 한국재료학회지
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• 제29권6호
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• pp.392-397
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• 2019

A cold roll-bonding process is applied to fabricate an AA6061/AA5052/AA6061 three-layer clad sheet. Two AA6061 and one AA5052 sheets of 2 mm thickness, 40 mm width, and 300 mm length are stacked, with the AA5052 sheet located in the center. After surface treatment such as degreasing and wire brushing, sample is reduced to a thickness of 1.5 mm by multi-pass cold rolling. The rolling is performed at ambient temperature without lubricant using a 2-high mill with a roll diameter of 400 mm at rolling speed of 6.0 m/sec. The roll bonded AA6061/AA5052/AA6061 complex sheet is then hardened by natural aging(T4) and artificial aging(T6) treatments. The microstructures of the as-roll bonded and age-hardened Al complex sheets are revealed by optical microscopy; the mechanical properties are investigated by tensile testing and hardness testing. After rolling, the roll-bonded AA6061/AA5052/AA6061 sheets show a typical deformation structure in which grains are elongated in the rolling direction. However, after T4 and T6 aging treatment, there is a recrystallization structure consisting of coarse equiaxed grains in both AA5052 and AA6061 sheets. The as roll-bonded specimen shows a sandwich structure in which an AA5052 sheet is inserted into two AA6061 sheets with higher hardness. However, after T4 and T6 aging treatment, there is a different sandwich structure in which the hardness of the upper and lower layers of the AA6061 sheets is higher than that of the center of the AA5052 sheet. The strength values of the T4 and T6 age-treated specimens are found to increase by 1.3 and 1.4 times, respectively, compared to that value of the starting material.

• 한국재료학회지
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• 제33권9호
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• pp.367-371
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• 2023

In this study we examine variations in the structure of perovskite compounds of LaBa₂Cu₂O₉, LaBa2₂CaCu₃O₁₂ and LaBa₂Ca₂Cu₅O₁₅ synthesized using the solid state reaction method. The samples' compositions were assessed using X-ray fluorescence (XRF) analysis. The La: Ba: Ca: Cu ratios for samples LaBa₂Cu₂O₉, LaBa2₂CaCu₃O₁₂ and LaBa₂Ca₂Cu₅O₁₅ were found by XRF analysis to be around 1:2:0:2, 1:2:1:3, and 1:2:2:5, respectively. The samples' well-known structures were then analyzed using X-ray diffraction. The three samples largely consist of phases 1202, 1213, and 1225, with a trace quantity of an unknown secondary phase, based on the intensities and locations of the diffraction peaks. According to the measured parameters a, b, and c, every sample has a tetragonal symmetry structure. Each sample's mass density was observed to alter as the lead oxide content rose. Scanning electron microscope (SEM) images of the three phases revealed that different Ca-O and Cu-O layers can cause different grain sizes, characterized by elongated thin grains, without a preferred orientation.

• 한국화재소방학회논문지
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• 제25권6호
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• pp.83-88
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• 2011

본 연구에서는 전기기기 및 가전기기 등의 배선으로 사용되는 비닐코드의 구조 및 특성을 제시하고, 에너지원의 종류에 따라 소손된 비닐평형코드(VFF, $1.25mm^2$)의 실체 사진 및 용융된 도체의 금속 단면 구조를 분석하였다. 정상 VFF는 소선 여러 가닥을 꼬아서 제작되었으며, 도체의 표면은 적갈색이다. 또한 도체의 금속 조직 분석에서 그레인이 연신된 것을 알 수 있었다. 일반 화염에 의해 소손된 VFF의 표면은 절연물이 탄화되어 도체의 표면에 융착되었고, 윤기가 없는 것을 알 수 있었다. 또한 용융 부분의 단면 구조 분석에서 일정한 모양의 보이드가 형성되었고, 전선 고유의 연신 구조는 확인할 수 없었다. 통전중인 VFF에 외부 화염이 인가되어 소손된 용융 도체의 단면 분석에서 전선 고유의 연신 구조는 없었고, 불규칙적인 보이드 및 주상 조직 등이 성장한 것을 알 수 있었다. 과전류에 의해 소손된 VFF는 표면이 고르게 탄화되었으며, 용융된 도체의 단면 구조 분석에서 수지상 조직의 성장이 확인되었다. 단락에 의해 용융된 VFF의 특성 분석에서 표면의 일부가 오염되었지만 약간의 윤기가 있고, 용융되어 재결합한 부분이 둥근 모양을 나타냈다. 또한 금속 현미경을 이용한 단면 구조 분석에서 경계면 및 주상 조직 등이 확인되었고, 용융된 도체 이외의 부분에서는 정상 구리와 같은 비정질체인 구조가 확인되었다.

• Steel and Composite Structures
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• 제21권5호
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• pp.1031-1043
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• 2016

Optimization of the construction scheme of the cable-strut tensile structure based on error sensitivity analysis is studied in this paper. First, the element length was extracted as a fundamental variable, and the relationship between element length change and element internal force was established. By setting all pre-stresses in active cables to zero, the equation between the pre-stress deviation in the passive cables and the element length error was obtained to analyze and evaluate the error effects under different construction schemes. Afterwards, based on the probability statistics theory, the mathematical model of element length error is set up. The statistical features of the pre-stress deviation were achieved. Finally, a cable-strut tensile structure model with a diameter of 5.0 m was fabricated. The element length errors are simulated by adjusting the element length, and each member in one symmetrical unit was elongated by 3 mm to explore the error sensitivity of each type of element. The numerical analysis of error sensitivity was also carried out by the FEA model in ANSYS software, where the element length change was simulated by implementing appropriate temperature changes. The theoretical analysis and experimental results both indicated that different elements had different error sensitivities. Likewise, different construction schemes had different construction precisions, and the optimal construction scheme should be chosen for the real construction projects to achieve lower error effects, lower cost and greater convenience.