• Title/Summary/Keyword: electron microscope analysis

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Ultrastructural and Molecular Characterization of Surirella atomus Hustedt 1955 (Bacillariophyta, Surirellalceae), A Newly Recorded Species in Korea

  • An, Sung Min;Noh, Jae Hoon;Kim, Ji Hoon;Kang, Nam Seon
    • Ocean and Polar Research
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    • v.43 no.4
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    • pp.245-253
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    • 2021
  • Surirella atomus Hustedt 1955, surirelloid diatom, were obtained from Hampyeong Bay, Mu-an, in the west coast of Korea. We describe the first record of S. atomus in Korea and report its ultrastructure and molecular characteristics for the first time. For molecular analysis, rbcL gene and cob gene were sequenced. This species is very small in size, making it difficult to observe its morphological features under a light microscope. Even with a scanning electron microscope, it has no unique structure in the valve. It is morphologically very simple. This rare species was known as a marine benthic species. However, it appears to be widely distributed in marine, freshwater, and brackish environments according to the literature documenting this species. In terms of phylogeny, S. atomus has been tentatively linked to Petrodictyon gemma, but the phylogenetic placement of S. atomus seems to be still uncertain, in a manner that is similar to S. febigeri. However, morphological observations derived from this study suggest that this species belongs to the genus Surirella.

Effects of Al in TRIP steels on microstructure and phase transformation (TRIP강에서 Al이 미세구조와 상변태에 미치는 영향)

  • Lim, N.S.;Kim, S.I.;Park, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.10a
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    • pp.213-216
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    • 2009
  • In this study, three cold-rolled TRIP steels containing different Al content (0.04wt%, 1.0 wt.% and 2.00wt%) were fabricated to understand the complex effects of Al in TRIP steel. The influences of Al on microstructural evolution of cold-rolled TRIP steels have been analyzed by using advanced analysis techniques, such as transmission electron microscope (TEM) and three dimensional atom probe tomography (3D-APT). TEM results revealed that second phases such as bainte and retained austenite decrease with increase of Al content. In addition, 3D-APT was used to characterize atomic-scale distribution of alloying elements at the constituent phases. Through these analysis techniques, the advanced characteristics of constituent microstructure in TRIP steels were identified depending on Al contents in TRIP steels.

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Effects of Crystallization Behavior on Microwave Dielectric Properties of CaMgSi2O6 Glass-Ceramics

  • Choi, Bo Kyeong;Kim, Eung Soo
    • Journal of the Korean Ceramic Society
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    • v.50 no.1
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    • pp.70-74
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    • 2013
  • Dependence of microwave dielectric properties on the crystallization behaviors of $CaMgSi_2O_6$ (diopside) glass-ceramics was investigated with different heat treatment methods (one and/or two-step). The crystallization behaviors of the specimens, crystallite size and degree of crystallization, were evaluated by differential thermal analysis (DTA), scanning electron microscope (SEM) and X-ray diffraction (XRD) analysis by combined Rietveld and reference intensity ratio (RIR) methods. With an increase in heattreatment temperature, the dielectric constant (K) and the quality factor (Qf) increased due to the increase of the crystallite size and degree of crystallization. The specimens heat-treated by the two-step method had a higher degree of crystallization than the specimens heat-treated by the one-step method, which induced improvement in the quality factor (Qf) of the specimens.

The Destruction Effects of Semiconductors by High Power Electromagnetic Wave (고출력 과도전자파에 의한 반도체 소자의 파괴효과)

  • Hwang, Sun-Mook;Hong, Joo-Il;Huh, Chang-Su
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.56 no.9
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    • pp.1638-1642
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    • 2007
  • This paper investigated the destruction effect of the semiconductors by impact of high power electromagnetic wave. The experiments is employed as an open-ended waveguide to study the destruction effects on semiconductor using a 2.45 GHz 600 W Magnetron as a high power electromagnetic wave. The semiconductors are located at a distance of $31cm\sim40cm$ from the open-ended waveguide and are composed of a LED drive circuit for visual discernment. Also the chip condition of semiconductor is observed by SEM(Scanning Electron Microscope) analysis. The semiconductor are damaged by high power electromagnetic wave at about 860 V/m. The SEM analysis of the destructed devices showed onchipwire and bondwire destructions. Based on the result, semiconductor devices should have plan to protect the semiconductor devices form high power electromagnetic wave. And the database from this experiment provides the basis for future investigation.

Block Lifting Analysis to Examine the Cause of Cracking in the Hopper Top Plate (블록 리프팅 시 Hopper Tank부 균열 발생 가능성 검토를 위한 구조해석)

  • KIM SANG-IL
    • Journal of Ocean Engineering and Technology
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    • v.20 no.1 s.68
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    • pp.16-19
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    • 2006
  • With the fast growth of the shipbuilding industry, the number of lifting lugs used every year has reached onehundred. This paper is aimed at examining the cause of cracking in the hopper top plate, due to block lifting. First of all, we have investigated the fracture surface in the occurrence position of the crack of the hopper top plate, using the scanning electron microscope. In this study, we have evaluated the structural strength for COT super block under present lifting conditions. For this purpose, the equivalent stresses have been calculated by linear elastic analysis, using the finite element program ABAQUS.

A Study on the Ion Permeability Characteristics in Nano-Polymer Membrane Structures (나노고분자막 구조의 이온투과 특성에 관한 연구)

  • Kim, Yoo-Young
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.15 no.1
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    • pp.133-137
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    • 2006
  • Ion permeability characteristics in nano-polymer membrane structures are performed to investigate the chemical composition and characteristics of MEA(Membrane Electrolyte Assembly) which is one of the most important parts to decide the performance in PEMFC(Polymer Electrolyte Membrane Fuel Cell) system. Subsequently, the MEA manufacturing process is presented for the uniformed MEA product. In the meantime, the analysis of SEM(Scanning Electron Microscope) is carried out in order to investigate the joint aspect and chemical composition of MEA. As a result of SEM analysis, it is found that the bonded catalyst and carbon composition contain the reasonable amount to get unit cell output. It is also found that the humidification gives the better performance result slightly.

A Study of Characteristics of Weft Used in Wig Manufacturing (가발에 사용되는 원사의 특성 연구)

  • Lim, Sun-Nye
    • Textile Coloration and Finishing
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    • v.24 no.3
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    • pp.204-212
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    • 2012
  • This study was used a thermogravimetric analyzer to determine thermal characteristics, a hair analysis system to examine morphological changes of wefts-human hair, poly vinyl chloride(PVC) and polyethylene terephthalate (PET)-used in manufacturing wigs. According to a flammability test on human hair and synthetic wefts for wigs, the best results were observed in human hair. According to a thermal test, PET was the best in terms of thermal stability. Also good tensile strength was observed as well. In a scanning electron microscope observation, no human hair scale layer was found because of chemical treatment. In the PVC sample, homogeneous unevenness was observed. Due to a lack of human hair supply and increase in its price, recently, PET weft has emerged as a great substitution for human hair. Because it can be curled using an electric curling device and is more efficient than the conventional non-flammable material PVC in terms of thermal resistance, it will become the next-generation weft for wigs.

The Effects of Ball Size on Attritor Efficiency in the Processing of RBAO Ceramics (RBAO 세라믹스 공정에서 어트리터 효율에 미치는 볼 크기의 영향)

  • 김일수;강민수;박정현
    • Journal of the Korean Ceramic Society
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    • v.35 no.4
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    • pp.406-412
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    • 1998
  • The reaction bonded alumina ceramics was prepared through the addition of each SiC and ZrO2 powder to the mixture of Al metal powder and Al2O3 The mono sized (3mm) and biodal sized (3mm+5mm) balls were used in attrition milling of Al and starting powders. The milling efficiency of both cases was compared by the analysis of particle size and X-ray diffraction. After the forming and sintering of each powder batchs the weight gains dimensional changes and densities were determined. The specimens were investigated by X-ray diffraction analysis and scanning electron microscope. Bimodal sized balls had better milling effect than single ball size in the milling of Al powder. However in the milling which ceramic powders mono sized the green body during the reaction sintering at 1$600^{\circ}C$ for 5 hour was about 10% The densities attained the values of 92-98% theoretical. The SiC added specimen that was milled with 3mm ball media had 96% theoretical density and dense microstructure.

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Charaterization of GaN Films Grown on Si(100) by RF Magnetron Sputtering (RF magnetron sputtering 방법에 의해 Si(100) 기판 위에 성장된 GaN 박막의 특성에 대한 연구)

  • 이용일;성웅제;박천일;최우범;성만영
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.570-573
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    • 2001
  • In this paper, GaN films have been grown on SiO$_2$/Si(100) substrates by RF magnetron sputtering. To obtain high quality GaN films, we used ZnO buffer layer and modified the process conditions. The charateristics of GaN films on RF power, substrate temperature and Ar/N$_2$gas ratio have been investigated by Auger electron spectroscopy and X-ray diffraction analysis. At RF power 150W, substrate temperature 500 $^{\circ}C$ and Ar/N$_2$=1:2 gas ratio, we could grow high quality GaN films. Through the atomic force microscope and photoluminescence analysises, it was observed that the crystallization of GaN films was improved with increasing annealing temperature and the optimal crystallization of GaN films was found at 1100 $^{\circ}C$ annealing temperature.

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Fracture Characteristics and Stress Analysis of $Si_3N_4/SM45C$ Joint ($Si_3N_4/SM45C$ 접합부의 응력해석 및 파괴특성)

  • 김기성
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 1998.10a
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    • pp.248-253
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    • 1998
  • Recently, the uses of Ceramic/metal bonded joints, resin/metal joints, adhesive joints, composite materials which are composed of dissimiliar materials have increased in various industry fields. Since the ceramic/metal bonded joints material is made at a high temperature, residual stress distributions due to differences in material properties were investigated by varying material parameters. The two dimensional finite element analysis was performed to study residual stress distribution in Si3N4/SM45C bonded joint with a copper interlayer between the silicon nitride(Si3N4) and the structural carbon steel(SM45C) and 4-point bending tests were carried out under room temperature. Fracture surface and crack propagation path were observed using scanning electron microscope and characteristics of its fracture was discussed.

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