• 제목/요약/키워드: electron microscope analysis

검색결과 1,021건 처리시간 0.032초

$C_4A_3\bar{S}$계 클린커 및 하소돌로마이트를 자극제로 한 고환산염 슬라그 시멘트의 수화반응 (Hydration of Supersulphated Slag Cement with $C_4A_3\bar{S}$ type Clinker and Calcined Dolomite as Activator)

  • 박춘근;최상홀
    • 한국세라믹학회지
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    • 제22권2호
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    • pp.33-38
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    • 1985
  • The hydration of supersulphated slag cement which is the mixture of granuloated blast furnace slag anhydrite $C_4A_3$ type clinker and calcined dolomite was studied by X-ray diffraction differential thermal analysis scanning electron microscope observation and measurement of the rate of heat liberation. The main hydrates were ettrigite and C-S-H. This supersulphated slag cement enhanced rapid-hardening and increased in strength at early stage due to the much of ettrigite. Furthermore the hardened cement became stronger due to the C-S-H that was produced from the hydration of the $eta$-$C_2S$ in $C_4A_3$ type clinker and the hydration of the dissolved components from slag at later period.

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Effect of fiber-matrix adhesion on the fracture behavior of a carbon fiber reinforced thermoplastic-modified epoxy matrix

  • Carrillo-Escalante, H.J.;Alvarez-Castillo, A.;Valadez-Gonzalez, A.;Herrera-Franco, P. J.
    • Carbon letters
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    • 제19권
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    • pp.47-56
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    • 2016
  • In this study, the fracture behavior of a thermoplastic-modified epoxy resin reinforced with continuous carbon fibers for two levels of fiber-matrix adhesion was performed. A carbon fiber with commercial sizing was used and also treated with a known silane, (3-glycidoxy propyl trimethoxysilane) coupling agent. Toughness was determined using the double cantilever test, together with surface analysis after failure using scanning electron microscope. The presence of polysulfone particles improved the fracture behavior of the composite, but fiber-matrix adhesion seemed to play a very important role in the performance of the composite material. There appeared to be a synergy between the matrix modifier and the fiber-matrix adhesion coupling agent.

전자현미경내 마이크로 절삭의 화상처리에 의한 절삭 기구 해석 (Analysis of Cutting Mechanism by Image Processing on Micro-Cutting in SEM)

  • 허성중
    • 한국공작기계학회논문집
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    • 제12권3호
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    • pp.89-95
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    • 2003
  • This research analyzes the cutting mechanism of A1100-H18 of commercially pure aluminum by image processing in SEM(Scanning Electron Microscope) for the measurement of strain rate distribution near a cutting edge in orthogonal micro-cutting. The distribution is measured using various methods in order. The methods are in-situ observations of cutting process in SEM, inputting image data, a computer image processing, calculating displacements by SSDA(Sequential Similarity Detection Algorithm) and calculating strain rates by FEM. The min results obtained are as follows: (1)It enables to measure a microscopic displacement near a cutting edge. (2) An application of this system to cutting process of various materials will help to make cutting mechanism clear.

열처리된 친수성 카본 페이퍼 전극의 전기 물 분해 특성 (Electrode Properties for Water Electrolysis of Hydrophilic Carbon Paper with Thermal Anneal)

  • 유일한;서형탁
    • 한국재료학회지
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    • 제26권5호
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    • pp.241-245
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    • 2016
  • Hydrogen is considered a potential future energy source. Among other applications of hydrogen, hydrogen-rich water is emerging as a new health care product in industrial areas. Water electrolysis is typically used to generate a hydrogen rich water system. We annealed 10AA carbon paper in air to use it as an electrode of a hydrogen rich water generator. Driven by annealing, structural changes of the carbon paper were identified by secondary electron microscope analysis. Depending on the various annealing temperatures, changes of the hydrophilic characteristics were demonstrated. The crystal structures of pristine and heat-treated carbon paper were characterized by X-ray diffraction. Improvement of the efficiency of the electrochemical oxygen evolution reaction was measured via linear voltammetry. The optimized annealing temperature of 10AA carbon paper showed the possibility of using this material as an effective hydrogen rich water generator.

세라믹 접합부재에 대한 파괴역학인자 및 파면 해석 (Analysis of Fracture Mechanics Parameter and Fracture Surface in Bonded Ceramic Joints)

  • 김기성
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 1997년도 춘계학술대회 논문집
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    • pp.156-163
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    • 1997
  • Recently, attempts have been made to be join ceramics to metals in order to make up for the brittleness of ceramics. The difference in the coefficients of linear expansion of the two materials joined at high temperature will cause residual stress, which has a strong influence on the strength of the bonded joints. In this paper, the residual stress distribution and stress intensity factors of the ceramic/metal bonded joints were analyzed by 2-dimensional elastic boundary element method. Fracture toughness tests of ceramic/metal bonded joints with an interface crack were carried out. So the advanced method of quantitative strength evaluation for ceramic/metal bonded joints is to be suggested. Fracture surface and crack propagation path were observed using scanning electron microscope.

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Three-Dimensional Self-Assembly of Gold Nanoparticles Using a Virus Scaffold

  • Kang, Aeyeon;Lee, Young-Mi;Kang, Hyo Jin;Chung, Sang Jeon;Yun, Wan Soo
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.651-651
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    • 2013
  • Templated strategy is a very powerful tool for creating multi-dimensional self assembly of nanomaterials. Since viral protein cages have a uniform size with a well-defined structure, they can serve as an excellent template for the formation of a three-dimensional self-assembly of synthetic nanoparticles. In this study, we have examined the feasibility of the 3D self-assembly of gold nanoparticles of various sizes using a brome mosaic virus (BMV) capsid with cysteine groups expressed on its surface as a scaffold for the assembly. It was found that the three-dimensional clusters of gold nanoparticles with a designed structure were attainable by this approach, which was verified by transmission electron microscope (TEM) and dynamic light scattering (DLS) analysis.

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TFT-LCD BLU용 고압 케이블의 재료특성 및 제조공정 개선을 통한 성능 향상 (Evaluation in Performance of High Voltage Cable for BLU of TFT-LCD by Improvement for Material and Manufactured Process)

  • 정진도;김재훈;구경완;황승민
    • 전기학회논문지P
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    • 제58권4호
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    • pp.495-498
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    • 2009
  • To improve the efficiency of the high voltage cable for BLU(backlight unit) of TFT-LCD(Thin Film Transistor-Liquid Crystal Display), the analysis for the trial products(UL3239, UL3633) is conducted by using SEM(scanning electron microscope) and EDX(Energy Dispersive X-ray Spectroscopy). The result that it is possible to accumulate the know-how to about stranding pitch through effective improvement of stranding process. The troubles which are the badness of withstanding voltage and tensile strength etc. are solved by development of excellent material. Furthermore, phenomenon of conductor unfasten in the harness work is solved by improvement of the stranding wire process.

Uranium Isotopic Ratio Analysis of U-Bearing Particulates By SIMS in CIAE

  • Yonggang, Zhao
    • 한국방사성폐기물학회:학술대회논문집
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    • 한국방사성폐기물학회 2004년도 Proceedings of the 4th Korea-China Joint Workshop on Nuclear Waste Management
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    • pp.257-259
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    • 2004
  • In this paper measurement method of uranium isotope ratio of uranium-bearing particles in swipe samples was introduced; Swipe sample screening program was proposed on the basis of studying various destructive assay and non-destructive assays. Scanning electron microscope(SEM) equipped with an energy dispersive X-ray fluorescence(XRF) system was applied to locate the deposited uranium-containing particles on the graphite support, particle's composition and size can be identified. Some isotope ratio results were compared with those of other bulk analytical methods; By measuring the same prepared sample, we got the U-particle isotopic ratio data similar to those from IAEA NWAL, indicating that our operation parameters and experimental conditions are viable and can be used for measurement of U-particle isotopic ratio from swipe samples.

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공구강의 표면특성에 미치는 플라즈마 질화처리의 영향 (Effects of Plasma Nitriding on the Surface Characteristics of Tool Steels)

  • 이호종;최한철
    • 한국표면공학회지
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    • 제36권2호
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    • pp.206-213
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    • 2003
  • Effects of plasma nitriding on the surface characteristics of tool steels have been investigated using wear tester, micro-hardness tester and scanning electron microscope (SEM) Commercial SKD 11 and SM45 alloy were used as specimens and were plasma nitrided using a plasma nitriding equipment for 5 hr and 10hr at $500^{\circ}C$. Microstructure and phase analysis were performed using SEM and XRD. It was found that plasma nitriding for lour at $500^{\circ}C$, compared with plasma nitriding for 10hr at $500^{\circ}C$, had a thick nitrided layer and produced a layer with good wear resistance and hardness as nitriding time increased. SKD11 alloy showed that wear resistance and hardness decreased, whereas surface roughness increased, compared with SM45 alloy.

철도차량용 유리섬유직물/페놀릭 복합재의 가속노화 특성 (Aging Characteristics of Glass Fabric/Phenolic Composites in Train Carbody)

  • 윤성호;남정표;황영은;신광복
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2004년도 춘계학술대회 논문집
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    • pp.352-357
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    • 2004
  • In this study. the effects of combined environmental factors on mechanical and thermal analysis properties of graphite/epoxy composites were evaluated through a 2.5KW accelerated environmental aging tester. Environmental factors such as temperature. moisture, and ultraviolet were considered. A xenon-arc lamp was utilized for ultraviolet light. and exposure times of up to 3000 hours were applied. Several types of specimens - tensile, bending, and shear specimens those are warp direction and fill direction were used to investigate the effects of environmental factors on mechanical properties of the composites. The glass fabric $\sharp$650/AP300 was used for the fabrication of specimens. Mechanical degradations for tensile, bending and shear properties were evaluated through a UTM. Also. storage shear modulus. loss shear modulus, and tan $\delta$ were measured as a function of exposure times through a dynamic mechanical analyzer. Finally exposed surfaces of the composites were examined using II scanning electron microscope.

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